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Showing papers in "Review of Scientific Instruments in 2018"


Journal ArticleDOI
TL;DR: A peak field of 1200 T was generated by the electromagnetic flux-compression technique with a newly developed megagauss generator system and a significant increase in the liner imploding speed of up to 5 km/s was shown.
Abstract: A peak field of 1200 T was generated by the electromagnetic flux-compression (EMFC) technique with a newly developed megagauss generator system. Magnetic fields closely up to the turn-around peak were recorded by a reflection-type Faraday rotation magnetic-field optical-fiber probe. The performance was analyzed and compared with data obtained by the preceding EMFC experiments to show a significant increase in the liner imploding speed of up to 5 km/s.

119 citations


Journal ArticleDOI
TL;DR: A laboratory-scale LPBF test bed designed to accommodate diffraction and imaging experiments at a synchrotron X-ray source during LPBF operation is described and experimental results using Ti-6Al-4V, a widely used aerospace alloy, as a model system are presented.
Abstract: In situ X-ray-based measurements of the laser powder bed fusion (LPBF) additive manufacturing process produce unique data for model validation and improved process understanding. Synchrotron X-ray imaging and diffraction provide high resolution, bulk sensitive information with sufficient sampling rates to probe melt pool dynamics as well as phase and microstructure evolution. Here, we describe a laboratory-scale LPBF test bed designed to accommodate diffraction and imaging experiments at a synchrotron X-ray source during LPBF operation. We also present experimental results using Ti-6Al-4V, a widely used aerospace alloy, as a model system. Both imaging and diffraction experiments were carried out at the Stanford Synchrotron Radiation Lightsource. Melt pool dynamics were imaged at frame rates up to 4 kHz with a ∼1.1 μm effective pixel size and revealed the formation of keyhole pores along the melt track due to vapor recoil forces. Diffraction experiments at sampling rates of 1 kHz captured phase evolution and lattice contraction during the rapid cooling present in LPBF within a ∼50 × 100 μm area. We also discuss the utility of these measurements for model validation and process improvement.

113 citations


Journal ArticleDOI
TL;DR: A brief overview of each powder instrument at ORNL is provided and the complementarity across the suite is detailed, including full refinements over large Q ranges, total scattering methods, fast measurements under changing conditions, and a wide array of sample environments.
Abstract: The suite of neutron powder diffractometers at Oak Ridge National Laboratory (ORNL) utilizes the distinct characteristics of the Spallation Neutron Source and High Flux Isotope Reactor to enable the measurements of powder samples over an unparalleled regime at a single laboratory. Full refinements over large Q ranges, total scattering methods, fast measurements under changing conditions, and a wide array of sample environments are available. This article provides a brief overview of each powder instrument at ORNL and details the complementarity across the suite. Future directions for the powder suite, including upgrades and new instruments, are also discussed.

92 citations


Journal ArticleDOI
TL;DR: The calibration procedures include the treatment of anharmonicities in the trapping potential, as well as a protocol using a harmonic driving force, which is applicable if the sensor is coupled to a heat bath of unknown temperature.
Abstract: Optically levitated nanoparticles offer enormous potential for precision sensing. However, as for any other metrology device, the absolute measurement performance of a levitated-particle sensor is limited by the accuracy of the calibration relating the measured signal to an absolute displacement of the particle. Here, we suggest and demonstrate calibration protocols for levitated-nanoparticle sensors. Our calibration procedures include the treatment of anharmonicities in the trapping potential, as well as a protocol using a harmonic driving force, which is applicable if the sensor is coupled to a heat bath of unknown temperature. Finally, using the calibration, we determine the center-of-mass temperature of an optically levitated particle in thermal equilibrium from its motion and discuss the optimal measurement time required to determine the said temperature.

67 citations


Journal ArticleDOI
TL;DR: In the upcoming experimental campaign, a graphite scraper element, in front of the island divertor throat, will be tested as a possible means to protect the divertor pumping gap edges during the transient discharge evolution.
Abstract: Wendelstein 7-X aims at quasi-steady state operation with up to 10 MW of heating power for 30 min. Power exhaust will be handled predominantly via 10 actively water cooled CFC (carbon-fiber-reinforced carbon) based divertor units designed to withstand power loads of 10 MW/m2 locally in steady state. If local loads exceed this value, a risk of local delamination of the CFC and failure of entire divertor modules arises. Infrared endoscopes to monitor all main plasma facing components are being prepared, and near real time software tools are under development to identify areas of excessive temperature rise, to distinguish them from non-critical events, and to trigger alarms. Tests with different cameras were made in the recent campaign. Long pulse operation enforces additional diagnostic design constraints: for example, the optics need to be thermally decoupled from the endoscope housing. In the upcoming experimental campaign, a graphite scraper element, in front of the island divertor throat, will be tested as a possible means to protect the divertor pumping gap edges during the transient discharge evolution.

59 citations


Journal ArticleDOI
Chong Shen1, Jiangtao Yang1, Jun Tang1, Jun Liu1, Huiliang Cao1 
TL;DR: A parallel processing algorithm of the temperature error based on variational mode decomposition (VMD) and an augmented nonlinear differentiator (AND) is proposed and an adaptive accelerometer factor determination method for AND is given based on the VMD, both of which improve the effectiveness of the de-noising process.
Abstract: The traditional processing model of the temperature error for a gyroscope is serial, meaning that de-noising and temperature drift compensation are implemented in a two-step procedure. Hence, the result of the latter depends on the performance of the former; in particular, negative de-noising produces a negative compensation result. To reduce this dependence, we propose a parallel processing algorithm of the temperature error based on variational mode decomposition (VMD) and an augmented nonlinear differentiator (AND). An application to a micro-electro-mechanical system gyroscope is described to demonstrate the effectiveness and applicability of the proposed algorithm. Its major advantages are (i) a combination of VMD, extreme learning machines, and AND is proposed, and an adaptive accelerometer factor determination method for AND is given based on the VMD, both of which improve the effectiveness of the de-noising process; (ii) temperature drift and noise in the temperature error can be extracted and processed synchronously, thereby reducing the dependency of drift compensation on the de-noising result and making the temperature error process more efficient.

58 citations


Journal ArticleDOI
TL;DR: A new laboratory-based instrument capable of delivering monochromated X-rays with an energy of 9.25 keV and a microfocused 30 × 45 μm2 X-ray spot is introduced that allows stable measurements under grazing incidence conditions to maximise signal intensities.
Abstract: Hard X-ray photoelectron spectroscopy (HAXPES) has seen continuous development since the first experiments in the 1970s. HAXPES systems are predominantly located at synchrotron sources due to low photoionization cross sections necessitating high X-ray intensities, which limits the technique’s availability to a wide range of users and potential applications. Here, a new laboratory-based instrument capable of delivering monochromated X-rays with an energy of 9.25 keV and a microfocused 30 × 45 μm2 X-ray spot is introduced. The system gives an excellent energy resolution of below 500 meV coupled with good X-ray intensity. It allows stable measurements under grazing incidence conditions to maximise signal intensities. This article outlines the instrument behavior, showcases applications including bulk and multilayer measurements, and describes the overall performance of the spectrometer. This system presents an alternative to synchrotron-based experimental end stations and will help expand the number and range of HAXPES experiments performed in the future.

55 citations


Journal ArticleDOI
TL;DR: The results of the preliminary experimental tests in a pulsed mode of operation are presented and the microwave power of up to 330 kW with an efficiency of 30% without collector depression was obtained.
Abstract: A 250 GHz continuous-wave (CW) gyrotron has been developed at the IAP RAS jointly with GYCOM Ltd., as a prototype of the microwave source for the envisaged prospective nuclear fusion power plants (DEMO). The main applications of such a tube are electron cyclotron resonance heating and electron cyclotron resonance current drive of magnetically confined plasma as well as its diagnostics based on collective Thomson scattering in various reactors for controlled thermonuclear fusion (e.g., tokamaks and stellarators). The results of the preliminary experimental tests in a pulsed mode of operation are presented. The microwave power of up to 330 kW with an efficiency of 30% without collector depression was obtained. At an accelerating voltage of 55 kV and an electron beam current of 12.5 A (which corresponds to the design parameters for CW operation), the measured output power was about 200 kW. The TEM00 mode content evaluated at the tube output is not less than 98.6%.

53 citations


Journal ArticleDOI
TL;DR: A comparison with a prototype spectrometer, based on the same principle, shows the substantial improvement in the spectral resolution and energy range for the present setup.
Abstract: We have built a laboratory spectrometer for X-ray emission spectroscopy. The instrument is employed in catalysis research. The key component is a von Hamos full cylinder optic with Highly Annealed Pyrolytic Graphite (HAPG) as a dispersive element. With this very efficient optic, the spectrometer subtends an effective solid angle of detection of around 1 msr, allowing for the analysis of dilute samples. The resolving power of the spectrometer is approximately E/ΔE = 4000, with an energy range of ∼2.3 keV–10 keV. The instrument and its characteristics are described herein. Further, a comparison with a prototype spectrometer, based on the same principle, shows the substantial improvement in the spectral resolution and energy range for the present setup. The paper concludes with a discussion of sample handling. A compilation of HAPG fundamentals and related publications are given in a brief Appendix.

50 citations


Journal ArticleDOI
TL;DR: This paper presents the current wall-embedded Langmuir probe system installed on the Tokamak à Configuration Variable (TCV), as well as the analysis tool chain used to interpret the current-voltage characteristic obtained when the probes are operated in swept-bias conditions, based on a four-parameter fit combined with a minimum temperature approach.
Abstract: This paper presents the current wall-embedded Langmuir probe system installed on the Tokamak a Configuration Variable (TCV), as well as the analysis tool chain used to interpret the current-voltage characteristic obtained when the probes are operated in swept-bias conditions. The analysis is based on a four-parameter fit combined with a minimum temperature approach. In order to reduce the effect of plasma fluctuations and measurement noise, several current-voltage characteristics are usually averaged before proceeding to the fitting. The impact of this procedure on the results is investigated, as well as the possible role of finite resistances in the circuitry, which could lead to an overestimation of the temperature. We study the application of the procedure in a specific regime, the plasma detachment, where results from other diagnostics indicate that the electron temperature derived from the Langmuir probes might be overestimated. To address this issue, we explore other fitting models and, in particular, an extension of the asymmetric double probe fit, which features effects of sheath expansion. We show that these models yield lower temperatures (up to approximately 60%) than the standard analysis in detached conditions, particularly for a temperature peak observed near the plasma strike point, but a discrepancy with other measurements remains. We explore a possible explanation for this observation, the presence of a fast electron population, and assess how robust the different methods are in such conditions.

49 citations


Journal ArticleDOI
TL;DR: In this article, the authors presented measured absolute detection efficiencies for protons of several micro-channel plates (MCPs), including efficiency enhanced “funnel MCPs.
Abstract: Modern momentum imaging techniques allow for the investigation of complex molecules in the gas phase by detection of several fragment ions in coincidence. For these studies, it is of great importance that the single-particle detection efficiency e is as high as possible, as the overall efficiency scales with en, i.e., the power of the number of detected particles. Here we present measured absolute detection efficiencies for protons of several micro-channel plates (MCPs), including efficiency enhanced “funnel MCPs.” Furthermore, the relative detection efficiency for two-, three-, four-, and five-body fragmentation of CHBrClF has been examined. The “funnel” MCPs exhibit an efficiency of approximately 90%, gaining a factor of 24 (as compared to “normal” MCPs) in the case of a five-fold ion coincidence detection.

Journal ArticleDOI
TL;DR: This work presents an instrument called "tOMography Nano crYo (OMNY)," dedicated to high resolution 3D scanning x-ray microscopy at cryogenic conditions via hard X-ray ptychography, achieved via dedicated laser interferometry and closed-loop position control reaching sub-10 nm positioning accuracy.
Abstract: For many scientific questions gaining three-dimensional insight into a specimen can provide valuable information. We here present an instrument called “tOMography Nano crYo (OMNY),” dedicated to high resolution 3D scanning x-ray microscopy at cryogenic conditions via hard X-ray ptychography. Ptychography is a lens-less imaging method requiring accurate sample positioning. In OMNY, this in achieved via dedicated laser interferometry and closed-loop position control reaching sub-10 nm positioning accuracy. Cryogenic sample conditions are maintained via conductive cooling. 90 K can be reached when using liquid nitrogen as coolant, and 10 K is possible with liquid helium. A cryogenic sample-change mechanism permits measurements of cryogenically fixed specimens. We compare images obtained with OMNY with older measurements performed using a nitrogen gas cryo-jet of stained, epoxy-embedded retina tissue and of frozen-hydrated Chlamydomonas cells.

Journal ArticleDOI
TL;DR: The 2nd generation of a measurement chip is reported on, which allows for a simplified sample preparation process, and the measurement of samples deposited from the liquid phase using techniques like spin coating and drop casting.
Abstract: The characterization of nanostructured samples with at least one restricted dimension like thin films or nanowires is challenging, but important to understand their structure and transport mechanism, and to improve current industrial products and production processes. We report on the 2nd generation of a measurement chip, which allows for a simplified sample preparation process, and the measurement of samples deposited from the liquid phase using techniques like spin coating and drop casting. The new design enables us to apply much higher temperature gradients for the Seebeck coefficient measurement in a shorter time, without influencing the sample holder’s temperature distribution. Furthermore, a two membrane correction method for the 3ω thermal conductivity measurement will be presented, which takes the heat loss due to radiation into account and increases the accuracy of the measurement results significantly. Errors caused by different sample compositions, varying sample geometries, and different heat ...

Journal ArticleDOI
Jiaqi Yan1, Saikang Shen1, Yanan Wang1, Siyu Zhang1, Le Cheng1, Weidong Ding1 
TL;DR: The main advantage of this trigger is the simultaneous combination of the high repetition rate, low jitter, long lifetime, and great simplicity in a compact structure.
Abstract: This paper presents the design and development of a trigger with a high repetition rate, low jitter, and compact structure for the pseudospark switch (PSS), which includes an improved Marx generator based on avalanche transistors and a corona-plasma trigger unit. The generator adopted a novel 3 × 12-stage Marx circuit based on avalanche transistors in which the failure rate of transistors in the first and second stages was significantly reduced by connecting the parallel capacitors compared to the previous similar generator. The reason for the improved performance was also discussed. The main parameters of output pulses were an amplitude of -7 kV, rise time of 6 ns, jitter of 0.2 ns, and repetition rate of 2 kHz. The corona-plasma trigger unit adopted BaTiO3 ceramics with high er as the dielectric and was arranged in the hollow cathode of the PSS. The experiments of triggering a PSS prototype were conducted. The influence of anode voltage and pressure on the trigger delay and jitter was studied, and the minimum trigger jitter achieved <1 ns. This trigger worked for 107 shots at the repetition rate of 2 kHz continuously without obvious performance degradation and any failure of the generator. The main advantage of this trigger is the simultaneous combination of the high repetition rate, low jitter, long lifetime, and great simplicity in a compact structure.

Journal ArticleDOI
TL;DR: An ultra-high vacuum scanning tunneling microscope working under combined extreme conditions of ultra-low temperatures and high magnetic fields is described and the lowest effective electron temperature is estimated to be below 90 mK by measuring the superconducting-gap spectrum of aluminum.
Abstract: We describe the development and performance of an ultra-high vacuum scanning tunneling microscope working under combined extreme conditions of ultra-low temperatures and high magnetic fields. We combined a top-loading dilution refrigerator and a standard bucket dewar with a bottom-loading superconducting magnet to achieve 4.5 days operating time, which is long enough to perform various spectroscopic-imaging measurements. To bring the effective electron temperature closer to the mixing-chamber temperature, we paid particular attention to filtering out radio-frequency noise, as well as enhancing the thermal link between the microscope unit and the mixing chamber. We estimated the lowest effective electron temperature to be below 90 mK by measuring the superconducting-gap spectrum of aluminum. We confirmed the long-term stability of the spectroscopic-imaging measurement by visualizing superconducting vortices in the cuprate superconductor Bi2Sr2CaCu2O8+δ.

Journal ArticleDOI
TL;DR: In this paper, a single-channel rubidium radio-frequency atomic magnetometer operating in unshielded environments and near room temperature with a measured sensitivity of 130 fT/Hz was presented.
Abstract: We report on a single-channel rubidium radio-frequency atomic magnetometer operating in unshielded environments and near room temperature with a measured sensitivity of 130 fT/Hz. We demonstrate consistent, narrow-bandwidth operation across the kHz–MHz band, corresponding to three orders of magnitude of the magnetic field amplitude. A compensation coil system controlled by a feedback loop actively and automatically stabilizes the magnetic field around the sensor. We measure a reduction in the 50 Hz noise contribution by an order of magnitude. The small effective sensor volume, 57 mm3, increases the spatial resolution of the measurements. Low temperature operation, without any magnetic shielding, coupled with the broad tunability, and low beam power, dramatically extends the range of potential field applications for our device.

Journal ArticleDOI
TL;DR: The Heidelberg Compact EBIT (HC-EBIT) as discussed by the authors is a compact, room-temperature design for electron beam ion traps that can trap and extract highly charged ions.
Abstract: Electron beam ion traps (EBITs) are ideal tools for both production and study of highly charged ions (HCIs). In order to reduce their construction, maintenance, and operation costs, we have developed a novel, compact, room-temperature design, the Heidelberg Compact EBIT (HC-EBIT). Four already commissioned devices operate at the strongest fields (up to 0.86 T) reported for such EBITs using permanent magnets, run electron beam currents up to 80 mA, and energies up to 10 keV. They demonstrate HCI production, trapping, and extraction of pulsed Ar16+ bunches and continuous 100 pA ion beams of highly charged Xe up to charge state 29+, already with a 4 mA, 2 keV electron beam. Moreover, HC-EBITs offer large solid-angle ports and thus high photon count rates, e.g., in x-ray spectroscopy of dielectronic recombination in HCIs up to Fe24+, achieving an electron-energy resolving power of E/ΔE > 1500 at 5 keV. Besides traditional on-axis electron guns, we have also implemented a novel off-axis gun for laser, synchrotron, and free-electron laser applications, offering clear optical access along the trap axis. We report on its first operation at a synchrotron radiation facility demonstrating the resonant photoexcitation of highly charged oxygen.

Journal ArticleDOI
TL;DR: Simulations indicate that more than 109 photons on the sample per pulse-pair and up to about 10% photon energy separation can be achieved in the hard X-ray region using the SDL.
Abstract: A hard X-ray Split-and-Delay Line (SDL) under construction for the Materials Imaging and Dynamics station at the European X-Ray Free-Electron Laser (XFEL) is presented. This device aims at providing pairs of X-ray pulses with a variable time delay ranging from -10 ps to 800 ps in a photon energy range from 5 to 10 keV for photon correlation and X-ray pump-probe experiments. A custom designed mechanical motion system including active feedback control ensures that the high demands for stability and accuracy can be met and the design goals achieved. Using special radiation configurations of the European XFEL's SASE-2 undulator (SASE: Self-Amplified Spontaneous Emission), two-color hard x-ray pump-probe schemes with varying photon energy separations have been proposed. Simulations indicate that more than 109 photons on the sample per pulse-pair and up to about 10% photon energy separation can be achieved in the hard X-ray region using the SDL.

Journal ArticleDOI
TL;DR: The thermal helium beam edge diagnostic has recently been upgraded at the AUG tokamak experiment, offering fast and spatially highly resolved electron temperature and density profile measurements that cover the plasma edge and scrape-off layer region.
Abstract: The thermal helium beam edge diagnostic has recently been upgraded at the ASDEX Upgrade (AUG) tokamak experiment Line ratio spectroscopy on neutral helium is a valuable tool for simultaneous determination of the electron temperature and density of plasmas The diagnostic now offers a temporal resolution of 900 kHz with a spatial resolution of up to 3 mm at 32 lines of sight (LOS) simultaneously The LOS covers a radial region of 85 cm, starting at the limiter radius and reaching into the confined region beyond the separatrix Two components are of particular importance for the aforementioned hardware improvements The first is the optical head, which collects the light from the experiment Equipped with an innovative clamping system for optical fiber ends, an arbitrary distribution pattern of LOS can be achieved to gain radial and poloidal profiles The second major development is a new polychromator system that measures the intensity of the 587 nm, 667 nm, 706 nm, and 728 nm helium lines simultaneously for 32 channels with filter-photomultiplier tube arrays Thus, the thermal helium beam diagnostic supplements the AUG edge diagnostics, offering fast and spatially highly resolved electron temperature and density profile measurements that cover the plasma edge and scrape-off layer region Plasma fluctuations, edge localized modes, filaments, and other turbulent structures are resolved, allowing analysis of their frequency and localization or their propagation velocity

Journal ArticleDOI
TL;DR: A remote in situ laser-induced breakdown spectroscopic (RIS-LIBS) system has been developed to be an effective and routine method for the diagnosis of the composition of the PFCs on Experimental Advanced Superconducting Tokamak (EAST).
Abstract: The diagnosis of the fuel retention and impurity deposition on the plasma facing components (PFCs) is very important for monitoring plasma-wall interactions and improving the performance of long-pulse operation for tokamak devices. In this study, a remote in situ laser-induced breakdown spectroscopic (RIS-LIBS) system has been developed to be an effective and routine method for the diagnosis of the composition of the PFCs on Experimental Advanced Superconducting Tokamak (EAST). The RIS-LIBS system can be operated between EAST discharges via a remote network control system. This allows a flexible diagnosis for the PFCs at a specific EAST discharge operation or under planned plasma scenarios according to the experimental requirement. Measurements on the fuel retention and impurity deposition of the PFCs have been performed for the test of the RIS-LIBS system, and the depth resolution and the lateral resolution of the RIS-LIBS system have been achieved to be ∼100 nm and ∼3.0 mm, respectively. For the test of detectable elements, the fuel (deuterium) and impurities have been detected and identified clearly. In addition, the measurement of fuel abundance on the first wall as a function of the days of EAST deuterium plasma discharges has been carried out for the first time. These results well manifest a significant prospect of the RIS-LIBS for the diagnosis of the PFCs in the upcoming fusion devices like China Fusion Engineering Test Reactor (CFETR) and ITER.

Journal ArticleDOI
TL;DR: A suite of single-crystal neutron diffractometers at the Oak Ridge National Laboratory has no equal at any other neutron scattering facility worldwide and offers the potential to re-assert singlecrystal diffraction using neutrons as a significant tool to study nuclear and magnetic structures of small unit cell crystals, nuclear structures of macromolecules, and diffuse scattering as discussed by the authors.
Abstract: The nascent suite of single-crystal neutron diffractometers at the Oak Ridge National Laboratory has no equal at any other neutron scattering facility worldwide and offers the potential to re-assert single-crystal diffraction using neutrons as a significant tool to study nuclear and magnetic structures of small unit cell crystals, nuclear structures of macromolecules, and diffuse scattering. Signature applications and features of single-crystal neutron diffraction are high resolution nuclear structure analysis, magnetic structure and spin density determinations, contrast variation (particularly D2O/H2O) for nuclear structural studies, lack of radiation damage when using crystals of biological molecules such as proteins, and the fidelity to measure nuclear and magnetic diffuse scattering with elastic discrimination.

Journal ArticleDOI
F. Tricot1, D. H. Phung1, M. Lours1, Stéphane Guérandel1, E. de Clercq1 
TL;DR: In this paper, the power stabilization of a diode laser with an acousto-optic modulator was investigated in the frequency domain and the relative power noise was reduced at the level of 2.2 × 10−8 Hz−1/2 in the range 1-100 kHz.
Abstract: Laser power fluctuations can significantly reduce the device performances in various applications. High frequency fluctuations impact the signal-to-noise ratio, while slow variations can reduce the device repeatability or accuracy. Here we report experimental investigations on the power stabilization of a diode laser with an acousto-optic modulator. In the frequency domain, the relative power noise is reduced at the level of 2.2 × 10−8 Hz−1/2 in the range 1-100 kHz. The slow variations are studied in the time domain. The relative Allan standard deviation is measured at the level of 6 × 10−7 at 100 s averaging time. Above 100 s, the instability increases and reaches 2 × 10−6 at 10 000 s.

Journal ArticleDOI
TL;DR: An acoustic levitation system that automatically injects, transports, merges and ejects liquid droplets in mid-air, integrated reliably into a single automatic system paves the way for the adoption of mid- air acoustophoretic processing in biological, chemical and pharmaceutical applications.
Abstract: We present an acoustic levitation system that automatically injects, transports, merges and ejects liquid droplets in mid-air. The system consists of a phased array operating at 40 kHz on top of a plane reflector. The phase array generates multiple focal points at independent positions that form standing waves between the array and the reflector. In the reflector there is an inlet for a piezoelectric droplet injector which automatically inserts liquid droplets at the lower pressure nodes of the standing waves, and a hole that serves as an outlet for ejecting the processed droplets out of the system. Simulations of the acoustic radiation potential acting on the levitating droplets are in good agreement with the experiments. High-speed footage captured the functioning of the system in four fluidic operations: injection, transport, merging and ejection of liquid droplets. Having these operations integrated reliably into a single automatic system paves the way for the adoption of mid-air acoustophoretic processing in biological, chemical and pharmaceutical applications.

Journal ArticleDOI
TL;DR: This review focuses on two aspects: How to perform the multi-tip STM measurements and how to analyze the acquired data in order to gain insight into nanoscale charge transport processes for a variety of samples.
Abstract: In scanning tunneling microscopy, we witness in recent years a paradigm shift from “just imaging” to detailed spectroscopic measurements at the nanoscale and multi-tip scanning tunneling microscope (STM) is a technique following this trend. It is capable of performing nanoscale charge transport measurements like a “multimeter at the nanoscale.” Distance-dependent four-point measurements, the acquisition of nanoscale potential maps at current carrying nanostructures and surfaces, as well as the acquisition of I − V curves of nanoelectronic devices are examples of the capabilities of the multi-tip STM technique. In this review, we focus on two aspects: How to perform the multi-tip STM measurements and how to analyze the acquired data in order to gain insight into nanoscale charge transport processes for a variety of samples. We further discuss specifics of the electronics for multi-tip STM and the properties of tips for multi-tip STM, and present methods for a tip approach to nanostructures on insulating substrates. We introduce methods on how to extract the conductivity/resistivity for mixed 2D/3D systems from four-point measurements, how to measure the conductivity of 2D sheets, and how to introduce scanning tunneling potentiometry measurements with a multi-tip setup. For the example of multi-tip measurements at freestanding vapor liquid solid grown nanowires, we discuss contact resistances as well as the influence of the presence of the probing tips on the four point measurements.

Journal ArticleDOI
TL;DR: The results obtained with a lock-in camera that paves the way for real-time, wide-field magnetometry at the nanotesla level and with a micrometer resolution are demonstrated.
Abstract: Sensitive, real-time optical magnetometry with nitrogen-vacancy centers in diamond relies on accurate imaging of small (≪10−2), fractional fluorescence changes across the diamond sample. We discuss the limitations on magnetic field sensitivity resulting from the limited number of photoelectrons that a camera can record in a given time. Several types of camera sensors are analyzed, and the smallest measurable magnetic field change is estimated for each type. We show that most common sensors are of a limited use in such applications, while certain highly specific cameras allow achieving nanotesla-level sensitivity in 1 s of a combined exposure. Finally, we demonstrate the results obtained with a lock-in camera that paves the way for real-time, wide-field magnetometry at the nanotesla level and with a micrometer resolution.

Journal ArticleDOI
TL;DR: The hybrid meta-heuristics optimization technique, namely, the salp swarm algorithm (SSA), is applied to the optimal sizing of a CMOS differential amplifier and the comparator circuit.
Abstract: In this paper, an automatic design method based on a swarm intelligence approach for CMOS analog integrated circuit (IC) design is presented. The hybrid meta-heuristics optimization technique, namely, the salp swarm algorithm (SSA), is applied to the optimal sizing of a CMOS differential amplifier and the comparator circuit. SSA is a nature-inspired optimization algorithm which mimics the navigating and hunting behavior of salp. The hybrid SSA is applied to optimize the circuit design parameters and to minimize the MOS transistor sizes. The proposed swarm intelligence approach was successfully implemented for an automatic design and optimization of CMOS analog ICs using Generic Process Design Kit (GPDK) 180 nm technology. The circuit design parameters and design specifications are validated through a simulation program for integrated circuit emphasis simulator. To investigate the efficiency of the proposed approach, comparisons have been carried out with other simulation-based circuit design methods. The performances of hybrid SSA based CMOS analog IC designs are better than the previously reported studies.

Journal ArticleDOI
TL;DR: The wavemeter-based frequency stabilization scheme can be applied to a wide range of atoms and molecules for laser spectroscopy, cooling, and trapping, and provides excellent stability in single-channel operation.
Abstract: We present the characterization of a laser frequency stabilization scheme using a state-of-the-art wavelength meter based on solid Fizeau interferometers. For a frequency-doubled Ti-sapphire laser operated at 461 nm, an absolute Allan deviation below 10-9 with a standard deviation of 1 MHz over 10 h is achieved. Using this laser for cooling and trapping of strontium atoms, the wavemeter scheme provides excellent stability in single-channel operation. Multi-channel operation with a multimode fiber switch results in fluctuations of the atomic fluorescence correlated to residual frequency excursions of the laser. The wavemeter-based frequency stabilization scheme can be applied to a wide range of atoms and molecules for laser spectroscopy, cooling, and trapping.

Journal ArticleDOI
TL;DR: This paper presents a lever-type stick-slip piezoelectric actuator based on the lever amplification principle that can achieve large strokes, high velocity, and bidirectional actuation with a single piezOElectric stack.
Abstract: This paper presents a lever-type stick-slip piezoelectric actuator based on the lever amplification principle. The proposed actuator can achieve large strokes, high velocity, and bidirectional actuation with a single piezoelectric stack. The finite element simulation of the lever-type flexible hinge is performed, and the designed prototype is tested. When the voltage is 100 Vp-p, the maximum forward velocity is 7.69 mm/s under the symmetry of 20%. The maximum reverse velocity is 7.12 mm/s under the symmetry of 80%. The maximum forward and reverse displacement deviation within 10 cycles is 0.88 μm, and the maximum load can reach 105 g.

Journal ArticleDOI
TL;DR: Results of this study suggest that electro-thermal co-design techniques and top-side thermal management solutions are necessary to exploit the full potential of the Ga2O3 material system.
Abstract: The higher critical electric field of β-gallium oxide (Ga2O3) gives promise to the development of next generation power electronic devices with improved size, weight, power, and efficiency over current state-of-the-art wide bandgap devices based on 4H-silicon carbide (SiC) and gallium nitride (GaN). However, it is expected that Ga2O3 devices will encounter serious thermal issues due to the poor thermal conductivity of the material. In this work, self-heating in Ga2O3 Schottky barrier diodes under different regimes of the diode operation was investigated using diverse optical thermography techniques including thermoreflectance thermal imaging, micro-Raman thermography, and infrared thermal microscopy. 3D coupled electro-thermal modeling was used to validate experimental results and to understand the mechanism of heat generation for the diode structures. Measured top-side and cross-sectional temperature fields suggest that device and circuit engineers should account for the concentrated heat generation that occurs near the anode/Ga2O3 interface and/or the lightly doped drift layer under both forward and high voltage reverse bias conditions. Results of this study suggest that electro-thermal co-design techniques and top-side thermal management solutions are necessary to exploit the full potential of the Ga2O3 material system.

Journal ArticleDOI
TL;DR: The Ion Cyclotron Emission (ICE) diagnostic on the DIII-D tokamak consists of two outboard midplane systems that collected a large set of radio frequency measurements in the 2015-2018 experimental campaigns by digitizing signals at 200 MSamples/s for ∼5 s per discharge.
Abstract: The Ion Cyclotron Emission (ICE) diagnostic on the DIII-D tokamak consists of two outboard midplane systems In the first system, straps of an ion cyclotron range of frequencies antenna are configured as receiving antennas For the second system, dedicated magnetic probes incorporated into the outer wall of carbon tiles have recently been restored These systems collected a large set of radio frequency measurements in the 2015–2018 experimental campaigns by digitizing signals at 200 MSamples/s for ∼5 s per discharge Each shot typically yields 32 GB of data; techniques for successful handling and analysis of this challengingly large dataset are discussed The raw voltage fluctuations (<02 V and <1 mW) are analyzed in frequency space via fast Fourier transforms Signals can be analyzed between 1 and 200 MHz with appropriate filtering and aliasing; this frequency range is limited by DC breaks used to provide 5 kV DC isolation These high-frequency signals are driven by energetic ions and electrons In particular, energetic-ion-driven ICE occurs at harmonics of the ion cyclotron frequency, enabling the frequency to be mapped to lab space via equilibrium reconstruction In many DIII-D plasmas, ICE is emitted from the radial center of the plasmaThe Ion Cyclotron Emission (ICE) diagnostic on the DIII-D tokamak consists of two outboard midplane systems In the first system, straps of an ion cyclotron range of frequencies antenna are configured as receiving antennas For the second system, dedicated magnetic probes incorporated into the outer wall of carbon tiles have recently been restored These systems collected a large set of radio frequency measurements in the 2015–2018 experimental campaigns by digitizing signals at 200 MSamples/s for ∼5 s per discharge Each shot typically yields 32 GB of data; techniques for successful handling and analysis of this challengingly large dataset are discussed The raw voltage fluctuations (<02 V and <1 mW) are analyzed in frequency space via fast Fourier transforms Signals can be analyzed between 1 and 200 MHz with appropriate filtering and aliasing; this frequency range is limited by DC breaks used to provide 5 kV DC isolation These high-frequency signals are driven by energetic ions and electrons In part