Study of the production of biodiesel by enzymatic and chemical processes from used cooking oil
Juan Camilo Acevedo-Páez,Nestor Andres Urbina-Suarez,Astrid Zuleima Acevedo-Rodríguez,Luis Carlos Becerra-Orozco +3 more
- Vol. 7, Iss: 2, pp 20-26
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TLDR
In this paper, chemical and enzymatic processes from used cooking oil (UCO) were analyzed by evaluating the quality and yield of the product obtained in each method. And the highest yield obtained was from the chemical transesterification under the conditions of 60 °C, 1% KOH and 70 min with a conversion percentage of 96.15% and an acid number of 1.33 mmKOH/g.Abstract:
The biodiesel production was analyzed by chemical and enzymatic processes, from used cooking oil (UCO), evaluating the quality and yield of the product obtained in each method. For the chemical process, an acid esterification followed by a basic transesterification was developed, (reaction temperature: 60 °C, oil:methanol 1:6 molar ratio, concentration of KOH catalyst: 1% w/w reaction times: 55 and 70 min); and enzymatic transesterification (temperature: 38 °C, oil:methanol 1:3 molar ratio, enzyme concentration lipase XX 25 split liquid: 5%, reaction times: 3 and 6 hours). Physicochemical properties (i.e. density, kinematic viscosity, moisture content, fatty acid profile, percentage of acidity, peroxides index and saponification) of the raw material were determined. Results showed the presence of oleic acid (42.45%) and palmitic acid (33.52%). The highest yield obtained was from the chemical transesterification under the conditions of 60 °C, 1% KOH and 70 min with a conversion percentage of 96.15% and an acid number of 1.33 mmKOH/g, compared to the enzymatic transesterification which registered a high acid number of 6.91 mmKOH/g and conversion percentage of 48.81% under the conditions of 38 °C, 5% of enzyme lipase and 3 hours.read more
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Journal ArticleDOI
Enzymatic Transesterification of Waste Frying Oil from Local Restaurants in East Colombia Using a Combined Lipase System
Mary Angélica Ferreira Vela,Juan Camilo Acevedo-Páez,Nestor Andres Urbina-Suarez,Yeily Adriana Rangel Basto,Ángel Darío González-Delgado +4 more
TL;DR: In this article, the authors implemented an enzymatic transesterification process to obtain biodiesel from waste frying oil (WFO), which was performed by varying reaction times (8 h, 12 h and 16 h), enzyme concentrations of lipase XX 25 split (14, 16% and 18%), pH of reaction media (6, 7 and 8) and reaction temperature (35, 38 and 40 °C) with a fixed alcohol-oil molar ratio of 3:1.
References
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Journal ArticleDOI
Environmental, economic, and energetic costs and benefits of biodiesel and ethanol biofuels
TL;DR: Transportation biofuels such as synfuel hydrocarbons or cellulosic ethanol, if produced from low-input biomass grown on agriculturally marginal land or from waste biomass, could provide much greater supplies and environmental benefits than food-basedBiofuels.
Journal ArticleDOI
Biodiesel production from waste cooking oils
Anh N. Phan,Tan M. Phan +1 more
TL;DR: In this article, the effects of methanol/waste cooking oils ratio, potassium hydroxide concentration and temperature on the biodiesel conversion were investigated, and the results showed that the resulting biodiesel experienced a higher but much narrower boiling range than conventional diesel.
Journal ArticleDOI
Overview of the production of biodiesel from Waste cooking oil
TL;DR: The most common process in the production of biodiesel is transesterification, and using a methanol-ethanol mixture will combine the advantages of both alcohols in biodiesel production.
Journal ArticleDOI
Technical aspects of production and analysis of biodiesel from used cooking oil—A review
TL;DR: In this paper, the analytical methods for high quality biodiesel fuel from used cooking oil like GC, TLC, HPLC, GPC and TGA have also been summarized in this paper.
Journal ArticleDOI
Comparison of purification methods for biodiesel
M. Berrios,R.L. Skelton +1 more
TL;DR: It has been found that it is necessary a previous methanol removal to avoid the saturation of the adsorbents in post transesterification purification.
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