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Showing papers in "Organic Preparations and Procedures International in 2004"


Journal ArticleDOI
TL;DR: In this paper, the authors present a review of recent developments in the history of theYDANTOIN CHEMISTRY, focusing on the use of chemical compounds in the production of synthetic drugs.

197 citations


Journal ArticleDOI
TL;DR: The preparation of TETRAMETHYLPIPERDINE-1-OXOAMMONlUM SALTS and their use as oxidanants in ORGANIC CHEMISTRY is described in this article.

91 citations


Journal ArticleDOI
TL;DR: In this article, the authors present recent advances in the CHEMISTRY of TRICHLOROMETHyl CHLOROFORMATE and bis-(TRICHLoromETHyl) CARBONATE.

54 citations


Journal ArticleDOI
TL;DR: In this article, the authors describe the reactivation of TETRONIC ACIDS in the context of base-promoted Dieckman cyclization and cyclization of y-Hydroxylated or y-Halogenated P-Ketoester.

45 citations


Journal ArticleDOI
TL;DR: DIBENZOZo et al. as discussed by the authors proposed a method for organic preparation and procedures, which can be found in OXEPINES: SYNTHESES AND APPLICATIONS.

28 citations



Journal ArticleDOI
TL;DR: In this article, the development of new synthetic methods leading to fused tri-and tetracyclic heterocycles, many of which have interesting biological activity such as antiviral and DNA intercalating properties, was discussed.

22 citations


Journal ArticleDOI
TL;DR: A Practical Synthesis of ETHYL L-GLUTAMINE (L-Theanine) Organic Preparations and Procedures International: Vol. 36, No. 2, pp. 182-185.

21 citations


Journal ArticleDOI
TL;DR: In this article, VILSMEIER-HAACK SYNTHESIS of AROMATIC ALDEHYDES USING bis-(TRICHLOROMETHYL) CARBONATE and DIMETHYLFORMAMIDE.

19 citations


Journal ArticleDOI
TL;DR: The most common method of synthesizing 5-aminopyrazoles involves the condensation of P-ketonitriles (2) with hydrazines (1) under a variety of conditions as mentioned in this paper.

18 citations


Journal ArticleDOI
TL;DR: In this paper, the authors present a review of the MolYBDENUM in ORGANIC SYNTHESIS and its application in the field of organic preparation and procedures.

Journal ArticleDOI
TL;DR: In this paper, a nucleophilic substitution of an allylic alkoxide on 2-fluoro-lnitrobenzene has been proposed for a variety of akyl nitroaromatic ethers.

Journal ArticleDOI
TL;DR: In this paper, it has been demonstrated that application of microwave irradiation (MWI) to organic reactions not only results in reduced reaction times but also in improved yield compared to those obtained under conventional conditions.

Journal ArticleDOI
TL;DR: A novel and an efficient procedure for preparation of 4-amino-l,l,3,3-tetrasubstituted guanidines in solution under very mild conditions, which involves the use of chloroformamidinium salts and the chloroimidazolidinium salt.

Journal ArticleDOI
TL;DR: Mammals have several enzyme systems for the detoxification of cyanide, a militarylcivilian threat agent of contemporary concern, viz., rhodanase and p-mercaptopyruvate sulfurtransferase, both enzymes catalyzing the conversion of cyanides to the non-toxic thiocyanate, the latter being excreted in the urine.

Journal ArticleDOI
TL;DR: In this paper, a comparison of the HYDROGENATION OF INTERMEDIATE (IRA) with direct reduction of the number of intermediates is presented, showing that the latter is more efficient than the former.

Journal ArticleDOI
TL;DR: In this paper, it was shown that 6 and 7-hydroxy flavones can be synthesized by sodium hydroxide-catalyzed cyclization of the corresponding 1,3-diketone in water.

Journal ArticleDOI
TL;DR: A FACILE one-pot preparation of isothiocyanates from N-formamides and sulfur powder with bis(TRICHLOROMETHyl) CARBONATE is described in this article.

Journal ArticleDOI
TL;DR: In this article, an expEDITIOUS, PRACTICAL LARGE SCALE SYNTHESIS of 4-AMINO-2-CHLORO-6,7-DIMETHOXYQUINAZOLINAZolinazoline.

Journal ArticleDOI
TL;DR: In this paper, a new route for 3-aminofurazan4carboxylic acid (2) was discovered, which was used for the synthesis of bioactive amides.

Journal ArticleDOI
Guangyu Xu1, Yuyuan Xie1, Xihan Wu1
TL;DR: In this paper, the authors present a detailed and direct synthesis of the ledendonate from the pyrolidone from PYRROLIDONE, and present a methodology for its use in organic preparation.

Journal ArticleDOI
TL;DR: In this paper, the authors describe the reaction of the williamson reaction in IONIC LIQUIDS to an ionic jellyfish attack, and present a detailed discussion of the event.

Journal ArticleDOI
Surya K. De1
TL;DR: In this article, the authors present a list of Tetrahedron Lett., 43, 1373 (2002) and E. Heldin, K. Linder, C. Pettersson, W. Szewczyk, L. Schreiber, J. Repic and T. Waykole.

Journal ArticleDOI
TL;DR: In this article, the authors present an efficient synthysis of IMIDAZO using a HYPERVALENT IODINE (III) sULFONATE.

Journal ArticleDOI
TL;DR: In this article, a synthesis of the title compounds was envisaged from the condensation of methyl 4amino1 -methyl-3-n-propyl pyrazole-5-carboxylate (1) with triethyl orthoformate (TEOF) in the presence of aromatic amines.

Journal ArticleDOI
TL;DR: In this paper, an N-(3-butenyl)-N-(2-nitrophenyl) amide derivatives were used as precursors for a new synthesis of 2,3,4,5,tetrahydrolH-l,5-benzodiazepines.

Journal ArticleDOI
TL;DR: In this article, an efficient one-step conversion of 3-FORMYLCHROMONES into 3-CYANOCHEMONES is described. But the conversion process is not described.

Journal ArticleDOI
TL;DR: The benzyl functionality is a useful protecting group for the phenolic hydroxyl group in organic synthesis as discussed by the authors, and it has been shown that benzyl ethers are stable under basic or mildly acidic conditions but readily cleaved by hydrogenolysis.

Journal ArticleDOI
TL;DR: In this paper, an efficient route to quinazolines bearing different substituents, such as nbutoxyand diethylaminoethoxy groups at the 6and 7-positions of the Quinazoline ring (Scheme I), is presented.

Journal ArticleDOI
TL;DR: In this paper, the authors present an efficient synthysis of 2,3-DICYANOINDOLE for organic preparation and procedures, and present a methodology for its implementation.