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Institution

Federal University of São Carlos

EducationSão Carlos, Brazil
About: Federal University of São Carlos is a education organization based out in São Carlos, Brazil. It is known for research contribution in the topics: Population & Microstructure. The organization has 16471 authors who have published 34057 publications receiving 456654 citations. The organization is also known as: UFSCar & Federal University of São Carlos.


Papers
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Journal ArticleDOI
TL;DR: In this article, the surface morphology and crystal structure of polycrystalline thin films were investigated using scanning electron microscopy (SEM), AFM, X-ray diffraction, and specular reflectance infrared Fourier transform spectroscopy, respectively.
Abstract: Polycrystalline BaWO4 and PbWO4 thin films having a tetragonal scheelite structure were prepared at different temperatures. Soluble precursors such as barium carbonate, lead acetate trihydrate and tungstic acid, as starting materials, were mixed in aqueous solution. The thin films were deposited on silicon, platinum-coated silicon and quartz substrates by means of the spinning technique. The surface morphology and crystal structure of the thin films were investigated using scanning electron microscopy (SEM), atomic force microscopy (AFM), X-ray diffraction, and specular reflectance infrared Fourier transform spectroscopy, respectively. Nucleation stages and surface morphology evolution of thin films on silicon substrates have been studied by atomic force microscopy. XRD characterization of these films showed that BaWO4 and PbWO4 phase crystallize at 500 � C from an inorganic amorphous phase. FTIR spectra revealed the complete decomposition of the organic ligands at 500 � C and the appearance of two sharp and intense bands between 1000 and 600 cm � 1 assigned to vibrations of the antisymmetric stretches resulting from the high crystallinity of both thin films. The optical properties were also studied. It was found that BaWO4 and PbWO4 thin films have Eg=5.78 eV and 4.20 eV, respectively, of a direct transition nature. The excellent microstructural quality and chemical homogeneity results confirmed that soft solution processing provides an inexpensive and environmentally friendly route for the preparation of BaWO4 and PbWO4 thin films. # 2003 Elsevier Ltd. All rights reserved.

88 citations

Journal ArticleDOI
TL;DR: Exercise therapy should be the first-line treatment to improve pain, function and range of motion in individuals with subacromial pain syndrome.
Abstract: Aim To summarise the current evidence regarding the effectiveness of physical therapy on pain, function and range of motion in individuals with subacromial pain syndrome (SAPS). Design Systematic review. Data sources PubMed, Web of Science, CINAHL, Cochrane, Embase, Lilacs, Ibecs and Scielo databases. Eligibility criteria for selecting studies Randomised controlled trials (RCTs) investigating physical therapy modalities for SAPS on pain, function/disability or range of motion were included. Results 64 high-quality RCTs were included. Exercise therapy provided high evidence of being as effective as surgery intervention and better than no treatment or placebo treatment to improve pain, function and range of motion in the short, mid and long terms. The combination of mobilisation and exercises provided high evidence to decrease pain and improve function in the short term. There is limited evidence for improvements on the outcomes with the isolated application of manual therapy. High level of evidence was synthesised regarding the lack of beneficial effects of physical resources such as low-level laser, ultrasound and pulsed electromagnetic field (PEMF) on pain, function or range of motion in the treatment of SAPS. There is limited evidence for microwave diathermy and transcutaneous electrical nerve stimulation. There is moderate evidence to no benefits with taping in the short term. Effects of diacutaneous fibrolysis and acupuncture are not well established yet. Conclusions Exercise therapy should be the first-line treatment to improve pain, function and range of motion. The addition of mobilisations to exercises may accelerate reduction of pain in the short term. Low-level laser therapy, PEMF and taping should not be recommended.

88 citations

Journal ArticleDOI
TL;DR: This review covers the most recent developments of deaminative strategies by using Katritzky Salts as alkyl radical reservoirs, with particular concern on photoinduced processes applied to organic synthesis.

88 citations

Journal ArticleDOI
TL;DR: To study the degree of interpopulational differentiation and racial admixture in Africanized honeybees, worker bees from three regions of Brazil and from Uruguay are collected and their genotypes for 10 enzyme loci are determined.
Abstract: To study the degree of interpopulational differentiation and racial admixture in Africanized honeybees, we collected worker bees from three regions of Brazil (the northeast, the state of Sao Paulo, and Porto Alegre) and from Uruguay and determined their genotypes for 10 enzyme loci. We also performed a morphometric analysis on forewing measurements of worker bees from the northeast and Porto Alegre regions of Brazil and from Paysandu, Uruguay. Comparative analysis of interpopulational heterogeneity snowed that there are significant differences, especially at the Mdh locus, among the populations from different regions. An increase in the frequency of the MdhB allele was observed from north to south, with predominance in the Uruguayan populations. A small component of interpopulational variability was detected in the populations studied. Racial admixture was calculated from information obtained for Mdh in Africa and Europe. The percentages of racial admixture differed slightly but significantly among Brazilian regions. The morphometric study based on canonical variables exhibited a similar pattern. The greater proportions of Apis mellifera adansonii alleles in the admixture may be explained by selection during the initial stage of migration of Africanized bees and by preferential mating between individuals of the same race. Differences in the proportions of A. m. adansonii alleles between regions indicate incipient populational differentiation of Africanized bees. We suggest that greater gene flow from the European races in the south of Brazil could be one of the causes of this phenomenon.

88 citations

Journal ArticleDOI
TL;DR: In this paper, a phase transformation technique was applied to produce porous ceramics by decomposing an aluminum-magnesium hydro-carbonate known as hydrotalcite (Mg 6 Al 2 (CO 3 )(OH) 16 ·4H 2 O).

88 citations


Authors

Showing all 16693 results

NameH-indexPapersCitations
Akihisa Inoue126265293980
Michael R. Hamblin11789959533
Daniel P. Costa8953126309
Elson Longo86145440494
Ross Arena8167139949
Tom M. Mitchell7631541956
José Arana Varela7674823005
Luiz H. C. Mattoso6645517432
Steve F. Perry6629413842
Edson R. Leite6353515303
Juan Andrés6049313499
Edward R. T. Tiekink60196721052
Alex A. Freitas6034514789
Mary F. Mahon5953914258
Osvaldo N. Oliveira5961416369
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Performance
Metrics
No. of papers from the Institution in previous years
YearPapers
202365
2022371
20212,710
20202,728
20192,435
20182,346