R. Calabrò

Bio: R. Calabrò is an academic researcher from Polytechnic University of Milan. The author has contributed to research in topics: Natural rubber & Biaxial tensile test. The author has an hindex of 3, co-authored 5 publications receiving 23 citations.

Effect of Molecular Orientation on the Fracture Behavior of Carbon Black-Filled Natural Rubber Compounds

Abstract: The fracture behavior of carbon black-filled natural rubber compounds, differing in filler content, was studied performing tensile tests in biaxial loading conditions, using a central notched cross-shaped specimen. The test consisted of two steps: a drawing step was initially performed loading the specimen in the direction parallel to the notch plane, up to different draw ratios, and then the specimen was loaded in the direction normal to the notch plane up to fracture. Using a fracture mechanics approach, the fracture toughness was evaluated as a function of the draw ratio applied in the drawing step. A correlation between the fracture phenomenology observed and molecular orientability and orientation was attempted.

J‐Integral from Full Field Kinematic Data for Natural Rubber Compounds

Abstract: The application of the digital image correlation technique to the determination of the J-integral at fracture initiation for carbon black-filled natural rubber compounds is discussed. Three different compounds with varying carbon black content were tested, using two different test configurations: pure shear and biaxial tensile test. Digital image correlation was used to measure the displacement field around the crack tip in the tested specimens. From the displacement field, which was interpolated using a finite element scheme, the stresses were evaluated by using Ogden's hyperelastic model, and the J-integral could be calculated. The results compare well with both theoretical and finite element results.

J-Integral Calculation by Finite Element Processing of Measured Full-Field Surface Displacements

Abstract: A novel method has been developed based on the conjoint use of digital image correlation to measure full field displacements and finite element simulations to extract the strain energy release rate of surface cracks. In this approach, a finite element model with imported full-field displacements measured by DIC is solved and the J-integral is calculated, without knowledge of the specimen geometry and applied loads. This can be done even in a specimen that develops crack tip plasticity, if the elastic and yield behaviour of the material are known. The application of the method is demonstrated in an analysis of a fatigue crack, introduced to an aluminium alloy compact tension specimen (Al 2024, T351 heat condition).

Sideways and stable crack propagation in a silicone elastomer

Abstract: We have discovered a peculiar form of fracture that occurs in a highly stretchable silicone elastomer (Smooth-On Ecoflex 00–30). Under certain conditions, cracks propagate in a direction perpendicular to the initial precut and in the direction of the applied load. In other words, the crack deviates from the standard trajectory and instead propagates perpendicular to that trajectory. The crack arrests stably, and thus the material ahead of the crack front continues to sustain load, thereby enabling enormous stretchabilities. We call this phenomenon “sideways” and stable cracking. To explain this behavior, we first perform finite-element simulations that demonstrate a propensity for sideways cracking, even in an isotropic material. The simulations also highlight the importance of crack-tip blunting on the formation of sideways cracks. Next, we provide a hypothesis on the origin of sideways cracking that relates to microstructural anisotropy (in a nominally isotropic elastomer). To substantiate this hypothesis, we transversely prestretch samples to various extents before fracture testing, as to determine the influence of microstructural arrangement (chain alignment and strain-induced crystallization) on fracture energy. We also perform microstructural characterization that indicates that significant chain alignment and strain-induced crystallization indeed occur in this material upon stretching. We conclude by characterizing how a number of loading conditions, such as sample geometry and strain rate, affect this phenomenon. Overall, this paper provides fundamental mechanical insight into basic phenomena associated with fracture of elastomers.

Strain-Induced Crystallization in Natural Rubber: Flory’s Theory Revisited

Abstract: In this paper, some aspects of the physical mechanisms involved in strain-induced crystallization (SIC) in cross-linked natural rubber networks are discussed. The theory of SIC as developed by Flor...

Fracture phenomenology and toughness of filled natural rubber compounds via the pure shear test specimen

Abstract: Material anisotropy induced by strain in filled vulcanized rubbers strongly affects fracture toughness. The influence of carbon black content on fracture phenomenology and fracture toughness was investigated by performing video-recorded tests adopting a suitable grooved notched pure shear test specimen. In such a way, it was possible to analyze the so-called “knotty tearing” deformation mechanism occurring at the crack tip: sideways cracks perpendicular to the notch plane develop before the onset and propagation of a forward crack parallel to the notch plane. The J-integral fracture mechanics approach was adopted and digital image correlation analysis was performed to measure the strain at the crack tip. The presence of carbon black modifies the maximum chain extensibility and strain-induced crystallizability of the rubber matrix in the compound. The formation of sideways cracks occurred in all filled compounds and resulted in a link to the maximum chain extensibility. Nevertheless, toughness enh...