One of the most intriguing protein materials found in nature is bone, a material composed of assemblies of tropocollagen molecules and tiny hydroxyapatite mineral crystals that form an extremely tough, yet lightweight, adaptive and multifunctional material. Bone has evolved to provide structural support to organisms, and therefore its mechanical properties are of great physiological relevance. In this article, we review the structure and properties of bone, focusing on mechanical deformation and fracture behavior from the perspective of the multidimensional hierarchical nature of its structure. In fact, bone derives its resistance to fracture with a multitude of deformation and toughening mechanisms at many size scales ranging from the nanoscale structure of its protein molecules to the macroscopic physiological scale.

On the Mechanistic Origins of Toughness in Bone

BACKGROUNDMetallic components are the cornerstone of modern industries such as aviation, aerospace, automobile manufacturing, and energy production. The stringent requirements for high-performance metallic components impede the optimization of materials selection and manufacturing. Laser-based additive manufacturing (AM) is a key strategic technology for technological innovation and industrial sustainability. As the number of applications increases, so do the scientific and technological challenges. Because laser AM has domain-by-domain (e.g., point-by-point, line-by-line, and layer-by-layer) localized forming characteristics, the requisite for printing process and performance control encompasses more than six orders of magnitude, from the microstructure (nanometer- to micrometer-scale) to macroscale structure and performance of components (millimeter- to meter-scale). The traditional route of laser-metal AM follows a typical “series mode” from design to build, resulting in a cumbersome trial-and-error methodology that creates challenges for obtaining high-performance goals.ADVANCESWe propose a holistic concept of material-structure-performance integrated additive manufacturing (MSPI-AM) to cope with the extensive challenges of AM. We define MSPI-AM as a one-step AM production of an integral metallic component by integrating multimaterial layout and innovative structures, with an aim to proactively achieve the designed high performance and multifunctionality. Driven by the performance or function to be realized, the MSPI-AM methodology enables the design of multiple materials, new structures, and corresponding printing processes in parallel and emphasizes their mutual compatibility, providing a systematic solution to the existing challenges for laser-metal AM. MSPI-AM is defined by two methodological ideas: “the right materials printed in the right positions” and “unique structures printed for unique functions.” The increasingly creative methods for engineering both micro- and macrostructures within single printed components have led to the use of AM to produce more complicated structures with multimaterials. It is now feasible to design and print multimaterial components with spatially varying microstructures and properties (e.g., nanocomposites, in situ composites, and gradient materials), further enabling the integration of functional structures with electronics within the volume of a laser-printed monolithic part. These complicated structures (e.g., integral topology optimization structures, biomimetic structures learned from nature, and multiscale hierarchical lattice or cellular structures) have led to breakthroughs in both mechanical performance and physical/chemical functionality. Proactive realization of high performance and multifunctionality requires cross-scale coordination mechanisms (i.e., from the nano/microscale to the macroscale).OUTLOOKOur MSPI-AM continues to develop into a practical methodology that contributes to the high performance and multifunctionality goals of AM. Many opportunities exist to enhance MSPI-AM. MSPI-AM relies on a more digitized material and structure development and printing, which could be accomplished by considering different paradigms for AM materials discovery with the Materials Genome Initiative, standardization of formats for digitizing materials and structures to accelerate data aggregation, and a systematic printability database to enhance autonomous decision-making of printers. MSPI-oriented AM becomes more intelligent in processes and production, with the integration of intelligent detection, sensing and monitoring, big-data statistics and analytics, machine learning, and digital twins. MSPI-AM further calls for more hybrid approaches to yield the final high-performance/multifunctional achievements, with more versatile materials selection and more comprehensive integration of virtual manufacturing and real production to navigate more complex printing. We hope that MSPI-AM can become a key strategy for the sustainable development of AM technologies. Download high-res image Open in new tab Download PowerpointMaterial-structure-performance integrated additive manufacturing (MSPI-AM).Versatile designed materials and innovative structures are simultaneously printed within an integral metallic component to yield high performance and multifunctionality, integrating in parallel the core elements of material, structure, process, and performance and a large number of related coupling elements and future potential elements to enhance the multifunctionality of printed components and the maturity and sustainability of laser AM technologies.

Material-structure-performance integrated laser-metal additive manufacturing.

https://spiral.imperial.ac.uk/bitstream/10044/1/73026/9/1-s2.0-S0264127519306021-main.pdf

Review on design and structural optimisation in additive manufacturing: Towards next-generation lightweight structures

As the water-soluble derivative of graphene,graphene oxide (GO), with many functional groups on thesurface, is one of the best candidates for fabricating artificialnacre, because functional surface groups allow for chemicalcross-linking to improve the interfacial strength of theadjacent GO layers. Until now, several methods have beendeveloped to functionalize individual GO sheets and enhancethe resultant mechanical properties, including divalent ion(Mg

/pdf/ultratough-artificial-nacre-based-on-conjugated-cross-linked-4g7k87y26j.pdf

Ultratough artificial nacre based on conjugated cross-linked graphene oxide

Additive manufacturing of industrially-relevant high-performance parts and products is today a reality, especially for metal additive manufacturing technologies. The design complexity that is now possible makes it particularly useful to improve product performance in a variety of applications. Metal additive manufacturing is especially well matured and is being used for production of end-use mission-critical parts. The next level of this development includes the use of intentionally designed porous metals - architected cellular or lattice structures. Cellular structures can be designed or tailored for specific mechanical or other performance characteristics and have numerous advantages due to their large surface area, low mass, regular repeated structure and open interconnected pore spaces. This is considered particularly useful for medical implants and for lightweight automotive and aerospace components, which are the main industry drivers at present. Architected cellular structures behave similar to open cell foams, which have found many other industrial applications to date, such as sandwich panels for impact absorption, radiators for thermal management, filters or catalyst materials, sound insulation, amongst others. The advantage of additively manufactured cellular structures is the precise control of the micro-architecture which becomes possible. The huge potential of these porous architected cellular materials manufactured by additive manufacturing is currently limited by concerns over their structural integrity. This is a valid concern, when considering the complexity of the manufacturing process, and the only recent maturation of metal additive manufacturing technologies. Many potential manufacturing errors can occur, which have so far resulted in a widely disparate set of results in the literature for these types of structures, with especially poor fatigue properties often found. These have improved over the years, matching the maturation and improvement of the metal additive manufacturing processes. As the causes of errors and effects of these on mechanical properties are now better understood, many of the underlying issues can be removed or mitigated. This makes additively manufactured cellular structures a highly valid option for disruptive new and improved industrial products. This review paper discusses the progress to date in the improvement of the fatigue performance of cellular structures manufactured by additive manufacturing, especially metal-based, providing insights and a glimpse to the future for fatigue-tolerant additively manufactured architected cellular materials.

Architected cellular materials: A review on their mechanical properties towards fatigue-tolerant design and fabrication

Architectured structures, particularly functionally graded lattices, are receiving much attention in both industry and academia as they facilitate the customization of the structural response and harness the potential for multi-functional applications. This work experimentally investigates how the severity of density and unit cell size grading as well as the building direction affects the stiffness, energy absorption and structural response of additively manufactured (AM) short fibre-reinforced lattices with same relative density. Specimens composed of tessellated body-centred cubic (BCC), Schwarz-P (SP) and Gyroid (GY) unit cells were tested under compression. Compared to the uniform lattices of equal density, it was found, that modest density grading has a positive and no effect on the total compressive stiffness of SP and BCC lattices, respectively. More severe grading gradually reduces the total stiffness, with the modulus of the SP lattices never dropping below that of the uniform counterparts. Unit cell size grading had no significant influence on the stiffness and revealed an elastomer-like performance as opposed to the density graded lattices of the same relative density, suggesting a foam-like behaviour. Density grading of bending-dominated unit cell lattices showcased better energy absorption capability for small displacements, whereas grading of the stretching-dominated counterparts is advantageous for large displacements when compared to the ungraded lattice. The severity of unit cell size graded lattices does not affect the energy absorption capability. Finally, a power-law approach was used to semi-empirically derive a formula that predicts the cumulative energy absorption as a function of the density gradient and relative density. Overall, these findings will provide engineers with valuable knowledge that will ease the design choices for lightweight multi-functional AM-parts.

Effect of density and unit cell size grading on the stiffness and energy absorption of short fibre-reinforced functionally graded lattice structures

Learning from nature: Bio-inspiration for damage-tolerant high-performance fibre-reinforced composites

Latticing has become a common design practice in additive manufacturing (AM) and represents a key lightweighting strategy to date. Functional graded lattices (FGLs) have recently gained immense traction in the AM community, offering a unique way of tailoring the structural performance. This paper constitutes the first ever investigation on the combination of graded strut- and surface-based lattices with fiber-reinforced AM to further increase the performance-to-weight ratio. The energy absorption behavior of cubic lattice specimens composed of body-centered cubic and Schwarz-P unit cells with different severities of grading but the same mass, considered for uniaxial compression testing and printed by fused deposition modelling of short fiber-reinforced nylon, were investigated. The results elucidate that grading affects the energy absorption capability and deformation behavior of these lattice types differently. These findings can provide engineers with valuable insight into the properties of FGLs, aiding targeted rather than expertise-driven utilization of lattices in design for AM.

/pdf/mechanical-performance-of-additively-manufactured-fiber-54pquy34oj.pdf

Mechanical Performance of Additively Manufactured Fiber-Reinforced Functionally Graded Lattices


Purpose
Fibre-reinforced additive manufacturing (FRAM) with short and continuous fibres yields light and stiff parts and thus increasing industry acceptance. High material anisotropy and specific manufacturing constraints shift the focus towards design for AM (DfAM), particularly on toolpath strategies. Assessing the design-property-processing relations of infill patterns is fundamental to establishing design guidelines for FRAM.


Design/methodology/approach
Subject to the DfAM factors performance, economy and manufacturability, the efficacy of two conventional infill patterns (grid and concentric) was compared with two custom strategies derived from the medial axis transformation (MAT) and guided by the principal stresses (MPS). The recorded stiffness and strength, the required CPU and print time, and the degree of path undulation and effective fibre utilisation (minimum printable fibre length) associated with each pattern, served as assessment indices for different case studies. Moreover, the influence of material anisotropy was examined, and a stiffness-alignment index was introduced to predict a pattern’s performance.


Findings
The highest stiffnesses and strengths were recorded for the MPS infill, emphasising the need for tailoring print paths rather than using fixed patterns. In contrast to the grid infill, the concentric infill offered short print times and reasonable utilisation of continuous fibres. The MAT-based infill yielded an excellent compromise between the three DfAM factors and experimentally resulted in the best performance.


Originality/value
This constitutes the first comprehensive investigation into infill patterns under DfAM consideration for FRAM, facilitating design and processing choices.


http://spiral.imperial.ac.uk/bitstream/10044/1/94244/2/Plocher%20et%20al%282022%29_AcceptedManuscript_RPJ.pdf

János Plocher

Papers

Review on design and structural optimisation in additive manufacturing: Towards next-generation lightweight structures

Effect of density and unit cell size grading on the stiffness and energy absorption of short fibre-reinforced functionally graded lattice structures

Learning from nature: Bio-inspiration for damage-tolerant high-performance fibre-reinforced composites

Mechanical Performance of Additively Manufactured Fiber-Reinforced Functionally Graded Lattices

Additive manufacturing with fibre-reinforcement – design guidelines and investigation into the influence of infill patterns