Vadim V. Silberschmidt

Bio: Vadim V. Silberschmidt is an academic researcher from Loughborough University. The author has contributed to research in topics: Machining & Materials science. The author has an hindex of 44, co-authored 543 publications receiving 8619 citations. Previous affiliations of Vadim V. Silberschmidt include University of Rhode Island & Universities UK.

Microstructural and Mechanical Characterization of Thin-Walled Tube Manufactured with Selective Laser Melting for Stent Application

Abstract: This paper focuses on microstructural and mechanical characterization of metallic thin-walled tube produced with additive manufacturing (AM), as a promising alternative technique for the manufacturing of tubes as a feedstock for stents micromachining. Tubes, with a wall thickness of 500 μm, were made of 316L stainless steel using selective laser melting. Its surface roughness, constituting phases, underlying microstructures and chemical composition were analyzed. The dependence of hardness and elastic modulus on the crystallographic orientation were investigated using electron backscatter diffraction and nanoindentation. Spherical nanoindentation was performed to extract the indentation stress–strain curve from the load–displacement data. The obtained results were compared with those for a commercial 316L stainless steel stent. Both tube and commercial stent samples were fully austenitic, and the as-fabricated surface finish for the tube was much rougher than the stent. Microstructural characterization revealed that the tube had a columnar and coarse grain microstructure, compared to equiaxed grains in the commercial stent. Berkovich nanoindentation suggested an effect for the grain orientation on the hardness and Young’s modulus. The stress–strain curves and the indentation yield strength for the tube and stent were similar. The work is an important step toward AM of patient-specific stents.

Mechanical performance of 3D printed polylactide during degradation

Abstract: Although widely-used biodegradable polymers have been extensively studied for conventional manufacturing processes, this is the first study considering the effect of interfacial bonds between extruded filaments – the most important aspect related to additive manufacturing – on degradation at 37 °C. Its results improve the confidence in the material extrusion additive manufacturing process and negate one of the crucial unknown factors for bioresorbable products, by demonstrating that the interface degrades in a similar manner to the bulk polymer material. To do this, specially designed micro-tensile specimens were developed to analyse the degradation of 3D-printed parts for the first time at 37 °C and accelerated temperatures. The mechanical properties of the interface between extruded filaments (Z specimen) were compared against the control, i.e. along filaments (F specimen), under medically relevant testing conditions (submerged at 37 °C). Monitoring the degradation of tensile strength showed that both specimen types behaved similarly, exhibiting an initial delay followed by a reduction in properties. Comparison of thermal and chemical properties revealed that during the early stage of degradation, crystallinity was the dominating factor, whilst at later stages, mechanical properties were mainly defined by the molecular weight and autocatalytic degradation. The findings suggest that understanding developed in the long-standing field of polymer degradation can be applied to additive-manufactured medical devices, which unavoidably contain interlayer interfaces.

Incorporation and evolution of ZrO2 nano-particles in Pt-modified aluminide coating for high temperature applications

Abstract: ZrO2 nano-particles were incorporated into electro-deposited PtAl coatings in an attempt to enhance their performance by exploiting the effect of reactive element oxides. PtAl coatings with and without ZrO2 particles were deposited onto three commercially available Ni-based superalloys: Mar-M247, Mar-M246 and Inconel 718. After aluminising and annealing, thermal cycling oxidation tests were carried out to evaluate the influence of ZrO2 addition and substrate composition. Cross-sectional SEM images were obtained to characterise the coatings after deposition, after heat treatment and after 200 thermal cycles. The addition of ZrO2 particles to PtAl coatings on Mar-M-246 and Inconel 718 appeared to increase the growth of thermally grown oxide and reduce its rumpling. However, such effects were not observed for the addition of ZrO2 particles to the PtAl coatings on Mar-M247. The analysis of the coatings on different substrates revealed and elucidated the interactions between Hf, Al and ZrO2, providing better understanding of reactions of ZrO2 and the influence of the substrate on bond coat behaviour.

Fast parallel algorithms for short-range molecular dynamics

Abstract: Three parallel algorithms for classical molecular dynamics are presented. The first assigns each processor a fixed subset of atoms; the second assigns each a fixed subset of inter-atomic forces to compute; the third assigns each a fixed spatial region. The algorithms are suitable for molecular dynamics models which can be difficult to parallelize efficiently—those with short-range forces where the neighbors of each atom change rapidly. They can be implemented on any distributed-memory parallel machine which allows for message-passing of data between independently executing processors. The algorithms are tested on a standard Lennard-Jones benchmark problem for system sizes ranging from 500 to 100,000,000 atoms on several parallel supercomputers--the nCUBE 2, Intel iPSC/860 and Paragon, and Cray T3D. Comparing the results to the fastest reported vectorized Cray Y-MP and C90 algorithm shows that the current generation of parallel machines is competitive with conventional vector supercomputers even for small problems. For large problems, the spatial algorithm achieves parallel efficiencies of 90% and a 1840-node Intel Paragon performs up to 165 faster than a single Cray C9O processor. Trade-offs between the three algorithms and guidelines for adapting them to more complex molecular dynamics simulations are also discussed.

The Design and Analysis of Experiments

Abstract: THE DESIGN AND ANALYSIS OF EXPERIMENTS. By Oscar Kempthorne. New York, John Wiley and Sons, Inc., 1952. 631 pp. $8.50. This book by a teacher of statistics (as well as a consultant for \"experimenters\") is a comprehensive study of the philosophical background for the statistical design of experiment. It is necessary to have some facility with algebraic notation and manipulation to be able to use the volume intelligently. The problems are presented from the theoretical point of view, without such practical examples as would be helpful for those not acquainted with mathematics. The mathematical justification for the techniques is given. As a somewhat advanced treatment of the design and analysis of experiments, this volume will be interesting and helpful for many who approach statistics theoretically as well as practically. With emphasis on the \"why,\" and with description given broadly, the author relates the subject matter to the general theory of statistics and to the general problem of experimental inference. MARGARET J. ROBERTSON

American Society for Testing and Materials

Abstract: The American Society for Testing and Materials (ASTM) is an independent organization devoted to the development of standards.

Effect of Temperature

Abstract: A positive temperature coefficient is the term which has been used to indicate that an increase in solubility occurs as the temperature is raised, whereas a negative coefficient indicates a decrease in solubility with rise in temperature.