Showing papers in "Review of Scientific Instruments in 2020"
TL;DR: An overview of considerations for designing accurate resonator experiments to characterize loss, including applicable types of losses, cryogenic setup, device design, and methods for extracting material and interface losses are provided, summarizing techniques that have been evolving for over two decades.
Abstract: The performance of superconducting circuits for quantum computing is limited by materials losses. In particular, coherence times are typically bounded by two-level system (TLS) losses at single photon powers and millikelvin temperatures. The identification of low loss fabrication techniques, materials, and thin film dielectrics is critical to achieving scalable architectures for superconducting quantum computing. Superconducting microwave resonators provide a convenient qubit proxy for assessing performance and studying TLS loss and other mechanisms relevant to superconducting circuits such as non-equilibrium quasiparticles and magnetic flux vortices. In this review article, we provide an overview of considerations for designing accurate resonator experiments to characterize loss, including applicable types of losses, cryogenic setup, device design, and methods for extracting material and interface losses, summarizing techniques that have been evolving for over two decades. Results from measurements of a wide variety of materials and processes are also summarized. Finally, we present recommendations for the reporting of loss data from superconducting microwave resonators to facilitate materials comparisons across the field.
105 citations
TL;DR: The requirements for multiplexed sources are studied, various approaches to multiplexing using different degrees of freedom are compared and higher single-photon probabilities are allowed.
Abstract: We review the rapid recent progress in single-photon sources based on multiplexing multiple probabilistic photon-creation events. Such multiplexing allows higher single-photon probabilities and lower contamination from higher-order photon states. We study the requirements for multiplexed sources and compare various approaches to multiplexing using different degrees of freedom.
93 citations
TL;DR: In this article, a full-field imaging momentum microscope with time-of-flight energy recording as the detector for mapping of 3D band structures in (kx, ky, E) parameter space with unprecedented efficiency.
Abstract: Time-resolved photoemission with ultrafast pump and probe pulses is an emerging technique with wide application potential. Real-time recording of nonequilibrium electronic processes, transient states in chemical reactions, or the interplay of electronic and structural dynamics offers fascinating opportunities for future research. Combining valence-band and core-level spectroscopy with photoelectron diffraction for electronic, chemical, and structural analyses requires few 10 fs soft X-ray pulses with some 10 meV spectral resolution, which are currently available at high repetition rate free-electron lasers. We have constructed and optimized a versatile setup commissioned at FLASH/PG2 that combines free-electron laser capabilities together with a multidimensional recording scheme for photoemission studies. We use a full-field imaging momentum microscope with time-of-flight energy recording as the detector for mapping of 3D band structures in (kx, ky, E) parameter space with unprecedented efficiency. Our instrument can image full surface Brillouin zones with up to 7 A−1 diameter in a binding-energy range of several eV, resolving about 2.5 × 105 data voxels simultaneously. Using the ultrafast excited state dynamics in the van der Waals semiconductor WSe2 measured at photon energies of 36.5 eV and 109.5 eV, we demonstrate an experimental energy resolution of 130 meV, a momentum resolution of 0.06 A−1, and a system response function of 150 fs.
73 citations
TL;DR: The transition from old space to new space along with increasing commercialization has a major impact on space flight, in general, and on electric propulsion (EP) by ion thrusters, in particular.
Abstract: The transition from old space to new space along with increasing commercialization has a major impact on space flight, in general, and on electric propulsion (EP) by ion thrusters, in particular Ion thrusters are nowadays used as primary propulsion systems in space This article describes how these changes related to new space affect various aspects that are important for the development of EP systems Starting with a historical overview of the development of space flight and of the technology of EP systems, a number of important missions with EP and the underlying technologies are presented The focus of our discussion is the technology of the radio frequency ion thruster as a prominent member of the gridded ion engine family Based on this discussion, we give an overview of important research topics such as the search for alternative propellants, the development of reliable neutralizer concepts based on novel insert materials, as well as promising neutralizer-free propulsion concepts In addition, aspects of thruster modeling and requirements for test facilities are discussed Furthermore, we address aspects of space electronics with regard to the development of highly efficient electronic components as well as aspects of electromagnetic compatibility and radiation hardness This article concludes with a presentation of the interaction of EP systems with the spacecraft
63 citations
TL;DR: A systematized review of the research on the production of nanosecond high-power pulses using solid-state generators based on an inductive energy store and a semiconductor opening switch that have been performed in the past 25 years is presented.
Abstract: This paper presents a systematized review of the research on the production of nanosecond high-power pulses using solid-state generators based on an inductive energy store and a semiconductor opening switch that have been performed in the past 25 years. This research has been underway since 1992-1993 when the nanosecond cutoff of ultrahigh-density currents in semiconductor diodes was discovered and named the SOS (Semiconductor Opening Switch) effect. The discovery of the SOS effect provided a breakthrough in the development of semiconductor generators, as their most important characteristics, such as pulse power and output voltage, were increased tens and hundreds of times compared with previously known semiconductor generators. In particular, in the nanosecond semiconductor technology, megavolt voltages combined with gigawatt peak powers have been achieved. This review considers the main physical processes that determine the mechanism of operation of a SOS based on the SOS effect. The principle of operation, design, and characteristics of SOS diodes and SOS generators is described, and prospects for their further development are discussed. Examples are given of using SOS generators in various pulsed power applications such as electron accelerators, X-ray pulse devices, high-power microwave electronics, pumping of gas lasers, and ignition of electrical discharges.
62 citations
TL;DR: This review discusses the evolution of PDV, its operational details, practical analysis, and outstanding challenges of this conceptually simple application of the optical Doppler effect.
Abstract: Photonic Doppler Velocimetry (PDV) is a fiber-based diagnostic for the extreme conditions created by high-speed impact, explosive detonation, electrical pulsed power, and intense laser ablation. PDV is a conceptually simple application of the optical Doppler effect, but measurements above 1 km/s only became practical at the beginning of the twenty-first century. This review discusses the evolution of PDV, its operational details, practical analysis, and outstanding challenges.
60 citations
TL;DR: The present paper gives an account of the status of the procurements, of the timeline, and of the voltage holding tests and experiments for MITICA, the full-scale prototype of the entire injector, devoted to the issues related to the accelerator, including voltage holding at low gas pressure.
Abstract: The requirements of ITER neutral beam injectors (1 MeV, 40 A negative deuterium ion current for 1 h) have never been simultaneously attained; therefore, a dedicated Neutral Beam Test Facility (NBTF) was set up at Consorzio RFX (Padova, Italy). The NBTF includes two experiments: SPIDER (Source for the Production of Ions of Deuterium Extracted from Rf plasma), the full-scale prototype of the source of ITER injectors, with a 100 keV accelerator, to investigate and optimize the properties of the ion source; and MITICA, the full-scale prototype of the entire injector, devoted to the issues related to the accelerator, including voltage holding at low gas pressure. The present paper gives an account of the status of the procurements, of the timeline, and of the voltage holding tests and experiments for MITICA. As for SPIDER, the first year of operation is described, regarding the solution of some issues connected with the radiofrequency power, the source operation, and the characterization of the first negative ion beam.
57 citations
TL;DR: This experimental platform has been used up to 2 TPa (20 Mbar) to determine the crystal structure, measure the density, and evaluate the strain-induced texturing of a variety of compressed samples spanning periods 2-7 on the periodic table.
Abstract: We report details of an experimental platform implemented at the National Ignition Facility to obtain in situ powder diffraction data from solids dynamically compressed to extreme pressures. Thin samples are sandwiched between tamper layers and ramp compressed using a gradual increase in the drive-laser irradiance. Pressure history in the sample is determined using high-precision velocimetry measurements. Up to two independently timed pulses of x rays are produced at or near the time of peak pressure by laser illumination of thin metal foils. The quasi-monochromatic x-ray pulses have a mean wavelength selectable between 0.6 A and 1.9 A depending on the foil material. The diffracted signal is recorded on image plates with a typical 2θ x-ray scattering angle uncertainty of about 0.2° and resolution of about 1°. Analytic expressions are reported for systematic corrections to 2θ due to finite pinhole size and sample offset. A new variant of a nonlinear background subtraction algorithm is described, which has been used to observe diffraction lines at signal-to-background ratios as low as a few percent. Variations in system response over the detector area are compensated in order to obtain accurate line intensities; this system response calculation includes a new analytic approximation for image-plate sensitivity as a function of photon energy and incident angle. This experimental platform has been used up to 2 TPa (20 Mbar) to determine the crystal structure, measure the density, and evaluate the strain-induced texturing of a variety of compressed samples spanning periods 2–7 on the periodic table.
45 citations
TL;DR: The results of characterization studies of the neutronic performance and installed devices at RADEN are described and the results of several demonstration studies for pulsed neutron imaging are shown.
Abstract: The energy-resolved neutron imaging system, RADEN, has been installed at the pulsed neutron source in the Materials and Life Science Experimental Facility of the Japan Proton Accelerator Research Complex. In addition to conventional neutron radiography and tomography, RADEN, the world’s first imaging beam-line at a pulsed neutron source, provides three main options for new, quantitative neutron imaging techniques: Bragg-edge imaging to visualize the spatial distribution of crystallographic information, resonance absorption imaging for elemental composition and temperature information, and polarized neutron imaging for magnetic field information. This paper describes the results of characterization studies of the neutronic performance and installed devices at RADEN and shows the results of several demonstration studies for pulsed neutron imaging.
44 citations
TL;DR: The new endstation to perform operando chemical analysis at solid-liquid interfaces by means of ambient pressure x-ray photoelectron spectroscopy (APXPS) is presented and will offer unique opportunities for fundamental studies of phenomena that take place atSolid- liquid interfaces and that are relevant for fields such as electrochemistry, photochemistry, or biochemistry.
Abstract: A new endstation to perform operando chemical analysis at solid–liquid interfaces by means of ambient pressure x-ray photoelectron spectroscopy (APXPS) is presented. The endstation is located at the Swiss Light Source and can be attached to the soft x-ray in situ spectroscopy beamline (X07DB) for solid–gas type experiments and to a tender x-ray beamline (PHOENIX I) for solid–liquid interface experiments. The setup consists of three interconnected ultrahigh vacuum chambers: one for sample preparation using surface science techniques, the analysis chamber for APXPS experiments, and an entry-lock chamber for sample transfer across the two pressure regimes. The APXPS chamber is designed to study solid–liquid interfaces stabilized by the dip and pull method. Using a three-electrode setup, the potential difference across the solid-electrolyte interface can be controlled, as is demonstrated here using an Ir(001) electrode dipped and pulled from a 0.1M KOH electrolyte. The new endstation is successfully commissioned and will offer unique opportunities for fundamental studies of phenomena that take place at solid–liquid interfaces and that are relevant for fields such as electrochemistry, photochemistry, or biochemistry, to name a few.
40 citations
TL;DR: The design, construction, and operation results of an 18 T 70 mm cold-bore high temperature superconductor (HTS) no-insulation (NI) magnet, which is developed for an axion haloscope experiment, may represent the first high field HTS user magnet that experienced long-term operation of over one year.
Abstract: We report the design, construction, and operation results of an 18 T 70 mm cold-bore high temperature superconductor (HTS) no-insulation (NI) magnet, which is developed for an axion haloscope experiment. The magnet consists of 44 double-pancake coils wound with multi-width and multi-thickness REBa2Cu3O7−x (RE = rare earth) tapes. Owing to the NI feature, the magnet is highly compact; is 162 mm in outer diameter and 476 mm tall; and provides an environment of 0.22 T2 m3 within the cold-bore target space of 66 mm in diameter and 200 mm in length. After an initial performance test at SuNAM Co. Ltd., the magnet was installed at the Center for Axion and Precision Physics Research (CAPP) of the Institute for Basic Science in Daejeon, South Korea, in August 2017. The magnet has been successfully operating at the CAPP since then, except for maintenance in October 2018. The magnet may represent the first high field HTS user magnet that experienced long-term operation of over one year.
TL;DR: The mass spectra show that ion clusters of the dopants can be produced with only few helium atoms attached, which will be important for messenger spectroscopy and for the scientific research of clusters and nanoscale materials in general.
Abstract: The demand for nanoscale materials of ultra-high purity and narrow size distribution is addressed. Clusters of Au, C60, H2O, and serine are produced inside helium nanodroplets using a combination of ionization, mass filtering, collisions with atomic or molecular vapor, and electrostatic extraction, in a specific and novel sequence. The helium droplets are produced in an expansion of cold helium gas through a nozzle into vacuum. The droplets are ionized by electron bombardment and subjected to a mass filter. The ionic and mass-selected helium droplets are then guided through a vacuum chamber filled with atomic or molecular vapor where they collide and “pick up” the vapor. The dopants then agglomerate inside the helium droplets around charge centers to singly charged clusters. Evaporation of the helium droplets is induced by collisions in a helium-filled radio frequency (RF)-hexapole, which liberates the cluster ions from the host droplets. The clusters are analyzed with a time-of-flight mass spectrometer. It is demonstrated that using this sequence, the size distribution of the dopant cluster ions is distinctly narrower compared to ionization after pickup. Likewise, the ion cluster beam is more intense. The mass spectra show, as well, that ion clusters of the dopants can be produced with only few helium atoms attached, which will be important for messenger spectroscopy. All these findings are important for the scientific research of clusters and nanoscale materials in general.
TL;DR: A setup for time-resolved momentum microscopy driven by a 1 MHz fs EUV table-top light source optimized for the generation of 26.5 eV photons provides simultaneous access to the temporal evolution of the photoelectron's kinetic energy and in-plane momentum.
Abstract: Recent progress in laser-based high-repetition rate extreme ultraviolet (EUV) light sources and multidimensional photoelectron spectroscopy enables the build-up of a new generation of time-resolved photoemission experiments. Here, we present a setup for time-resolved momentum microscopy driven by a 1 MHz fs EUV table-top light source optimized for the generation of 26.5 eV photons. The setup provides simultaneous access to the temporal evolution of the photoelectron’s kinetic energy and in-plane momentum. We discuss opportunities and limitations of our new experiment based on a series of static and time-resolved measurements on graphene.
TL;DR: In this paper, an 11 eV tr-ARPES setup was presented, which can be operated at high repetition rates (up to 250 kHz) while using input pulse energies down to 3 µJ.
Abstract: Performing time- and angle-resolved photoemission (tr-ARPES) spectroscopy at high momenta necessitates extreme ultraviolet laser pulses, which are typically produced via high harmonic generation (HHG). Despite recent advances, HHG-based setups still require large pulse energies (from hundreds of μJ to mJ) and their energy resolution is limited to tens of meV. Here, we present a novel 11 eV tr-ARPES setup that generates a flux of 5 × 1010 photons/s and achieves an unprecedented energy resolution of 16 meV. It can be operated at high repetition rates (up to 250 kHz) while using input pulse energies down to 3 µJ. We demonstrate these unique capabilities by simultaneously capturing the energy and momentum resolved dynamics in two well-separated momentum space regions of a charge density wave material ErTe3. This novel setup offers the opportunity to study the non-equilibrium band structure of solids with exceptional energy and time resolutions at high repetition rates.
TL;DR: This work presents the implementation of high-frequency gating InGaAs/InP SPDs with a PDE as high as 60% at 1550 nm, and develops a monolithic readout circuit of weak avalanche extraction to minimize the parasitic capacitance for the suppression of the afterpulsing effect.
Abstract: InGaAs/InP single-photon detectors (SPDs) are widely used for near-infrared photon counting in practical applications. Photon detection efficiency (PDE) is one of the most important parameters for SPD characterization, and therefore, increasing PDE consistently plays a central role in both industrial development and academic research. Here, we present the implementation of high-frequency gating InGaAs/InP SPDs with a PDE as high as 60% at 1550 nm. On one hand, we optimize the structure design and device fabrication of InGaAs/InP single-photon avalanche diodes with an additional dielectric-metal reflection layer to relatively increase the absorption efficiency of incident photons by ∼20%. On the other hand, we develop a monolithic readout circuit of weak avalanche extraction to minimize the parasitic capacitance for the suppression of the afterpulsing effect. With 1.25 GHz sine wave gating and optimized gate amplitude and operation temperature, the SPD is characterized to reach a PDE of 60% with a dark count rate (DCR) of 340 kcps. For practical use, given 3 kcps DCR as a reference, the PDE reaches ∼40% PDE with an afterpulse probability of 5.5%, which can significantly improve the performance for the near-infrared SPD-based applications.
TL;DR: The FIREBIRD mission has addressed all of its primary science objectives, and its long lifetime and focus on conjunctions has enabled additional science beyond the scope of the original mission.
Abstract: FIREBIRD-II is a National Science Foundation funded CubeSat mission designed to study the scale size and energy spectrum of relativistic electron microbursts. The mission consists of two identical 1.5 U CubeSats in a low earth polar orbit, each with two solid state detectors that differ only in the size of their geometric factors and fields of view. Having two spacecraft in close orbit allows the scale size of microbursts to be investigated through the intra-spacecraft separation when microbursts are observed simultaneously on each unit. Each detector returns high cadence (10 s of ms) measurements of the electron population from 200 keV to >1 MeV across six energy channels. The energy channels were selected to fill a gap in the observations of the Heavy Ion Large Telescope instrument on the Solar, Anomalous, and Magnetospheric Particle Explorer. FIREBIRD-II has been in orbit for 5 years and continues to return high quality data. After the first month in orbit, the spacecraft had separated beyond the expected scale size of microbursts, so the focus has shifted toward conjunctions with other magnetospheric missions. FIREBIRD-II has addressed all of its primary science objectives, and its long lifetime and focus on conjunctions has enabled additional science beyond the scope of the original mission. This paper presents a brief history of the FIREBIRD mission’s science goals, followed by a description of the instrument and spacecraft. The data products are then discussed along with some caveats necessary for proper use of the data.
RWTH Aachen University1, University of Warsaw2, VU University Amsterdam3, University of Sassari4, University of Liège5, University of Sannio6, ATOMKI7, University of Debrecen8, University of Pisa9, National Institute of Geophysics and Volcanology10, INAF11, University of Minnesota12, University of Melbourne13, Sapienza University of Rome14, Roma Tre University15, IAC16, University of Pécs17, Budapest University of Technology and Economics18
TL;DR: This paper provides an overview of the site-selection criteria for ET, provides a formalism to evaluate the direct impact of environmental noise on ET sensitivity, and outline the necessary elements of a site-characterization campaign.
Abstract: The Einstein Telescope (ET) is a proposed next-generation, underground gravitational-wave detector to be based in Europe. It will provide about an order of magnitude sensitivity increase with respect to the currently operating detectors and, also extend the observation band targeting frequencies as low as 3 Hz. One of the first decisions that needs to be made is about the future ET site following an in-depth site characterization. Site evaluation and selection is a complicated process, which takes into account science, financial, political, and socio-economic criteria. In this paper, we provide an overview of the site-selection criteria for ET, provide a formalism to evaluate the direct impact of environmental noise on ET sensitivity, and outline the necessary elements of a site-characterization campaign.
TL;DR: In this paper, a table-top extreme ultraviolet time and angle-resolved photoemission spectroscopy (trARPES) system is presented, featuring both a hemispherical analyzer and a momentum microscope within the same setup.
Abstract: Time-of-flight-based momentum microscopy has a growing presence in photoemission studies, as it enables parallel energy- and momentum-resolved acquisition of the full photoelectron distribution. Here, we report table-top extreme ultraviolet time- and angle-resolved photoemission spectroscopy (trARPES) featuring both a hemispherical analyzer and a momentum microscope within the same setup. We present a systematic comparison of the two detection schemes and quantify experimentally relevant parameters, including pump- and probe-induced space-charge effects, detection efficiency, photoelectron count rates, and depth of focus. We highlight the advantages and limitations of both instruments based on exemplary trARPES measurements of bulk WSe2. Our analysis demonstrates the complementary nature of the two spectrometers for time-resolved ARPES experiments. Their combination in a single experimental apparatus allows us to address a broad range of scientific questions with trARPES.
TL;DR: In this paper, a nano-nodiamond hyperpolarizer was proposed for room-temperature DNP, where 13C nuclei within the diamond particles are hyper-polarized via the Nitrogen-Vacancy (NV) centers.
Abstract: Dynamic Nuclear Polarization (DNP) is a powerful suite of techniques that deliver multifold signal enhancements in nuclear magnetic resonance (NMR) and MRI. The generated athermal spin states can also be exploited for quantum sensing and as probes for many-body physics. Typical DNP methods require the use of cryogens, large magnetic fields, and high power microwave excitation, which are expensive and unwieldy. Nanodiamond particles, rich in Nitrogen-Vacancy (NV) centers, have attracted attention as alternative DNP agents because they can potentially be optically hyperpolarized at room temperature. Here, unraveling new physics underlying an optical DNP mechanism first introduced by Ajoy et al. [Sci. Adv. 4, eaar5492 (2018)], we report the realization of a miniature "optical nanodiamond hyperpolarizer," where 13C nuclei within the diamond particles are hyperpolarized via the NV centers. The device occupies a compact footprint and operates at room temperature. Instrumental requirements are very modest: low polarizing fields, low optical and microwave irradiation powers, and convenient frequency ranges that enable miniaturization. We obtain the best reported optical 13C hyperpolarization in diamond particles exceeding 720 times of the thermal 7 T value (0.86% bulk polarization), corresponding to a ten-million-fold gain in averaging time to detect them by NMR. In addition, the hyperpolarization signal can be background-suppressed by over two-orders of magnitude, retained for multiple-minute long periods at low fields, and deployed efficiently even to 13C enriched particles. Besides applications in quantum sensing and bright-contrast MRI imaging, this work opens possibilities for low-cost room-temperature DNP platforms that relay the 13C polarization to liquids in contact with the high surface-area particles.
TL;DR: A new approach to positron emission particle tracking based on machine learning algorithms is introduced, demonstrating novel methods for particle location, tracking, and trajectory separation that require no prior knowledge of the number of tracers within the system.
Abstract: We introduce a new approach to positron emission particle tracking based on machine learning algorithms, demonstrating novel methods for particle location, tracking, and trajectory separation. The method allows radioactively labeled particles to be located, in three-dimensional space, with high temporal and spatial resolution, requiring no prior knowledge of the number of tracers within the system and can successfully distinguish multiple particles separated by distances as small as 2 mm. The technique's spatial resolution is observed to be invariant with the number of tracers used, allowing large numbers of particles to be tracked simultaneously, with no loss of data quality.
TL;DR: The elements inserted into the beam path, challenges encountered during integration with an in-service microscope, and early results from an electric-field-driven pump-probe experiment are described, with ideas for making this class of instruments broadly applicable for examining cyclical and repeatable phenomena.
Abstract: A 300 keV transmission electron microscope was modified to produce broadband pulsed beams that can be, in principle, between 40 MHz and 12 GHz, corresponding to temporal resolution in the nanosecond to picosecond range without an excitation laser. The key enabling technology is a pair of phase-matched modulating and de-modulating traveling wave metallic comb striplines (pulsers). An initial temporal resolution of 30 ps was achieved with a strobe frequency of 6.0 GHz. The placement of the pulsers, mounted immediately below the gun, allows for preservation of all optical configurations, otherwise available to the unmodified instrument, and therefore makes such a post-modified instrument for dual-use, i.e., both pulsed-beam mode (i.e., stroboscopic time-resolved) and conventional continuous waveform mode. In this article, we describe the elements inserted into the beam path, challenges encountered during integration with an in-service microscope, and early results from an electric-field-driven pump–probe experiment. We conclude with ideas for making this class of instruments broadly applicable for examining cyclical and repeatable phenomena.
TL;DR: The design specifics of the W7-X CXRS system are outlined and examples of the initial results obtained, including typical ion temperature profiles for several common heating scenarios, toroidal flow and radial electric field derived from velocity measurements, beam attenuation via beam emission spectra, and normalized impurity density profiles under some typical plasma conditions.
Abstract: The Charge Exchange Recombination Spectroscopy (CXRS) diagnostic has become a routine diagnostic on almost all major high temperature fusion experimental devices. For the optimized stellarator Wendelstein 7-X (W7-X), a highly flexible and extensive CXRS diagnostic has been built to provide high-resolution local measurements of several important plasma parameters using the recently commissioned neutral beam heating. This paper outlines the design specifics of the W7-X CXRS system and gives examples of the initial results obtained, including typical ion temperature profiles for several common heating scenarios, toroidal flow and radial electric field derived from velocity measurements, beam attenuation via beam emission spectra, and normalized impurity density profiles under some typical plasma conditions.
TL;DR: A high energy resolution x-ray spectrometer for the tender x-rays regime (1.6-5.0 keV) that was designed and operated at Stanford Synchrotron Radiation Lightsource is presented and performance is discussed.
Abstract: We present a high energy resolution x-ray spectrometer for the tender x-ray regime (1.6–5.0 keV) that was designed and operated at Stanford Synchrotron Radiation Lightsource. The instrument is developed on a Rowland geometry (500 mm of radius) using cylindrically bent Johansson analyzers and a position sensitive detector. By placing the sample inside the Rowland circle, the spectrometer operates in an energy-dispersive mode with a subnatural line-width energy resolution (∼0.32 eV at 2400 eV), even when an extended incident x-ray beam is used across a wide range of diffraction angles (∼30° to 65°). The spectrometer is enclosed in a vacuum chamber, and a sample chamber with independent ambient conditions is introduced to enable a versatile and fast-access sample environment (e.g., solid/gas/liquid samples, in situ cells, and radioactive materials). The design, capabilities, and performance are presented and discussed.
TL;DR: This work discussed the methodology for measuring in-plane thermal conductivity of layered semiconductors and semimetals without any transducer layer and demonstrated using the analytical thermal model that the measurements showed much-improved accuracy compared with conventional FDTR measurement with a transducers.
Abstract: Measuring anisotropic thermal conductivity has always been a challenging task in thermal metrology. Although recent developments of pump-probe thermoreflectance techniques such as variable spot sizes, offset pump-probe beams, and elliptical beams have enabled the measurement of anisotropic thermal conductivity, a metal film transducer enabled for the absorption of the modulated pump laser beam and the detection of the thermoreflectance signal. However, the existence of the transducer would cause in-plane heat spreading, suppressing the measurement sensitivity to the in-plane thermal conductivity. In addition, the transducer film also adds complexity to data processing, since it requires careful calibration or fitting to determine extra parameters such as the film thickness and conductivity, and interface conductance between the transducer and the sample. In this work, we discussed the methodology for measuring in-plane thermal conductivity of layered semiconductors and semimetals without any transducer layer. We show that the removal of transducer results in the dominantly large sensitivity to in-plane thermal conductivity compared with other parameters, such as cross-plane thermal conductivity and the absorption depth of the laser beams. Transducerless frequency-domain thermoreflectance (FDTR) measurements are performed on three reference layered-materials, highly ordered pyrolytic graphite, molybdenum disulfide (MoS2), and bismuth selenide (Bi2Se3) and demonstrated using the analytical thermal model that the measured in-plane thermal conductivity showed much-improved accuracy compared with conventional FDTR measurement with a transducer.
TL;DR: This contribution describes the characterization of the SPIDER negative ion beam as a function of the source and accelerator parameters by means of the diagnostic calorimeter STRIKE in the volume regime.
Abstract: The full-size ITER ion source prototype SPIDER (Source for the Production of Ions of Deuterium Extracted from a Radio frequency plasma) has recently started beam operation, whose objective is to produce 100 keV, 60 A hydrogen negative ions for 1 h. The source is presently operated in the volume regime, and the beam power is consequently limited. In such a configuration, the high resolution calorimeter STRIKE (Short-Time Retractable Instrumented Kalorimeter Experiment), even though uncooled, may be used instead of the SPIDER beam dump without limiting the beam-on time. STRIKE is formed by unidirectional carbon fiber–carbon matrix (CFC) composite tiles that are exposed to the beam while their temperature is recorded by using two infra-red cameras. This setup, thanks to the moderate broadening of the temperature profile guaranteed by the anisotropy of CFC, allows for the determination of detailed features of the beam current distribution (spatial resolution is about 2 mm). Furthermore, positively biasing the CFC tiles permits a direct electrical measurement of the negative ion beam current. Besides the total beam current and beam uniformity, which can be retrieved both by calorimetry and electrical measurement, beamlet divergence and deflection can be determined by infra-red thermography. This contribution describes the characterization of the SPIDER negative ion beam as a function of the source and accelerator parameters by means of the diagnostic calorimeter STRIKE in the volume regime.
TL;DR: The average image correlation coefficient of the new network increases 0.0320 and 0.0616 compared with the DNN and 2D-CNN, which demonstrates that the proposed method could give better reconstruction results, especially for the distribution of complex geometries.
Abstract: In recent years, due to the strong autonomous learning ability of neural network algorithms, they have been applied for electrical impedance tomography (EIT). Although their imaging accuracy is greatly improved compared with traditional algorithms, generalization for both simulation and experimental data is required to be improved. According to the characteristics of voltage data collected in EIT, a one-dimensional convolutional neural network (1D-CNN) is proposed to solve the inverse problem of image reconstruction. Abundant samples are generated with numerical simulation to improve the edge-preservation of reconstructed images. The TensorFlow-graphics processing unit environment and Adam optimizer are used to train and optimize the network, respectively. The reconstruction results of the new network are compared with the Deep Neural Network (DNN) and 2D-CNN to prove the effectiveness and edge-preservation. The anti-noise and generalization capabilities of the new network are also validated. Furthermore, experiments with the EIT system are carried out to verify the practicability of the new network. The average image correlation coefficient of the new network increases 0.0320 and 0.0616 compared with the DNN and 2D-CNN, respectively, which demonstrates that the proposed method could give better reconstruction results, especially for the distribution of complex geometries.
TL;DR: A Mach-Zehnder interferometer for measurement of temperature is proposed and experimentally demonstrated, which consists of two sections of single mode fiber and a section of thin core fiber spliced between the two SMFs, suitable for temperature measurement applications.
Abstract: A Mach-Zehnder interferometer for measurement of temperature is proposed and experimentally demonstrated, which consists of two sections of single mode fiber (SMF) and a section of thin core fiber spliced between the two SMFs. The two welding areas are heated and stretched to improve the split and recombination of light. The wavelength of the resonant dip will shift when temperature varies due to the thermo-optic and thermal expansion effect. The experimental results show that a temperature sensitivity of 65 pm/°C with a linear correlation coefficient of 0.996 can be achieved in a temperature range from 25 °C to 80 °C. Due to its ease of manufacture, low cost, and high sensitivity, the fiber optic temperature sensor is suitable for temperature measurement applications.
TL;DR: In this article, the authors describe the design, construction, and performance of an ultra-high vacuum (UHV) scanning tunneling microscope (STM) capable of imaging at dilution-refrigerator temperatures and equipped with a vector magnet.
Abstract: We describe the design, construction, and performance of an ultra-high vacuum (UHV) scanning tunneling microscope (STM) capable of imaging at dilution-refrigerator temperatures and equipped with a vector magnet. The primary objective of our design is to achieve a high level of modularity by partitioning the STM system into a set of easily separable, interchangeable components. This naturally segregates the UHV needs of STM instrumentation from the typically non-UHV construction of a dilution refrigerator, facilitating the usage of non-UHV materials while maintaining a fully bakeable UHV chamber that houses the STM. The modular design also permits speedy removal of the microscope head from the rest of the system, allowing for repairs, modifications, and even replacement of the entire microscope head to be made at any time without warming the cryostat or compromising the vacuum. Without using cryogenic filters, we measured an electron temperature of 184 mK on a superconducting Al(100) single crystal.
TL;DR: It is shown how pulse-pileup occurring in the detector signals at high photon flux can be corrected for and how this data acquisition scheme performs in terms of accuracy and efficiency.
Abstract: Time-Correlated Single Photon Counting (TCSPC) and time tagging of individual photon detections are powerful tools in many quantum optical experiments and other areas of applied physics. Using TCSPC, e.g., for the purpose of fluorescence lifetime measurements, is often limited in speed due to dead-time losses and pileup. We show that this limitation can be lifted by reducing the dead-time of the timing electronics to the absolute minimum imposed by the speed of the detector signals while maintaining high temporal resolution. A complementing approach to speedy data acquisition is parallelization by means of simultaneous readout of many detector channels. This puts high demands on the data throughput of the TCSPC system, especially in time tagging of individual photon arrivals. Here, we present a new design approach, supporting up to 16 input channels, an extremely short dead-time of 650 ps, very high time tagging throughput, and a timing resolution of 80 ps. In order to facilitate remote synchronization of multiple such instruments with highest precision, the new TCSPC electronics provide an interface for White Rabbit fiber optic networks. Beside fundamental research in the field of astronomy, such remote synchronization tasks arise routinely in quantum communication networks with node to node distances on the order of tens of kilometers. In addition to showing design features and benchmark results of new TCSPC electronics, we present application results from spectrally resolved and high-speed fluorescence lifetime imaging in medical research. We furthermore show how pulse-pileup occurring in the detector signals at high photon flux can be corrected for and how this data acquisition scheme performs in terms of accuracy and efficiency.
TL;DR: The development of a chemical vapor deposition (CVD) reactor which allows the investigation of ongoing chemical reactions on the surface of a molten metal at elevated temperatures and under reactive conditions is reported.
Abstract: Liquid metal catalysts (LMCats) (e.g., molten copper) can provide a new mass-production method for two-dimensional materials (2DMs) (e.g., graphene) with significantly higher quality and speed and lower energy and material consumption. To reach such technological excellence, the physicochemical properties of LMCats and the growth mechanisms of 2DMs on LMCats should be investigated. Here, we report the development of a chemical vapor deposition (CVD) reactor which allows the investigation of ongoing chemical reactions on the surface of a molten metal at elevated temperatures and under reactive conditions. The surface of the molten metal is monitored simultaneously using synchrotron x-ray scattering, Raman spectroscopy, and optical microscopy, thereby providing complementary information about the atomic structure and chemical state of the surface. To enable in situ characterization on a molten substrate at high temperatures (e.g., ∼1370 K for copper), the optical and x-ray windows need to be protected from the evaporating LMCat, reaction products, and intense heat. This has been achieved by creating specific gas-flow patterns inside the reactor. The optimized design of the reactor has been achieved using multiphysics COMSOL simulations, which take into account the heat transfer, fluid dynamics, and transport of LMCat vapor inside the reactor. The setup has been successfully tested and is currently used to investigate the CVD growth of graphene on the surface of molten copper under pressures ranging from medium vacuum up to atmospheric pressure.