The microstructure of Additive Manufactured (AM) Inconel 718 in general and Selective Laser Melting (SLM), in particular is different from the material produced by conventional methods due to the rapid solidification process associated with the former. As a result, the widely adapted standard solution heat treatment temperature (

Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment

Inconel 718 is one of the most commonly employed alloys for metal additive manufacturing (MAM) and has a wide range of applications in aircraft, gas turbines, turbocharger rotors, and a variety of other corrosive and structural applications involving temperatures of up to ∼700 °C. Numerous studies have investigated different aspects of the mechanical behaviour of additively manufactured (AM) Inconel 718. This study analyses the observations from more than 170 publications to provide an unbiased engineering overview for the mechanical response of AM Inconel 718 (and its variations and spread among different reports). First, a brief review of the microstructural features of AM Inconel 718 is presented. This is followed by a comprehensive summary of tensile strength, hardness, fatigue strength, and high-temperature creep behaviour of AM Inconel 718 for different types of MAM techniques and for different process and post-process conditions.

A review of mechanical properties of additively manufactured Inconel 718

The influence of Laves phases on the room temperature tensile properties of Inconel 718 fabricated by powder feeding laser additive manufacturing

Residual stress profiles were mapped using neutron diffraction in two simple prism builds of Inconel 718: one fabricated with electron beam melting (EBM) and the other with direct laser metal sintering. Spatially indexed stress-free cubes were obtained by electrical discharge machining (EDM) equivalent prisms of similar shape. The (311) interplanar spacings from the EDM sectioned sample were compared to the interplanar spacings calculated to fulfill stress and moment balance. We have shown that applying stress and moment balance is a necessary supplement to the measurements for the stress-free cubes with respect to accurate stress calculations in additively manufactured components. In addition, our work has shown that residual stresses in electron beam melted parts are much smaller than that of direct laser metal sintered parts most likely due to the powder preheating step in the EBM process.

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Comparison of residual stresses in Inconel 718 simple parts made by electron beam melting and direct laser metal sintering

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[신간서적 안내] 재료과학과 공학 (Fundamentals of Materials Science and Engineering)

An IN718 alloy coating was prepared by high-power diode laser cladding. 980STA standard heat treatment and direct aging (DA) were employed to improve the properties of this coating. The niobium segregation in the as-deposited coating and the heat-treated coating had been investigated using a scanning electron microscope (SEM) equipped with energy-dispersive X-ray spectroscopy (EDAX). The results showed that 980STA standard heat treatment improved the microhardness of the coating significantly, and Laves concentration was reduced from 30.6 vol pct to about 11.4 vol pct after 980STA. The niobium concentration in Laves of the 980STA-treated coating was higher than that of DA-treated coating and as-deposited coating. Only a small portion of niobium in the coating was precipitated in the form of γ″ during the 980STA heat treatment. The rest of niobium was the alloying element for solid-solution strengthening and the constituent element of Laves. The niobium segregation facilitated the formation of Laves.

Effect of Heat Treatment on Niobium Segregation of Laser-Cladded IN718 Alloy Coating

IN718 alloy clad coating cooled in liquid nitrogen was fabricated by high power diode laser. The microstructure of the coating was investigated using SEM equipped with energy disperse spectroscopy, and the precipitation phase was analysed using TEM after standard heat treatment. The results showed that the liquid nitrogen provided the clad coating an ultrarapid cooling rate during laser cladding. Laves in the ultrarapid cooled clad coating was refined, and Laves concentration and dendritic space were decreased compared with the air cooled clad coating. The ultrarapid cooling rate reduced the constitutional supercooling and restrained Nb segregation in the Laves during solidification. More Nb was distributed in austenite and precipitated as γ″-Ni3Nb during the standard heat treatment to improve the mechanical properties of the clad coating.

Effect of ultrarapid cooling on microstructure of laser cladding IN718 coating

The rapid cooling rate was achieved during laser remelting with high scanning speed. The microstructure and precipitations in the INCONEL 718 remelted layer were investigated by scanning electron microscope (SEM), transmission electron microscope (TEM), and solid phase microextraction (SPME). The phase transition temperatures were carried out by differential thermal analysis (DTA). The results showed that columnar-dendritic and equiaxial structures appeared in different regions of the remelted layer. The dendritic spacing of the columnar dendrite and equiaxed grain size decreased with increasing scanning speed. The precipitations in the remelted layer consisted of Laves, granular phase, and a small quantity of quadrangular nitride (Ti, Nb)N. The granular phase Nb(Al, Ti) was precipitated at about 1272 K (999 °C) with the spontaneous decomposition of the supersaturation Laves during the cooling stage, and the small-size granule became coarsened to 0.2 to 0.9 μm during the cooling stage. The noncoherent relationship existed between the granular phase and austenite, and the coarsening of granule was related to the cube root of the diffusion coefficient, interfacial energy, and diffusion time. The microhardness of the remelted layer was increased by increasing the cooling rate due to the Nb atomic solid solution strengthening caused by the distorted elastic stress field and the short-range internal stress.

Yaocheng Zhang

Papers

Effect of Heat Treatment on Niobium Segregation of Laser-Cladded IN718 Alloy Coating

Effect of ultrarapid cooling on microstructure of laser cladding IN718 coating

Effect of Cooling Rate on the Microstructure of Laser-Remelted INCONEL 718 Coating

Microstructure, interfacial IMC and mechanical properties of Sn–0.7Cu–xAl (x = 0–0.075) lead-free solder alloy

Microstructure, IMCs layer and reliability of Sn-58Bi solder joint reinforced by Mo nanoparticles during thermal cycling