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Showing papers in "Experimental Mechanics in 2013"


Journal ArticleDOI
TL;DR: In this article, a Gauss-Newton-based digital image correlation (DIC) method was proposed to eliminate the redundant computations involved in conventional DIC method using forward additive matching strategy and classic Newton-Raphson (FA-NR) algorithm without sacrificing its sub-pixel registration accuracy.
Abstract: High-efficiency and high-accuracy deformation analysis using digital image correlation (DIC) has become increasingly important in recent years, considering the ongoing trend of using higher resolution digital cameras and common requirement of processing a large sequence of images recorded in a dynamic testing. In this work, to eliminate the redundant computations involved in conventional DIC method using forward additive matching strategy and classic Newton–Raphson (FA-NR) algorithm without sacrificing its sub-pixel registration accuracy, we proposed an equivalent but more efficient DIC method by combining inverse compositional matching strategy and Gauss-Newton (IC-GN) algorithm for fast, robust and accurate full-field displacement measurement. To this purpose, first, an efficient IC-GN algorithm, without the need of re-evaluating and inverting Hessian matrix in each iteration, is introduced to optimize the robust zero-mean normalized sum of squared difference (ZNSSD) criterion to determine the desired deformation parameters of each interrogated subset. Then, an improved reliability-guided displacement tracking strategy is employed to achieve further speed advantage by automatically providing accurate and complete initial guess of deformation for the IC-GN algorithm implemented on each calculation point. Finally, an easy-to-implement interpolation coefficient look-up table approach is employed to avoid the repeated calculation of bicubic interpolation at sub-pixel locations. With the above improvements, redundant calculations involved in various procedures (i.e. initial guess of deformation, sub-pixel displacement registration and sub-pixel intensity interpolation) of conventional DIC method are entirely eliminated. The registration accuracy and computational efficiency of the proposed DIC method are carefully tested using numerical experiments and real experimental images. Experimental results verify that the proposed DIC method using IC-GN algorithm and the existing DIC method using classic FA-NR algorithm generate similar results, but the former is about three to five times faster. The proposed reliability-guided IC-GN algorithm is expected to be a new standard full-field displacement tracking algorithm in DIC.

391 citations


Journal ArticleDOI
TL;DR: It is shown that time varying drift distortion is a larger problem at high magnification while spatial distortion is more problematic at low magnification and the new use of sample-independent calibration and a method to eliminate the detrimental effects of stress relaxation in the displacement fields prior to distortion correction are introduced.
Abstract: The recent combination of scanning electron microscopy and digital image correlation (SEM-DIC) enables the experimental investigation of full-field deformations at much smaller length scales than is possible using optical digital image correlation methods. However, the high spatial resolution of SEM-DIC comes at the cost of complex image distortions, long image scan times that can capture gradients from stress relaxation, and a high noise sensitivity to SEM parameters. In this paper, it is shown that these sources of error can significantly impact the quality of the results and must be accounted for in order to perform accurate SEM-DIC experiments. An existing framework for distortion corrections is adapted to improve accuracy and the procedures are described in detail. As the results demonstrate, time varying drift distortion is a larger problem at high magnification while spatial distortion is more problematic at low magnification. Additionally, the new use of sample-independent calibration and a method to eliminate the detrimental effects of stress relaxation in the displacement fields prior to distortion correction are introduced. The impact of SEM settings on image noise is quantified and noise minimization schemes are examined. Finally, a uniaxial tension test on coarse-grained 1100-O aluminum is used to demonstrate these techniques, where active slip planes are identified and strain localization is examined in relation to the underlying microstructure.

234 citations


Journal ArticleDOI
TL;DR: In this article, an artificial speckle pattern was generated by the remodelling of a deposited gold layer, which accelerated the remodeling process and promoted the formation of finer nano-scale speckles with sizes ranging 30 nm to 150 nm and of similar spacing.
Abstract: Digital image correlation (DIC) of images obtained using scanning electron microscopy has been used to study, quantitatively, the plastic deformation of stainless steel at the microstructural scale. An artificial speckle pattern was generated by the remodelling of a deposited gold layer. A new experimental setup was shown to accelerate the remodelling process and promote the formation of finer nano-scale speckles with sizes ranging 30 nm to 150 nm and of similar spacing. The effects of surface preparation on speckle morphology are discussed. The high density of speckles enabled displacement mapping with resolution of one displacement vector each 0.2 × 0.2 μm2 of surface area. It is shown that sub-micron resolution is necessary to capture the plastic deformation associated with the formation of slip bands in stainless steel, which are an important component of the deformation of these materials at the microscale. Electron backscatter diffraction (EBSD) was used to reconstruct the surface grain boundaries and enabled these deformation features to be linked to the microstructure.

196 citations


Journal ArticleDOI
TL;DR: In this article, a self-assembled gold nanoparticle surface patterning technique is presented that enables nanometer spatial resolution for digital image correlation (DIC) experiments in a scanning electron microscope.
Abstract: A self-assembled gold nanoparticle surface patterning technique is presented that enables nanometer spatial resolution for digital image correlation (DIC) experiments in a scanning electron microscope. This technique, originally developed for surface-enhanced Raman scattering substrates, results in the assembly of individual 15–136 nm diameter gold nanoparticles over the surface of the test sample. The resulting dense, randomly isotropic, and high contrast pattern enables DIC down to an unprecedented image resolution of approximately 4 nm/pixel. The technique is inexpensive, fast, results in even coverage over the entire surface of the test sample, and can be applied to metallic and non-metallic substrates as well as curved or delicate specimens. In addition, the pattern is appropriate for multi-scale experimental investigations through the utilization of nanoparticle aggregates that collect on the surface in combination with the pattern formed by individual nanoparticles.

138 citations


Journal ArticleDOI
TL;DR: In this paper, a high-accuracy 2D-DIC system using a bilateral telecentric lens is established, which is not only insensitive to out-of-plane motion of the test object and the self-heating of a camera, but also demonstrates negligible lens distortion.
Abstract: By comparing two digital images of a test planar specimen surface recorded in different configurations, two-dimensional digital image correlation (2D-DIC) provides full-field displacements to sub-pixel accuracy and full-field strains in the recorded images. For the 2D-DIC systems using an optical lens, a simple pinhole imaging model is commonly used to describe the linear relationship between the measured sensor plane displacements and the actual displacements in the object surface. However, in a practical measurement, various unavoidable disadvantageous factors, such as small out-of-plane motion of the test object surface occurred after loading, small out-of-plane motion of the sensor target due to the self-heating or temperature variation of a camera, and geometric distortion of the imaging lens, may seriously impair or slightly change the originally assumed linear correspondence. In certain cases, these disadvantages may lead to significant errors in displacements and strains measured by 2D-DIC. In this work, the measurement errors of 2D-DIC due to the above three disadvantageous factors are first described in detail. Then, to minimize the errors associated with these disadvantages, a high-accuracy 2D-DIC system using a bilateral telecentric lens is established. The performance of the established 2D-DIC system and other two 2D-DIC systems using a conventional lens and an object-side telecentric lens are investigated experimentally using easy-to-implement stationary, out-of-plane and in-plane rigid body translation tests. A detailed examination reveals that a high-quality bilateral telecentric lens is not only insensitive to out-of-plane motion of the test object and the self-heating of a camera, but also demonstrates negligible lens distortion. Uniaxial tensile tests of an aluminum specimen were also performed to quantitatively compare the axial and transversal strains measured by the proposed 2D-DIC system and those measured by strain gage rosettes. The perfect agreement between the two measurements further verifies the accuracy of the established 2D-DIC system.

129 citations


Journal ArticleDOI
TL;DR: In this paper, rubberized concrete samples were prepared by partial substitution of sand by waste crumb rubber, and tested under impact three-point bending load, as well as static load.
Abstract: In this study, rubberized concrete samples were prepared by partial substitution (5 %, 10 % and 20 % replacements by volume) of sand by waste crumb rubber, and tested under impact three-point bending load, as well as static load. Three types of specimens (size 50 × 100 × 500 mm) namely, plain concrete, rubberized concrete, and double layer concrete (with rubberized concrete top and plain concrete bottom) were loaded to failure in a drop-weight impact machine by subjecting to 20 N weight from a height of 300 mm, and another three similar specimens were used for the static load test. In both the tests, the load–displacement and fracture energy of each specimen were investigated. Finite-element simulations were also performed to study the dynamic behaviors of the samples, by using LUSAS V.14 software. It was noticed that, the impact tup, and inertial and bending loads increased with the increase in the percentage of sand replacement by crumb rubber. It was interesting to observe that these effects were more significant in the double layer specimen compared to the plain and rubberized concrete samples. The static peak bending load always decreased with increase of rubber in the mix. In general, the strength and energy absorbing capability of rubberized concrete was better under impact loading than under static loading. The simulated load against displacement behaviors of all the samples were validated by the experimental results.

89 citations


Journal ArticleDOI
TL;DR: In this paper, a new approach based on the fractal analysis of residual crack patterns is proposed to assess the structural integrity of reinforced concrete elements and a new damage index is presented to quantitatively perform a damage classification.
Abstract: Currently, assessing the performance and safety of reinforced concrete structures relies on routine-based visual inspection (VI). Cracks width measurements are commonly used as a convenient indicator of damage; however other factors, such as distribution and pattern of the cracks should be considered equally important in measuring the extent of damage present in the structure. As a result, condition assessed by VI is subjective in nature and depends on the experience, knowledge, expertise, and judgment of the inspector carrying out the assessment. A new approach based on the fractal analysis of residual crack patterns is proposed in this paper to assess the structural integrity of reinforced concrete elements. A new damage index is presented to quantitatively perform a damage classification. The methodology is validated through experimental studies on two large-scale reinforced concrete shear walls subjected to a displacement controlled reversed cyclic loading. Damage grades are also identified based on width of cracks and proposed damage index (DI). The results demonstrate a more accurate estimation of damage grades using DI. Furthermore, it is demonstrated that the DI can estimate the relative stiffness loss of the specimens with acceptable accuracy.

83 citations


Journal ArticleDOI
TL;DR: In this article, a feasibility study of measuring 3D displacement fields in the bulk during ductile crack initiation via combined Synchrotron Radiation Computed Laminography (SRCL) and Digital Volume Correlation (DVC) is performed.
Abstract: A feasibility study of measuring 3D displacement fields in the bulk during ductile crack initiation via combined Synchrotron Radiation Computed Laminography (SRCL) and Digital Volume Correlation (DVC) is performed. In contrast to tomography, SRCL is a technique that is particularly adapted to obtain three-dimensional (3D) reconstructed volumes of objects that are laterally extended (i.e., in 2 directions) and thin in the third direction, i.e. sheet-like objects. In-situ laminography data of an initiating crack ahead of a machined notch are used with a voxel size of 0.7 μm. The natural contrast of the observed 2XXX Al-alloy caused by intermetallic particles and initial porosity is used to measure displacement fields via a global DVC technique assuming a continuous displacement field. An initial performance study is carried out on data of the same undeformed material but after a substantial shift of the laminography rotation axis with respect to the imaged specimen. Volume correlations between different loading steps provide displacement fields that are qualitatively consistent with the remote loading conditions. Computed strain fields display a strain concentration close to the notch tip.

81 citations


Journal ArticleDOI
TL;DR: In this article, the dynamic response of a two-dimensional square packing of uncompressed stainless steel spheres excited by impulsive loadings was studied and the observed solitary waves were determined to have similar (Hertzian) properties to the extensively studied solitary waves supported by an uncompressed, uniform, one-dimensional chain of spheres.
Abstract: We studied the dynamic response of a two-dimensional square packing of uncompressed stainless steel spheres excited by impulsive loadings. We developed a new experimental measurement technique, employing miniature tri-axial accelerometers, to determine the stress wave properties in the array resulting from both an in-plane and out-of-plane impact. Results from our numerical simulations, based on a discrete particle model, were in good agreement with the experimental results. We observed that the impulsive excitations were resolved into solitary waves traveling only through initially excited chains. The observed solitary waves were determined to have similar (Hertzian) properties to the extensively studied solitary waves supported by an uncompressed, uniform, one-dimensional chain of spheres. The highly directional response of this system could be used as a basis to design granular crystals with predetermined wave propagation paths capable of mitigating stress wave energy.

77 citations


Journal ArticleDOI
TL;DR: In this paper, a specific in situ loading device is presented for three-point bending tests, which enables the visualization of transverse shear effects in composite structures, where composite fibres and epoxy resin are associated with metallic particles to create contrast during X-ray acquisition.
Abstract: The complex mechanical behaviour of composite materials, due to internal heterogeneity and multi-layered composition impose deeper studies. This paper presents an experimental investigation technique to perform volume kinematic measurements in composite materials. The association of X-ray micro-computed tomography acquisitions and Digital Volume Correlation (DVC) technique allows the measurement of displacements and deformations in the whole volume of composite specimen. To elaborate the latter, composite fibres and epoxy resin are associated with metallic particles to create contrast during X-ray acquisition. A specific in situ loading device is presented for three-point bending tests, which enables the visualization of transverse shear effects in composite structures.

76 citations


Journal ArticleDOI
TL;DR: In this article, the width of a localized zone on the surface of notched concrete beams under quasi-static three-point bending was measured using the 2D Digital Image Correlation technique.
Abstract: The measurements of the width of a localized zone on the surface of notched concrete beams under quasi-static three-point bending were performed using the 2D Digital Image Correlation technique. Different image length resolutions, image search patches and distances between search patch centres were tested. Attention was paid to the accuracy and objectivity of surface displacements measured. An original method was proposed to determine the width of localized zones above the notch based on experiments.

Journal ArticleDOI
TL;DR: A Monte Carlo approach is presented as a method to discover the magnitude of the stereo-DIC calibration uncertainty and the error propagation results are interpreted to provide some best-practices guidelines for DIC.
Abstract: Stereo digital image correlation (DIC) is now a standard measurement technique. It is, therefore, important to quantify the measurement uncertainties when using it for experiments. Because of the complexity of the DIC measurement process, a Monte Carlo approach is presented as a method to discover the magnitude of the stereo-DIC calibration uncertainty. Then, the calibration errors, along with an assumed sensor position error, are propagated through the stereo-triangulation process to find the uncertainty in three-dimensional position and object motion. Details on the statistical results of the calibration parameters are presented, with estimated errors for different calibration targets and calibration image quality. A sensitivity study was done to look at the influence of the different calibration error sources. Details on the best approach for propagating the errors from a statistical perspective are discussed, including the importance of using a “boot-strap” approach for error propagation because of the covariance of many of the calibration parameters. The calibration and error propagation results are then interpreted to provide some best-practices guidelines for DIC.

Journal ArticleDOI
TL;DR: In this paper, a modified Arcan fixture is used to induce various loading conditions ranging from pure shear or axial loading in tension or compression to bidirectional loading, and a numerical optimization study was performed with different loading angles of the Arcan test fixture and off-axis angles of principal material axes.
Abstract: This paper presents an effective methodology to characterize all the constitutive (elastic) parameters of an orthotropic polymeric foam material (Divinycell H100) in one single test using Digital Image Correlation (DIC) in combination with the Virtual Fields Method (VFM). A modified Arcan fixture is used to induce various loading conditions ranging from pure shear or axial loading in tension or compression to bidirectional loading. A numerical optimization study was performed with different loading angles of the Arcan test fixture and off-axis angles of the principal material axes. The objective is to identify the configuration that gives the minimum sensitivity to noise and missing data on the specimen edges, which are the two major issues when identifying the stiffness components from actual DIC measurements. Two optimized Arcan test configurations were chosen. The experimental results obtained for these two optimized test configurations show a significant improvement of the measurement accuracy compared with a pure shear load configuration. The larger sensitivity of the pure shear test to missing data as opposed to the tensile test is also evident from the experimental data and confirms the analysis from the optimization study. The recovery of missing data along the specimen edges is a promising way to further improve the identification results.

Journal ArticleDOI
TL;DR: In this article, the multiple cut contour method is applied to map longitudinal and transverse components of residual stress in two nominally identical 50 mm thick electron beam welded Ti-6Al-4V alloy plates, one in the as-welded condition and a second welded plate in a post weld heat treated (PWHT) condition.
Abstract: The multiple cut contour method is applied to map longitudinal and transverse components of residual stress in two nominally identical 50 mm thick electron beam welded Ti-6Al-4V alloy plates, one in the as-welded condition and a second welded plate in a post weld heat treated (PWHT) condition. The accuracy and resolution of the contour method results are directly linked to the quality of the electro-discharge machining cut made. Two symmetric surface contour artefacts associated with cutting titanium, surface bowing and a flared edge, are identified and their influence on residual stresses calculated by the contour method is quantified. The former artefact is controlled by undertaking a series of cutting trials with reduced power settings to find optimal cutting conditions. The latter is mitigated by attaching 5 mm thick sacrificial plates to the wire exit side of the test specimen. The low level of noise in the measured stress profiles for both the as-welded and PWHT plates demonstrates the importance of controlling the quality of a contour cut and the added value of undertaking cutting trials.

Journal ArticleDOI
TL;DR: In this article, the distribution of axial and radial residual stresses in a martensitic-ferritic steel pipe with a multi-pass girth weld was measured using a hybrid contour measurement approach.
Abstract: The contour method is applied in an innovative manner to measure the distribution of hoop residual stress in a large martensitic-ferritic steel pipe containing a multi-pass girth weld. First, a novel one-step wire electro-discharge machining cut is conducted to divide the pipe lengthways into two halves. The deformation of the cut halves is then measured and analysed in a way that simultaneously gives maps of hoop stress across the wall thickness on both sides of the pipe and automatically accounts for through-thickness hoop bending effects and how they may vary along the pipe. Finally the contour method results are combined with X-ray diffraction residual stress measurements using the principle of superposition to determine the distribution of the axial and radial residual stresses in the pipe. It is thereby demonstrated how the distribution of three direct components of the residual stress tensor in a welded pipe can be readily determined using a “hybrid” contour measurement approach.

Journal ArticleDOI
TL;DR: In this article, a series of experimental investigations have been carried out on various non-crystalline ceramics (glass), single crystal (sapphire) and polycrystaline ceramic (AlON) materials for the Edge-on Impact (EOI) test.
Abstract: Structural transparent material systems are critical for many military and civilian applications. Transparent armor systems can consist of a wide variety of glass laminate assemblies with polymeric bonding interfaces and backing as well as the inclusion of polycrystalline ceramic (AlON, spinel) and single crystals (sapphire) as front facing materials. Over the last 20 years as the threats have escalated and become more varied, the challenges for rapidly developing optimized threat specific transparent armor packages have become extremely complex. Ultimate failure of structural ceramics in impact events is a function of the temporal and spatial interaction of the macro-stresses at the macro-, micro- and nano-structural scale, including elastic and inelastic (plastic) deformation, crack nucleation, damage evolution and resulting failure from the macro-scale (top down) and/or from the nano-scale (bottom up). In order to accelerate the development of validated design and predictive performance models, a systematic series of experimental investigations have been carried out on various non-crystalline ceramics (glass), single crystal (sapphire) and polycrystalline ceramics (AlON). The Edge-on Impact (EOI) test coupled with a high-speed Cranz-Schardin film camera has been extensively used on a variety of monolithic and laminated glasses, AlON and crystallographically controlled sapphire single crystals to visualize and quantify stress wave, crack and damage propagation. A modified Kolsky bar technique instrumented with a high speed digital camera has been utilized in an unconfined and confined test sample mode to examine the dynamic deformation and failure of AlON undergoing uniaxial, high strain rate compression. Real time photography has clearly demonstrated the critical influence of defects and post mortem characterization of fragments resulting from these tests have revealed the influence of micro-deformational twining and cleavage down to the nano-scale. Finally, a brief summary of work using ultra-high-speed photography of the impact of conventional projectiles on glass and AlON will be presented. These experimental results will be absolutely critical to help evolve and validate existing models used in computer codes to simulate the impact performance of brittle materials.

Journal ArticleDOI
TL;DR: In this paper, a full-field, multi-axial computation technique for determining residual stresses using the hole-drilling method with DIC is described, which takes advantage of the large quantity of data available from full field images to ameliorate the effect of modest deformation sensitivity of DIC measurements.
Abstract: A full-field, multi-axial computation technique is described for determining residual stresses using the hole-drilling method with DIC. The computational method takes advantage of the large quantity of data available from full-field images to ameliorate the effect of modest deformation sensitivity of DIC measurements. It also provides uniform residual stress sensitivity in all in-plane directions and accounts for artifacts that commonly occur within experimental measurements. These artifacts include image shift, stretch and shear. The calculation method uses a large fraction of the pixels available within the measured images and requires minimal human guidance in its operation. The method is demonstrated using measurements where residual stresses are made on a microscopic scale with hole drilling done using a Focused Ion Beam – Scanning Electron Microscope (FIB-SEM). This is a very challenging application because SEM images are subject to fluctuations that can introduce large artifacts when using DIC. Several series of measurements are described to illustrate the operation and effectiveness of the proposed residual stress computation technique.

Journal ArticleDOI
TL;DR: In this article, a diffraction assisted image correlation (DAIC) method for 3D displacement measurement using a single camera and 2D-DIC algorithm is presented, where a transmission diffraction grating is placed between the specimen and the camera, resulting in multiple images which are then used to obtain apparent in-plane displacements using 2D DIC.
Abstract: Digital Image Correlation (DIC) provides a full-field non-contact optical method for accurate deformation measurement of materials, devices and structures. The measurement of three-dimensional (3D) deformation using DIC in general requires imaging with two cameras and a 3D-DIC code. In the present work, a new experimental technique, namely, Diffraction Assisted Image Correlation (DAIC) for 3D displacement measurement using a single camera and 2D-DIC algorithm is presented. A transmission diffraction grating is placed between the specimen and the camera, resulting in multiple images which are then used to obtain apparent in-plane displacements using 2D-DIC. The true in-plane and out-of-plane displacements of the specimen are obtained from the apparent in-plane displacements and the diffraction angle of the grating. The validity and accuracy of the DAIC method are demonstrated through 3D displacement measurement of a small thin membrane. This technique provides new avenues for performing 3D deformation measurements at small length scales and/or dynamic loading conditions.

Journal ArticleDOI
TL;DR: In this article, a test equipment has been developed to measure the in-plane cyclic behavior of sheet metals at elevated temperatures, which can be wellsuited to measure cyclic material behavior, especially the anisotropic and asymmetric hardening of lightweight materials.
Abstract: New test equipment has been developed to measure the in-plane cyclic behavior of sheet metals at elevated temperatures. The tester has clamping dies with adjustable side force to prevent the sheet specimens from buckling during compressive loading. In addition to the room temperature experiment, cartridge type heaters are inserted in the clamping dies so that the specimen can be heated up to 400 °C during the cyclic tests. For the strain measurement, a non-contact type laser extensometer is used. In order to validate the newly developed test device, the tension-compression (and compression-tension) tests under pre-strains and various temperatures have been performed. As model materials, the aluminum alloy sheet which exhibits a large Bauschinger effect and the magnesium alloy sheet which exhibits different amounts of asymmetry under cyclic loading are used. The developed device can be well-suited to measure the cyclic material behavior, especially the anisotropic and asymmetric hardening of light-weight materials.

Journal ArticleDOI
TL;DR: In this paper, a novel subpixel registration algorithm with Gaussian windows is proposed for accurate deformation measurement in digital image correlation technique, which automatically minimize the influence of subset sizes by self-adaptively tuning the Gaussian window shapes with the aid of a weighted sum-of-squared difference correlation criterion.
Abstract: A novel subpixel registration algorithm with Gaussian windows is put forward for accurate deformation measurement in digital image correlation technique. Based on speckle image quality and potential deformation states, this algorithm can automatically minimize the influence of subset sizes by self-adaptively tuning the Gaussian window shapes with the aid of a so-called weighted sum-of-squared difference correlation criterion. Numerical results of synthetic speckle images undergoing in-plane sinusoidal displacement fields demonstrate that the proposed algorithm can significantly improve displacement and strain measurement accuracy especially in the case with relatively large deformation.

Journal ArticleDOI
TL;DR: In this article, the authors used microlithography, digital image correlation and tensile test in order to investigate the reasons behind the heterogeneous strain distribution at the grain scale, which was carried out on single phase ferritic steel and two dual phase steels with ferrite and different hard particle martensite contents.
Abstract: This work uses microlithography, digital image correlation and tensile test in order to investigate the reasons behind the heterogeneous strain distribution at the grain scale. Scanning Electron Microscope images are taken to examine the relationship between microstructure features and strain heterogeneity. The study is carried out on single phase ferritic steel and two dual phase steels with ferrite and different hard particle martensite contents. Useful image correlation is obtained in grains with diameters of 2–3 μm for the martensite and ranging from 10 to 20 μm for the ferrite. To prevent a decrease of image correlation success, some technical aspects as the microgrid step and bar width are extensively tackled with for intermediate deformations (>10 %). The different levels of longitudinal intragranular strains observed inside the ferrite grains are not correlated with their orientation, shape, size or the presence (and content) of hard phase in the material.

Journal ArticleDOI
TL;DR: In this paper, the authors analyze the phenomenon of neutron emissions from very brittle rock specimens in com- pression from an exper- imental point of view and conclude that the anomalous chemical balances of major events that have affected the geo- mechanical and geochemical evolution of the Earth's Crust should be considered as an indirect evidence of the piezo- nuclear fission reactions considered above.
Abstract: Neutron emission measurements, by means of He 3 devices and bubble detectors, were performed during three different kinds of compression tests on brittle rocks: (i) under monotonic displacement control, (ii) under cyclic loading, and (iii) by ultrasonic vibration. The material used for the tests was Luserna stone, with different specimen sizes and shapes, and consequently with different brittleness numbers. Some studies had been already conducted on the different forms of energy emitted during the failure of brittle materials. They are based on the signals captured by acous- tic emission measurement systems, or on the detection of electromagnetic charge. On the other hand, piezonuclear neutron emissions from very brittle rock specimens in com- pression have been discovered only very recently. In this paper, the authors analyse this phenomenon from an exper- imental point of view. Since the analyzed material contains iron, additional experiments have been performed on steel specimens subjected to tension and compression, observing, also in this case, neutron emissions well distinguishable from the background level. Our conjecture is that piezonu- clear reactions involving fission of iron into aluminum, or into magnesium and silicon, should have occurred during compression damage and failure. This hypothesis is con- firmed by the direct evidence of Energy Dispersive X-ray Spectroscopy (EDS) tests conducted on the specimens. It is also interesting to emphasize that the anomalous chemical balances of the major events that have affected the geo- mechanical and geochemical evolution of the Earth's Crust should be considered as an indirect evidence of the piezo- nuclear fission reactions considered above.

Journal ArticleDOI
TL;DR: In this article, a full-field optical method called Digital Gradient Sensing (DGS) for measuring stress gradients due to an impact load on a planar transparent sheet is presented.
Abstract: A full-field optical method called Digital Gradient Sensing (DGS) for measuring stress gradients due to an impact load on a planar transparent sheet is presented. The technique is based on the elasto-optic effect exhibited by transparent solids due to an imposed stress field causing angular deflections of light rays quantified using 2D digital image correlation method. The measured angular deflections are proportional to the in-plane gradients of stresses under plane stress conditions. The method is relatively simple to implement and is capable of measuring stress gradients in two orthogonal directions simultaneously. The feasibility of this method to study material failure/damage is demonstrated on transparent planar sheets of PMMA subjected to both quasi-static and dynamic line load acting on an edge. In the latter case, ultra high-speed digital photography is used to perform time-resolved measurements. The quasi-static measurements are successfully compared with those based on the Flamant solution for a line-load acting on a half-space in regions where plane stress conditions prevail. The dynamic measurements, prior to material failure, are also successfully compared with finite element computations. The measured stress gradients near the impact point after damage initiation are also presented and failure behavior is discussed.

Journal ArticleDOI
TL;DR: In this paper, the authors used a laminated plate with an open-hole under traction loading to identify all four ply elastic constants (E>>\ 1>>\, E>>\ 2>>\, ν"]=> 12>>\, G>>\ 12>>\ ) at once.
Abstract: The ply elastic constants needed for classical lamination theory analysis of multi-directional laminates may differ from those obtained from unidirectional laminates because of three dimensional effects. In addition, the unidirectional laminates may not be available for testing. In such cases, full-field displacement measurements offer the potential of identifying several material properties simultaneously. For that, it is desirable to create complex displacement fields that are strongly influenced by all the elastic constants. In this work, we explore the potential of using a laminated plate with an open-hole under traction loading to achieve that and identify all four ply elastic constants (E 1 , E 2 , ν 12 , G 12 ) at once. However, the accuracy of the identified properties may not be as good as properties measured from individual tests due to the complexity of the experiment, the relative insensitivity of the measured quantities to some of the properties and the various possible sources of uncertainty. It is thus important to quantify the uncertainty (or confidence) with which these properties are identified. Here, Bayesian identification is used for this purpose, because it can readily model all the uncertainties in the analysis and measurements, and because it provides the full coupled probability distribution of the identified material properties. In addition, it offers the potential to combine properties identified based on substantially different experiments. The full-field measurement is obtained by moire interferometry. For computational efficiency the Bayesian approach was applied to a proper orthogonal decomposition (POD) of the displacement fields. The analysis showed that the four orthotropic elastic constants are determined with quite different confidence levels as well as with significant correlation. Comparison with manufacturing specifications showed substantial difference in one constant, and this conclusion agreed with earlier measurement of that constant by a traditional four-point bending test. It is possible that the POD approach did not take full advantage of the copious data provided by the full field measurements, and for that reason that data is provided for others to use (as on line material attached to the article).

Journal ArticleDOI
TL;DR: In this article, a robust experimental fabrication procedure was developed to fabricate thermally stable unit cells with high aspect ratios, which can be assembled over a large area to create thin low-CTE foils.
Abstract: We design, fabricate, and test thin thermally stable metastructures consisting of bi-metallic unit cells and show how the coefficient of thermal expansion (CTE) of these metastructures can be finely and coarsely tuned by varying the CTE of the constituent materials and the unit cell geometry. Planar and three-dimensional finite element method modeling (FEM) is used to drive our design and inform experiments, and predict the response of these metastructures. We develop a robust experimental fabrication procedure in order to fabricate thermally stable samples with high aspect ratios. We use digital image correlation (DIC) and an infrared camera to experimentally measure displacement and temperature during testing and compute the CTE of our samples. The samples, composed of an aluminum core and an external titanium frame, exhibit a CTE of 2.6 ppm/°C, which is significantly lower than either constituent. These unit cells can be assembled over a large area to create thin low-CTE foils. Finally, we demonstrate how the approach developed in this work can be used to fabricate metastructures with CTE’s ranging from −3.6 ppm/°C to 8.4 ppm/°C.

Journal ArticleDOI
TL;DR: In this article, the authors investigated the reason why accurate pressure measurements are difficult to perform by identifying the parameters affecting the pressure recordings during water impact and formulated precautions in order to meet this goal.
Abstract: Water wave slamming is known as one of the most important load which marine constructions encounter. Especially the large and spiky local pressures moving fast over the body surface during a slamming event can be harmful for the structure. Analytical and numerical research on these pressure loads has already been performed, but however, quantitative experimental information necessary for validation of these studies is restricted. This lack in experimental data may originate from the fact that accurate pressure measurements are difficult to perform. This paper investigates the reason why this type of measurements is so difficult by identifying the parameters affecting the pressure recordings during water impact. According to the authors’ knowledge, no other paper is available in the open literature which investigates all these influencing factors. It has been observed that the pressure signal sampling rate, sensor position, water temperature, object surface conditions and water surface conditions all have an effect on the measured pressures. Only by controlling these parameters, accurate and reproducible results are possible. Precautions in order to meet this goal are formulated.

Journal ArticleDOI
TL;DR: In this article, the identification of macroscopic elastic parameters of a layer-to-layer interlock woven composite from a full-field measurement is dealt with, and their respective uncertainty is characterized with the help of numerical simulations.
Abstract: This study deals with the identification of macroscopic elastic parameters of a layer-to-layer interlock woven composite from a full-field measurement. As this woven composite has a coarse microstructure, the characteristic length of the weaving is not small as compared to the specimen size. A procedure based on an inverse identification method and full-field digital image correlation kinematic measurement is proposed to exploit a three-point bending test on short coupons to characterize the out-of-plane shear modulus. Each step of the proposed procedure is presented, and their respective uncertainty is characterized with the help of numerical simulations. The shear modulus is identified with an accuracy of about 1.5 % and is 15 % lower than the estimate obtained through Iosipescu tests. The proposed procedure shows a correlation between the ideal mesh size and the weaving period. It also reveals that the actual boundary conditions deviate from the ideal ones and hence a special attention is paid to their optimization.

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TL;DR: In this article, the acoustic emission (AE) study of precursory micro-cracking activity and fracture behavior of quasi-brittle materials such as concrete and cement mortar was performed.
Abstract: This article reports the acoustic emission (AE) study of precursory micro-cracking activity and fracture behaviour of quasi-brittle materials such as concrete and cement mortar. In the present study, notched three-point bend specimens (TPB) were tested under crack mouth opening displacement (CMOD) control at a rate of 0.0004 mm/sec and the accompanying AE were recorded using a 8 channel AE monitoring system. The various AE statistical parameters including AE event rate $$ \left( {\frac{dn }{dt }} \right) $$ , AE energy release rate $$ \left( {\frac{dE }{dt }} \right) $$ , amplitude distribution for computing the AE based b-value, cumulative energy (ΣE) and ring down count (RDC) were used for the analysis. The results show that the micro-cracks initiated and grew at an early stage in mortar in the pre peak regime. While in the case of concrete, the micro-crack growth occurred during the peak load regime. However, both concrete and mortar showed three distinct stages of micro-cracking activity, namely initiation, stable growth and nucleation prior to the final failure. The AE statistical behavior of each individual stage is dependent on the number and size distribution of micro-cracks. The results obtained in the laboratory are useful to understand the various stages of micro-cracking activity during the fracture process in quasi-brittle materials such as concrete & mortar and extend them for field applications.

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TL;DR: In this paper, the authors developed a methodology to obtain near-surface residual stresses for laser-peened aluminium alloy samples using the contour method and a new data analysis method based on spline smoothing was applied.
Abstract: A study was conducted to develop a methodology to obtain near-surface residual stresses for laser-peened aluminium alloy samples using the contour method. After cutting trials to determine the optimal cut parameters, surface contours were obtained and a new data analysis method based on spline smoothing was applied. A new criterion for determining the optimal smoothing parameters is introduced. Near-surface residual stresses obtained from the contour method were compared with X-ray diffraction and incremental hole drilling results. It is concluded that with optimal cutting parameters and data analysis, reliable near-surface residual stresses can be obtained by the contour method.

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TL;DR: In this article, an indirect tensile testing method is proposed to measure the full dynamic tensile stress-strain curve of low strength brittle solids, where the flattened-Brazilian disc (FBD) sample is loaded by modified split Hopkinson pressure bars (SHPB) system.
Abstract: An indirect tensile testing method is proposed to measure the full dynamic tensile stress-strain curve of low strength brittle solids. In this method, the flattened-Brazilian disc (FBD) sample is loaded by modified split Hopkinson pressure bars (SHPB) system. Low amplitude dynamic forces were measured with a pair of piezoelectric force transducers embedded in the incident bar and the transmitted bar. The evolution of tensile stress at the center of the disc sample was determined through finite element analyses using the measured stress in SHPB as inputs. In a traditional Brazilian test, a strain gauge is mounted at the center of the specimen to measure the tensile strain, which is difficult to apply for low strength brittle materials. Thus, two types of non-contact methods, the Digital Image Correlation (DIC) technique and the Laser Gap Gauge (LGG), were used to measure the strain. The DIC method was used to monitor the displacement and the strain map of the specimen during the test, from which the strain at the center of the specimen can be obtained. The accuracy of the DIC results was assessed, and the displacement and strain uncertainties of our system were 0.003 mm and 0.003, respectively. LGG was used to monitor the expansion of the disc perpendicular to the loading axis, from which the average tensile strain is deduced. The numerical simulation revealed that the tensile strain at the center of the specimen is proportional to the average tensile strain and that the ratio is not sensitive to the material elastic parameters. The strain measured through LGG was compared with that measured by the DIC method using photos captured with a synchronized high-speed camera. The result of the LGG method was 20 % smaller than that of the DIC process. However, the latter was limited by the number of frames of the high-speed camera. The feasibility of this methodology was demonstrated using a polymer-bonded explosive (PBX).