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Journal ArticleDOI

Near-infrared spectroscopy applications in pharmaceutical analysis

Jan Luypaert, +2 more
- 15 May 2007 - 
- Vol. 72, Iss: 3, pp 865-883
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TLDR
Recent developments in the pharmaceutical domain where NIR spectroscopy can be applied from raw material identification to final product release are reviewed.
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This article is published in Talanta.The article was published on 2007-05-15. It has received 387 citations till now.

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Citations
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Journal ArticleDOI

A review of near infrared spectroscopy and chemometrics in pharmaceutical technologies.

TL;DR: This review focuses on chemometric techniques and pharmaceutical NIRS applications, covering qualitative analyses, quantitative methods and on-line applications for near-infrared spectroscopy for pharmaceutical forms.
Journal ArticleDOI

Near infrared spectroscopy: A mature analytical technique with new perspectives - A review.

TL;DR: Last decade's advances and modern aspects of near infrared spectroscopy are critically examined and reviewed in order to understand why the technique has found intensive application in the most diverse and modern areas of analytical importance during the last ten years.
Journal ArticleDOI

Analytical techniques in pharmaceutical analysis: A review

TL;DR: In this paper, the role of analytical instrumentation and the analytical methods in assessing the quality of the drugs is highlighted and a review highlights a variety of analytical techniques such as titrimetric, chromatographic, spectroscopic, electrophoretic, and electrochemical and their corresponding methods that have been applied in the analysis of pharmaceuticals.
Journal ArticleDOI

Near infrared and Raman spectroscopy for the in-process monitoring of pharmaceutical production processes.

TL;DR: This paper aims at reviewing the use of Raman and NIR spectroscopy in the PAT setting, i.e., during processing, with special emphasis in pharmaceutics and dosage forms.
Journal ArticleDOI

Multivariate data analysis in pharmaceutics: a tutorial review.

TL;DR: An overview of latent variable methods used in pharmaceutics and integrated with advanced characterization techniques such as vibrational spectroscopy is provided.
References
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Book

Handbook of near-infrared analysis

Abstract: INTRODUCTION AND BACKGROUND Historical Development P,H. Hindle Basic Principles of Near-Infrared Spectroscopy H.W. Siesler Continuum and Discontinuum Theories of Diffuse Reflection P.R. Griffiths and D.J. Dahm INSTRUMENTATION AND CALIBRATION Commercial NIR Instrumentation J.J. Workman and D.A. Burns Fourier Transform Spectrophotometers in the Near-Infrared W.J. McCarthy and G.J. Kemeny Analysis Using Fourier Transforms W.F. McClure NIR Spectroscopy Calibration Basics J.J. Workman, Jr. Data Analysis: Multilinear Regression and Principal Component Analysis H, Mark Data Analysis: Calibration of NIR Instruments by PLS Regression H.R. Bjorsvik and H. Martens Aspects of Multivariate Calibration Applied to Near-Infrared Spectroscopy M.K. Boysworth and K.S. Booksh Transfer of Multivariate Calibration Models Based on Near-Infrared Spectroscopy E. Bouveresse and B. Campbell Calibration and Validation of Process Sensors G.E. Ritchie METHODS DEVELOPMENT Sampling, Sample Preparation, and Sample Selection P. Williams Indicator Variables: How They May Save Time and Money in NIR Analysis D.A. Burns Qualitative Discriminant Analysis H. Mark Spectral Reconstruction W.R. Hruschka APPLICATIONS Application of NIR Spectroscopy to Agricultural Products J.S. Shenk, J.J. Workman, Jr., and M.O. Westerhaus The Role of Near-Infrared Spectroscopy in Verifying Label Information in Agro-Forestry Products A. Garrido-Varo and E. de Pedro NIR Analysis of Cereal Products B.G. Osborne NIR Analysis of Dairy Products R. Frankhuizen Near-Infrared Spectra of Gases C.W. Brown Application for NIR Analysis of Beverages L.R. Kington and T.M. Jones NIR Analysis of Wool M.J. Hammersley and P.E. Townsend FT/IR vs. NIR: A Study with Lignocellulose D.A. Burns and T.P. Schultz NIR Analysis of Textiles J. Rodgers and S. Ghosh Recent Advances in the Use of Near-IR Spectroscopy in the Petrochemical Industry B. Buchanan NIR Analysis of Polymers C. Kradjel and K.A. Lee Getting NIR Out of the Gutter: The Analysis of Bowling Lane Condition Using Near-Infrared Reflectance Spectroscopy D.S. Burns, A.J. Siegel, and T. Buist Process Analytical Technologies (PAT) in the Pharmaceutical Industry E.W. Ciurczak Pharmaceutical Applications of Near-Infrared Spectroscopy C. Anderson, J.K. Drennen, and E.W. Ciurczak NIR in the Dietary Supplement Industry: Qualitative and Quantitative Analysis of Ingredients, Process Blends, and Final Products C. Kradjel Your Viagras - Genuine, Imitation, or Counterfeit? M.J. Vredenbregt, D. Mooibroek, and R. Hoogerbrugge Biomedical Applications of Near-Infrared Spectroscopy E.W. Ciurczak Near-Infrared Spectrometry in Cardiovascular Disease A.A. Urbas and R.A. Lodder In Vivo and In Vitro Near-Infrared Spectroscopic Determination of Blood Glucose and Other Biomedical Components with Chemometrics Y.P. Du, S. Kasemsumran, J. Jiang, and Y. Ozaki Plastics Analysis at Two National Laboratories Part A: Resin Identification Using Near-Infrared Spectroscopy and Neural Networks M. Kathleen Alam, S. Stanton, and G.A. Hebner Part B: Characterization of Plastic and Rubber Waste in a Hot Glovebox D.A. Burns Process Analysis G.J. Kemeny Detection of Counterfeit Currency and Turquoise D.A. Burns Counterfeit Cigars: Can Near Infrared Detect Them? D.A. Burns Local Methods and CARNAC-D T. Davies and T. Fearn
Journal ArticleDOI

Analysis of water in food by near infrared spectroscopy

TL;DR: The analysis of water by near infrared spectroscopy (NIRS) was the first successful application of this rapid technology which has developed over the past 30 years into a routine method for many agricultural commodities and food constituents.
Journal ArticleDOI

Process control and scale-up of pharmaceutical wet granulation processes: a review.

TL;DR: For wet granulation in high-shear mixers, specific methods based on the liquid saturation and the consistency of the wet mass are described and engineering techniques based on particle size population balance modelling are under development for both fluid bed and high- shear granulation.
Journal ArticleDOI

An evaluation of orthogonal signal correction applied to calibration transfer of near infrared spectra

TL;DR: In this paper, Orthogonal signal correction (OSC) is applied to NIR-spectra that were used in a calibration for the water content in a pharmaceutical product, and the performance of OSC was on the same level as for piecewise direct standardisation and spectral offset correction for each individual instrument and PLS-models with both instruments included.
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