Powder characterization and part density for powder bed fusion of 17-4 PH stainless steel
TL;DR: In this paper, the authors measured the variability of commercial 17-4 PH stainless steel powders to determine the effect of powder variability on part density and demonstrate characterization methods that ensure part quality.
Abstract: Characteristics of the metal powder are a key factor in the success of powder bed fusion (PBF) additive manufacturing. Powders for PBF from different manufacturers may have a different particle size and/or bulk packing and flow behavior. Powder properties change as the powder is reused for multiple builds. This study seeks to measure the variability of commercial 17-4 PH stainless steel powders to determine the effect of powder variability on part density and demonstrate characterization methods that ensure part quality.,Commercial atomized metal powders from four different vendors were produced with two different atomizing gases (N2 and argon). Powder was characterized in both new and extensively reused conditions. All powders were characterized for flow and packing behavior, particle size and internal porosity. Coupons were manufactured using the laser PBF process with optimized scan strategy and exposure parameters. The quality of fabricated parts was measured using bulk density measurement.,Despite differences in powder flowability and particle size, fully dense parts (>99 per cent) were produced using all powders, except one. Residual porosity in these parts appeared to result from gas trapped in the powder particles. The powder with extensive reuse (400+ h in machine fabrication environment) exhibited reduced flowability and increased fraction of fine particles, but still produced full density parts.,This study demonstrates that full density parts can be fabricated using powders with a range of flowability and packing behavior. This suggests that a single flowability measurement may be sufficient for quality assurance in a production environment.
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TL;DR: In this paper , the authors proposed a methodology to control the fatigue life of 17-4Ph stainless steel by selecting the most relevant manufacturing parameters: i.e., laser power, laser travel speed, hatch spacing and laser defocusing.
Abstract:
Purpose
The mechanical characterization of selective laser melting (SLM) parts is an industrial challenge. This paper aims to propose a methodology to control the fatigue life of 17-4Ph stainless steel by selecting the most relevant manufacturing parameters: i.e. laser power, laser travel speed, hatch spacing and laser defocusing.
Design/methodology/approach
A rough and refined design of experiment (DOE) is carried out to target the best combination of process parameters. A response surface model is then constructed to predict the parameter combination that optimizes the fatigue performance.
Findings
This study results show that the fatigue limit of the specimens manufactured by SLM (471.7 MPa at 107 cycles) has reached near 90% of the value found in samples machined from a bar. This demonstrates the applicability of the method proposed to optimize the SLM process and control the fatigue life of 17-4Ph stainless steel. The study results are compared with other research works and provide an increase of 18% to the fatigue limit.
Originality/value
This study showcases a DOE methodology to optimize the SLM parameters to achieve fatigue performance as great as that of solid 17-4Ph stainless steel.
29 citations
TL;DR: In this article , the authors address the powder recoating process parameters, intrinsic and extrinsic, that affect the non-sintered powder layer quality and, ultimately, the finished part quality.
14 citations
03 Sep 2021
TL;DR: In this paper, the dynamic response of two distinct lattice configurations, in terms of fatigue damage and life, is investigated and numerically tested under resonant conditions and random vibrations, until their failure.
Abstract: Lattice structures are lightweight engineering components suitable for a great variety of applications, including those in which the structural integrity under vibration fatigue is of paramount importance. In this work, we experimentally and numerically investigate the dynamic response of two distinct lattice configurations, in terms of fatigue damage and life. Specifically, Face-Centered-Cubic (FCC) and Diamond lattice-based structures are numerically studied and experimentally tested under resonant conditions and random vibrations, until their failure. To this end, Finite Element (FE) models are employed to match the dynamic behavior of the system in the neighborhood of the first natural frequency. The FE models are employed to estimate the structural integrity by way of frequency and tip acceleration drops, which allow for the identification of the failure time and a corresponding number of cycles to failure. Fatigue life under resonant conditions is well predicted by the application of conventional multiaxial high cycle fatigue criteria to the local state of stress. The same approach, combined with the Rainflow algorithm and Miner’s rule, provides good results in predicting fatigue damage under random vibrations.
4 citations
TL;DR: In this article , a review of powder spreading and spreadability in metal additive manufacturing is presented, focusing on the current progress in understanding spreading dynamics, the role of powder characteristics, the spreading systems and the testing tools developed for assessing powder spreadability.
4 citations
DOI•
01 Jan 2018
TL;DR: In this paper, a 304L stainless steel powder is subjected to five reuses in the selective laser melting (SLM) process to assess its recyclability through characterization of both powder and mechanical properties.
Abstract: During part fabrication by selective laser melting (SLM), a powder-bed fusion process in Additive Manufacturing (AM), a large amount of energy is input from the laser into the melt pool, causing generation of spatter and condensate, both of which have the potential to settle in the surrounding powder-bed compromising its reusability. In this study, 304L stainless steel powder is subjected to five reuses in the SLM process to assess its recyclability through characterization of both powder and mechanical properties. Powder was characterized morphologically by particle size distribution measurements, oxygen content with inert gas fusion analysis, and phase identification by X-ray diffraction. The evolution of powder properties with reuse was also correlated to tensile properties of the as-built material. The results show that reused powder coarsens and accrues more oxygen with each reuse. The effects of powder coarsening and oxygen increase on the tensile properties of fabricated parts are being investigated.
2 citations
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TL;DR: A comprehensive review of the main 3D printing methods, materials and their development in trending applications was carried out in this paper, where the revolutionary applications of AM in biomedical, aerospace, buildings and protective structures were discussed.
Abstract: Freedom of design, mass customisation, waste minimisation and the ability to manufacture complex structures, as well as fast prototyping, are the main benefits of additive manufacturing (AM) or 3D printing. A comprehensive review of the main 3D printing methods, materials and their development in trending applications was carried out. In particular, the revolutionary applications of AM in biomedical, aerospace, buildings and protective structures were discussed. The current state of materials development, including metal alloys, polymer composites, ceramics and concrete, was presented. In addition, this paper discussed the main processing challenges with void formation, anisotropic behaviour, the limitation of computer design and layer-by-layer appearance. Overall, this paper gives an overview of 3D printing, including a survey on its benefits and drawbacks as a benchmark for future research and development.
4,159 citations
TL;DR: The state-of-the-art of additive manufacturing (AM) can be classified into three categories: direct digital manufacturing, free-form fabrication, or 3D printing as discussed by the authors.
Abstract: This paper reviews the state-of-the-art of an important, rapidly emerging, manufacturing technology that is alternatively called additive manufacturing (AM), direct digital manufacturing, free form fabrication, or 3D printing, etc. A broad contextual overview of metallic AM is provided. AM has the potential to revolutionize the global parts manufacturing and logistics landscape. It enables distributed manufacturing and the productions of parts-on-demand while offering the potential to reduce cost, energy consumption, and carbon footprint. This paper explores the material science, processes, and business consideration associated with achieving these performance gains. It is concluded that a paradigm shift is required in order to fully exploit AM potential.
4,055 citations
TL;DR: In this article, the accuracies of the three measurement principles: Archimedes method, microscopic analysis of cross sections and X-ray scanning were investigated for additive manufactured parts using selective laser melting (SLM) or electron beam melting (EBM).
Abstract: Purpose – In the optimisation of processing parameters for additive manufactured parts using, e.g. selective laser melting (SLM) or electron beam melting, the measurement of the part densities is essential and of high interest. However, there is no common standard. Different institutes and system providers are using their own principles and guidelines. This study investigates the accuracies of the three measurement principles: Archimedes method, microscopic analysis of cross sections and X‐ray scanning.Design/methodology/approach – A total of 15 test samples on five density levels (densities between 90 and 99.5 per cent) were produced using the SLM process. The samples are analysed regarding the accuracy of the measurement principles and their reproducibility taking into account influencing parameters like the buoyancy of a sample in air (Archimedes method) or different magnifications of a cross section.Findings – The Archimedes method shows a very high accuracy (±0.08 per cent for high densities) and rep...
409 citations
TL;DR: The results of systematic studies carried out on two different powder materials used for additive manufacturing are presented, showing how virgin powder changes after being exposed to and recycled from one or more Direct Metal Laser Sintering (DMLS) additive manufacturing build cycles.
Abstract: Additive manufacturing (AM) techniques can produce complex, high-value metal parts, with potential applications as critical parts, such as those found in aerospace components. The production of AM parts with consistent and predictable properties requires input materials (e.g., metal powders) with known and repeatable characteristics, which in turn requires standardized measurement methods for powder properties. First, based on our previous work, we assess the applicability of current standardized methods for powder characterization for metal AM powders. Then we present the results of systematic studies carried out on two different powder materials used for additive manufacturing: stainless steel and cobalt-chrome. The characterization of these powders is important in NIST efforts to develop appropriate measurements and standards for additive materials and to document the property of powders used in a NIST-led additive manufacturing material round robin. An extensive array of characterization techniques was applied to these two powders, in both virgin and recycled states. The physical techniques included laser diffraction particle size analysis, X-ray computed tomography for size and shape analysis, and optical and scanning electron microscopy. Techniques sensitive to structure and chemistry, including X-ray diffraction, energy dispersive analytical X-ray analysis using the X-rays generated during scanning electron microscopy, and X-Ray photoelectron spectroscopy were also employed. The results of these analyses show how virgin powder changes after being exposed to and recycled from one or more Direct Metal Laser Sintering (DMLS) additive manufacturing build cycles. In addition, these findings can give insight into the actual additive manufacturing process.
381 citations
TL;DR: In this paper, the authors examined 17-4 PH stainless steel powders produced by atomization in either argon or nitrogen atmospheres and correspondingly fabricated by selective laser melting (SLM) in either a nitrogen or argon atmosphere.
Abstract: Objective This research examines 17-4 PH stainless steel powders produced by atomization in either argon or nitrogen atmospheres (producing martensitic (α-Fe) or mostly austenitic (γ-Fe) phase powders, respectively) and correspondingly fabricated by selective laser melting (SLM) in either a nitrogen or argon atmosphere. Methods Pre-alloyed 17-4 stainless steel powders prepared by atomization in either argon or nitrogen atmospheres were fabricated by SLM. The initial powder microstructures and phase structures were examined by light (optical) microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction (XRD). Prototypes fabricated by SLM were similarly characterized, and in addition transmission electron microscopy (TEM) characterization was also performed. Results Martensitic powder fabricated by SLM in nitrogen gas produced a martensitic product while pre-alloyed austenitic powder produced a primarily austenitic product. In contrast, both powders produced martensitic products when fabricated by SLM in argon gas. This unusual behavior occurred because of the rapid cooling affected by nitrogen versus argon cover gas as a consequence of a 40% greater thermal conductivity of nitrogen gas versus argon gas. SLM fabricated martensitic products exhibited HRC 30 in contrast to HRC 43 when aged at 482°C for 1 hour. Austenitic products did not exhibit age-hardening. Conclusions Using an argon cover gas, SLM-fabricated products are martensitic (and magnetic) with either an austenitic or martensitic pre-alloyed 17-4 PH stainless steel powder. Using a nitrogen cover gas, the product phase is the same as the precursor powder phase (austenitic or martensitic).
306 citations