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Showing papers by "Nianbai Fang published in 2007"


Journal ArticleDOI
TL;DR: In this article, the authors used electrospray ionization mass spectrometry (ESI−MS) with both positive and negative ion modes to identify vitamin E and γ-oryzanol components in rice bran and germ.
Abstract: Rice bran is a rich natural source of vitamin E and γ-oryzanol, which have been extensively studied and reported to possess important health-promoting properties. However, commercial rice bran is a mixture of rice bran and germ, and profiles of vitamin E and γ-oryzanol components in these two different materials are less well-studied. In the current study, vitamin E and γ-oryzanol components in rice bran and germ were analyzed by liquid chromatography/mass spectrometry/mass spectrometry. The components were identified by electrospray ionization mass spectrometry (ESI−MS) with both positive- and negative-ion modes. Both deprotonated molecular ion [M − H]- and protonated molecular ion [M + H]+ found as the base peaks in spectra of vitamin E components made ESI−MS a valuable analytic method in detecting vitamin E compounds, especially when they were at very low levels in samples. Ultraviolet absorption was used for quantification of vitamin E and γ-oryzanol components. While the level of vitamin E in rice ge...

89 citations