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Showing papers in "Materials Research Bulletin in 2004"


Journal ArticleDOI
TL;DR: In this paper, the citric acid sol-gel combustion method has been used for the synthesis of nanocrystalline hydroxyapatite (HAP) powder from calcium nitrate, diammonium hydrogen phosphate and citric acids.

163 citations


Journal ArticleDOI
TL;DR: In this paper, the dielectric and piezoelectric properties of the SPS-sintered NbO 3 samples were investigated and compared to that of hot-pressed samples.

141 citations


Journal ArticleDOI
TL;DR: In this paper, the authors investigated the effect of thermal treatment temperature on the crystal size of NiFe2O4 nanoparticles and calculated the activation energy of nanoparticles formation during calcination.

137 citations


Journal ArticleDOI
TL;DR: The n-type tungsten oxide (WO{sub 3} polycrystalline thin films have been prepared at an optimized substrate temperature of 250 deg. C by spray pyrolysis technique as discussed by the authors.

133 citations


Journal ArticleDOI
TL;DR: Carbon fiber composites with an epoxy resin matrix were subjected to microwave-heating experiments in order to volatilise the polymer content and to produce clean fibres for potential reuse in high-grade applications.

131 citations


Journal ArticleDOI
TL;DR: In this article, the structure of the as-synthesized samples and the presence of intended anions in the interlayer gallery of hydrotalcites were determined by X-ray diffraction and FTIR spectroscopy.

125 citations


Journal ArticleDOI
TL;DR: In this article, large-scale CeO 2 nanowires were prepared successfully by an improved sol-gel process within the nanochannels of porous anodic alumina templates.

111 citations


Journal ArticleDOI
TL;DR: In this paper, a modified solution combustion approach was used for the first time in the preparation of nanosize zirconia toughened alumina (ZTA) composite, and the products formed were characterised by powder X-ray diffractometry, Transmission electron microscopy and BET surface area analysis.

109 citations


Journal ArticleDOI
TL;DR: The starting materials used for synthesizing hydroxyapatite (HA) were Ca(NO 3 ) 2 ·4H 2 O and H 3 PO 4 with a Ca/P ratio of 1.67 while poly(e-caprolactone) (PCL) was used as the biodegradable polymer as mentioned in this paper.

103 citations


Journal ArticleDOI
TL;DR: In this paper, the synthesis and study of oxygen-deficient rare earth nickelates were described and the boundaries of oxygen and cation homogeneity ranges of Nd 1− x NiO 3− δ were determined for the first time.

101 citations



Journal ArticleDOI
TL;DR: Sodium titanate nanowires from brookite (or anatase) nanocrystallites were synthesized by a hydrothermal treating in 10m NaOH aqueous solution at 180°C.

Journal ArticleDOI
Xia Li1, Hong Liu1, Jiyang Wang1, Hongmei Cui1, Feng Han1 
TL;DR: In this article, nano-sized Ce-doped YAG phosphor particles were synthesized by a mixed solvothermal method using the stoichiometric amounts of inorganic aluminum and yttrium salts.

Journal ArticleDOI
TL;DR: In this article, the phase relation in the CeO 2 -Gd 2 O 3 system has been established under slow cooled conditions from 1400°C. Two phase regions, namely F-type cubic and C-Type cubic, were observed in this system, and the lattice thermal expansion coefficient was found to gradually increase on increasing the Ce 4+ content, within the C-type homogeneity range.

Journal ArticleDOI
TL;DR: In this paper, the effect of (Li,Ce) or (K, Ce) doping on the structures and properties of bismuth layer-structured ferroelectric (BLSF) CaBi 4 Ti 4 O 15 -based ceramics was studied.

Journal ArticleDOI
TL;DR: In this article, the role of B{sub 2}O{sub 3} in realizing the long phosphorescence of Eu(II)+Dy(III) doped strontium aluminates has been investigated.

Journal ArticleDOI
TL;DR: LiFePO{sub 4} is a potential candidate for the cathode material of the lithium secondary batteries, and a co-precipitation method was adopted to prepare LiFePO[sub 4] because it is simple and cheap as discussed by the authors.

Journal ArticleDOI
TL;DR: In this paper, one-step pretreatment of mixed HNO 3 and H 2 SO 4 was found effective in order to attain nanosized copper particles, the electroless plating parameters should be closely controlled; eg, the pH value of the plating solution, the temperature, and the concentration and titrating speed of HCOH.

Journal ArticleDOI
TL;DR: In this article, the thermal decomposition of tungstic acids into WO 3 · n H 2 O, n = 1/3, 1, 2 was analyzed by TG and DSC methods.

Journal ArticleDOI
TL;DR: In this paper, the structural properties of complex perovskite lead iron tungstate, Pb(Fe 2/3 W 1/3 )O 3 (PFW) which belongs to a class off disordered magnetoelectrics has been studied by neutron powder diffraction.

Journal ArticleDOI
TL;DR: In this paper, a comparative study of gas sensing behavior of nanocrystalline nickel ferrite synthesized by micro-emulsion and hydrothermal method to liquefied petroleum gas (LPG) is presented.

Journal ArticleDOI
TL;DR: In this article, Bismuth iron titanate (Bi 8 Fe 4 Ti 3 O 24 ) was synthesized by solid-state route and showed a ferroelectric transition around 776°C.

Journal ArticleDOI
TL;DR: In this paper, the authors used polycrystalline discs of PbWO{sub 4} (PWWO-10), WO-sub 3} (WO-01), ZnWO(sub 4) (ZWWO)-10, PWO-28 and Z WWO-46 composites for humidity sensing.

Journal ArticleDOI
TL;DR: In this paper, a model was presented to evaluate the concentration of species in a citric solution for preparing MgAl{sub 2}O{sub 4} ultrafine powder.

Journal ArticleDOI
TL;DR: In this article, the microstructure of indium tin oxide thin films was analyzed in order to investigate its dependence on deposition pressure and annealing temperature, and a correlation between microstructures and electro-optical properties was also established.

Journal ArticleDOI
TL;DR: In this article, the synthesis of YAG nanoparticles by the coprecipitation technique and the optimum conditions for the processing of transparent ceramics were discussed. But the results were limited.

Journal ArticleDOI
TL;DR: In this paper, 3.0% lanthanide europium ion modified TiO 2 sol (Eu 3+ -TiO 2 ) was fabricated by chemical coprecipitation-peptization method with TiCl 4 as precursor.

Journal ArticleDOI
TL;DR: In this paper, a direct template-exchange of hexavalent-more-than-5+ species was used to obtain a larger amount of UMCM-41 and MCM-48 in mesoporous mesovoids.

Journal ArticleDOI
TL;DR: In this article, the zinc selenide (ZnSe) thin films are deposited onto glass substrate using relatively simple and inexpensive successive ionic layer adsorption and reaction (SILAR) method.

Journal ArticleDOI
TL;DR: In this paper, the highly ordered polyaniline (PANI) nanotubes array was prepared by in situ polymerization using anodic aluminum oxide (AAO) as template.