Microstructure and Mechanical Properties of Weld Fusion Zones in Modified 9Cr-1Mo Steel
01 Jun 2001-Journal of Materials Engineering and Performance (Springer US)-Vol. 10, Iss: 3, pp 320-330
TL;DR: In this article, a plate of modified 9Cr-1Mo steel was welded with three different filler materials: standard 9Cr 1Mo, modified 9 Cr 1Mo and nickel-base alloy Inconel 182 post-weld heat treatment (PWHT) for periods of 2 and 6 hours.
Abstract: Modified 9Cr-1Mo steel finds increasing application in power plant construction because of its excellent high-temperature properties While it has been shown to be weldable and resistant to all types of cracking in the weld metal and heat-affected zone (HAZ), the achievement of optimum weld metal properties has often caused concern The design of appropriate welding consumables is important in this regard In the present work, plates of modified 9Cr-1Mo steel were welded with three different filler materials: standard 9Cr-1Mo steel, modified 9Cr-1Mo, and nickel-base alloy Inconel 182 Post-weld heat treatment (PWHT) was carried out at 730 and 760 °C for periods of 2 and 6 h The joints were characterized in detail by metallography Hardness, tensile properties, and Charpy toughness were evaluated Among the three filler materials used, although Inconel 182 resulted in high weld metal toughness, the strength properties were too low Between modified and standard 9Cr-1Mo, the former led to superior hardness and strength in all conditions However, with modified 9Cr-1Mo, fusion zone toughness was low and an acceptable value could be obtained only after PWHT for 6 h at 760 °C The relatively poor toughness was correlated to the occurrence of local regions of untransformed ferrite in the microstructure
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TL;DR: In this article, an infrared heating system was employed to heat the samples to 860 (STOT), 900 (ICHAZ), and 940°C (FGHAZ) for 1min, followed by cooling to room temperature.
Abstract: Microstructures of the heat-affected zone (HAZ) of a Gr. 91 steel weld were simulated to evaluate their effects on the creep life of the weld at elevated temperatures. The Ac1 and Ac3 temperatures of the Gr. 91 steel were determined by a dilatometer to be at 867 and 907 °C, respectively. An infrared heating system was employed to heat the samples to 860 (STOT), 900 (ICHAZ) and 940 °C (FGHAZ) for 1 min, followed by cooling to room temperature. The simulated specimens were then subjected to conventional post-weld heat treatment (PWHT) at 750 °C/2 h. After the PWHT, the tempered ICHAZ specimen had a shortest creep life among the specimens tested at 650 °C/60 MPa. Moreover, the simulated specimen heated to 860 °C (STOT) was more likely to fracture at 615 °C/80 MPa than others.
14 citations
01 Jan 1998
Abstract: AbstractCracking, or disbonding, along the fusion boundary in dissimilar metal welds has been a persistent problem, particularly in applications where austenitic alloys are clad on to structural steels for corrosion protection. Many failures in dissimilar metal welds occur as a result of cracking along a boundary that runs parallel to the fusion boundary in the adjacent weld metal. A preliminary investigation was undertaken to determine the nature and evolution of boundaries and structure in dissimilar metal welds using a simple ternary system composed of a pure iron substrate and a 70Ni–30Cu (Monel) filler metal. Changes in base metal dilution were found to alter the evolution of boundaries and structures near the fusion boundary dramatically. Optical metallography and electron microanalysis reveal that the resulting weld microstructures and boundaries are similar to those observed in engineering materials used for cladding and corrosion resistant overlay. Transmission electron diffraction analysis revea...
13 citations
TL;DR: In this paper , microstructural characteristics, mechanical properties, and residual stress magnitude of dissimilar weld joints (DWJs) between creep strength enhanced ferritic-martensitic (CSEF) P92 steel and austenitic stainless steel (ASS) 304L has been investigated.
13 citations
TL;DR: In this paper, the contribution made by each heat affected zone (HAZ) to the overall tensile behavior of the P91 steel weld joint was analyzed and three principal microstructures were identified.
Abstract: The present work aims to understand the contribution made by each heat affected zone (HAZ) to the overall tensile behavior of the P91 steel weld joint. The three principal microstructures o...
12 citations
TL;DR: In this article, the results of influence of different heat treatment conditions on the microstructure stability and mechanical properties of high-chromium X10CrMoVNNB9-1(P91) cast and forged (C&F) P91 steel were dealt with.
Abstract: The present research work deals with the results of influence of different heat treatment conditions on the microstructure stability and mechanical properties of high-chromium X10CrMoVNNB9-1(P91) cast and forged (C&F) P91 steel. The C&F P91 steel was subjected to various tempering condition in the temperature range of 350–760 °C and tempering time of 2 h, after the normalizing at 1040 °C for 40 min. The steel was also subjected to furnace cooled and water quenched heat treatment. Tempering at 650 and 760 °C produced the fully tempered lath martensitic structure with M23C6, M7C3, M3C and MX precipitates along the prior austenite grain boundaries, lath boundaries and matrix region. Tempering at 350 and 1000 °C produced the partially tempered columnar laths and untempered columnar laths martensite, respectively. The tempering time was also varied from 2 to 8 h for fixed tempering temperature of 760 °C. The optimum microstructure evolution was obtained for 6 h of tempering at 760 °C that led to improved mechanical properties.
12 citations
References
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TL;DR: In this article, the authors investigated the influence of trace amounts of V and Nb on the sequence of precipitation processes and identified the basis for the enhanced high-temperature strength compared to the standard 9Cr-lMo composition.
Abstract: The tempering and subsequent annealing of modified 9Cr-lMo steel have been investigated to determine the influence of trace amounts of V and Nb on the sequence of precipitation processes and to identify the basis for the enhanced high-temperature strength compared to the standard 9Cr-lMo composition. Air cooling (normalizing) from 1045 °C results in the precipitation of fine (Fe, Cr)3C particles within the martensite laths. Additional carbide precipitation and changes in the dislocation structure occur during the tempering of martensite at 700 °C and 760 °C after normalizing. The precipitation of M23C6 carbides occurs preferentially at lath interfaces and dislocations. The formation of Cr2C was detected during the first hour of tempering over the range of 650 °C to 760 °C but was replaced by V4C3 within 1 hour at 760 °C. During prolonged annealing at 550 °C to 650 °C, following tempering, the lath morphology remains relatively stable; partitioning of the laths into subgrains and some carbide coarsening are evident after 400 hours of annealing at 650 °C, but the lath morphology persists. The enhanced martensite lath stability is attributed primarily to the V4C3 precipitates distributed along the lath interfaces and is suggested as the basis for the improved performance of the modified 9Cr-lMo alloy under elevated temperature tensile and creep conditions.
166 citations
TL;DR: In this paper, a ternary system composed of a pure iron substrate and a 70Ni-30Cu filler metal was used to determine the nature and evolution of boundaries and structure in dissimilar metal welds.
Abstract: Cracking, or disbonding, along the fusion boundary in dissimilar metal welds has been a persistent problem, particularly in applications where austenitic alloys are clad on to structural steels for corrosion protection. Many failures in dissimilar metal welds occur as a result of cracking along a boundary that runs parallel to the fusion boundary in the adjacent weld metal. A preliminary investigation was undertaken to determine the nature and evolution of boundaries and structure in dissimilar metal welds using a simple ternary system composed of a pure iron substrate and a 70Ni–30Cu (Monel) filler metal. Changes in base metal dilution were found to alter the evolution of boundaries and structures near the fusion boundary dramatically. Optical metallography and electron microanalysis reveal that the resulting weld microstructures and boundaries are similar to those observed in engineering materials used for cladding and corrosion resistant overlay. Transmission electron diffraction analysis revea...
63 citations
TL;DR: In this paper, the authors describe an investigation of the creep rupture strength (CRS) of 9Cr•1Mo•V•Nb•N steel welded joints by welding thermal cycle simulation.
Abstract: Summary This paper describes an investigation of the creep rupture strength (CRS) of 9Cr‐1Mo‐V‐Nb‐N steel welded joints by welding thermal cycle simulation. The reduction in the CRS of the welded joints is successfully reproduced, and the reasons for this reduction are discussed from the perspective of fine precipitates in the matrix. The CRS of the simulated HAZ (heat affected zone) varies with the peak temperature of welding thermal cycle simulation (PT). It falls sharply beyond the Ac1 temperature, gradually reaching the minimum at the Ac3 temperature of 925 °C. At any higher temperature than Ac3, it rises steadily, showing almost the same CRS as the base metal at 1100°C. The weakest CRS of the simulated HAZ lies at the lowest limit of the CRS data band of various welded joints prepared by GTA (TIG), MMA, and submerged‐arc (SA) welding with the same base metal. The simulated HAZ is useful for evaluation and analysis of the CRS reduction of welded joints. Heating to the Ac3 temperature by welding change...
30 citations
TL;DR: In this paper, the authors describe the Weldability of 9Cr•1Mo•Nb, V P91 steel intended for service in the power industry and show that it can be used in a number of applications.
Abstract: (1996). Weldability of 9Cr‐1Mo‐Nb, V P91 steel intended for service in the power industry. Welding International: Vol. 10, No. 5, pp. 370-380.
14 citations