Subcritical water extraction of phenolic compounds from potato peel
TL;DR: In this article, the authors investigated the extraction of eight phenolic compounds (Gallic acid, GAC, Chlorogenic acid, CGA; Caffeic acid CFA; Protocatechuic acid, PCA; Syringic acid SGA; p-hydroxyl benzoic acid PBA; Ferulic acid, FRA and Coumaric acids, CMA) from potato peel using subcritical water.
About: This article is published in Food Research International.The article was published on 2011-10-01. It has received 251 citations till now. The article focuses on the topics: Phenolic acid & Syringic acid.
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TL;DR: This review addresses the application of different methodologies utilized in the analysis of phenolic compounds in plant-based products, including recent technical developments in the quantification of phenolics.
Abstract: Phenolic compounds are well-known phytochemicals found in all plants. They consist of simple phenols, benzoic and cinnamic acid, coumarins, tannins, lignins, lignans and flavonoids. Substantial developments in research focused on the extraction, identification and quantification of phenolic compounds as medicinal and/or dietary molecules have occurred over the last 25 years. Organic solvent extraction is the main method used to extract phenolics. Chemical procedures are used to detect the presence of total phenolics, while spectrophotometric and chromatographic techniques are utilized to identify and quantify individual phenolic compounds. This review addresses the application of different methodologies utilized in the analysis of phenolic compounds in plant-based products, including recent technical developments in the quantification of phenolics.
919 citations
Cites background from "Subcritical water extraction of phe..."
...Cinnamon bark Phenolic compounds 150,200 60 60 -[146] Potato peel Phenolic compounds 100–240 30–120 60 -[147] Rice bran Phenolic compounds 125–200 5 20 2....
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TL;DR: In this paper the main classes of antioxidants are presented: vitamins, carotenoids and polyphenols.
401 citations
Cites background from "Subcritical water extraction of phe..."
...…for the extraction of phenolic compounds from pomegranate (Punicagranatum L.) seed residues (He et al. 2012), anthocyanins and other phenolic compounds from dried red grape skin (Ju & Howard, 2005) and potato peel (Singh & Saldana, 2011) and flavanones from citrus peel (Cheigh, Chung & Chung 2012)....
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TL;DR: In this article, the authors provide a thorough background to the fundamentals and applications of hot water extraction for the analysis of bioactive compounds, including equipment, method optimization, applications, coupling, and future prospects.
Abstract: The purpose of this review is to give the reader a thorough background to the fundamentals and applications of pressurized hot water extraction (PHWE) for the analysis of bioactive compounds. We summarize the field in the period 2009-14, and include fundamentals of water as a solvent: equipment; method optimization; applications; coupling; and, future prospects. We highlight that solvent properties of water are tunable by changing the temperature, particularly self-ionization, dielectric constant, viscosity, diffusivity, density and surface tension. Furthermore, important aspects to consider are the risk of degradation of the analytes and other potential reactions, such as hydrolysis, caramelization and Maillard reactions that may lead to erroneous results. For the extraction of bioactive compounds, we report PHWE methods based on using water of 80-175 degrees C and short extraction times. In conclusion, PHWE provides advantages over conventional extraction methods, such as being "greener", faster and more efficient. (C) 2015 The Authors. Published by Elsevier B.V. (Less)
396 citations
TL;DR: Methods for proper identification of plant material, problems of post-harvest changes in plantmaterial, extraction methods including application of ionic liquids, de-replication procedures during natural product isolation are discussed by the review.
295 citations
TL;DR: In this article, the authors focus on the extraction of bioactive compounds from food byproducts of plant origin by a number of novel methods, including supercritical CO2 extraction and pressurised liquid extraction.
275 citations
References
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Journal Article•
TL;DR: In this paper, the use of Folin-Ciocalteu reagent rather than the FolinDenis reagent, gallic acid as a reference standard, and a more reproducible time-temperature color development period was investigated.
Abstract: Several details of the assay of total phenolic substances have been investigated and an improved procedure developed. The improvements include the use of Folin-Ciocalteu reagent rather than the Folin-Denis reagent, gallic acid as a reference standard, and a more reproducible time-temperature color development period. The values obtained are less subject to variation and interference from several nonphenols, yet are directly comparable to the "tannin" values obtained by the previously standard method.
18,629 citations
Book•
30 Apr 1988
TL;DR: In this article, the authors present an overview of the second law of thermodynamics and its application in the context of a gas turbine power plant and evaluate the entropy of the system.
Abstract: 1 Getting Started: Introductory Concepts and Definitions. 1.1 Using Thermodynamics. 1.2 Defining Systems. 1.3 Describing Systems and Their Behavior. 1.4 Measuring Mass, Length, Time, and Force. 1.5 Specific Volume. 1.6 Pressure. 1.7 Temperature. Chapter Summary and Study Guide. 2 Energy and the First Law of Thermodynamics. 2.1 Reviewing Mechanical Concepts of Energy. 2.2 Broadening Our Understanding of Work. 2.3 Broadening Our Understanding of Energy. 2.4 Energy Transfer by Heat. 2.5 Energy Accounting: Energy Balance for Closed Systems. 2.6 Energy Analysis of Cycles. Chapter Summary and Study Guide. 3 Evaluating Properties. 3.1 Getting Started. Evaluating Properties: General Considerations. 3.2 p-v-T Relation. 3.3 Studying Phase Change. 3.4 Retrieving Thermodynamic Properties. 3.5 Evaluating Pressure, Specific Volume, and Temperature. 3.6 Evaluating Specific Internal Energy and Enthalpy. 3.7 Evaluating Properties Using Computer Software. 3.8 Applying the Energy Balance Using Property Tables and Software. Chapter Summary and Study Guide. 4 Control Volume Analysis Using Energy. 4.1 Conservation of Mass for a Control Volume. 4.2 Forms of the Mass Rate Balance. 4.3 Applications of the Mass Rate Balance. 4.4 Conservation of Energy for a Control Volume. Chapter Summary and Study Guide. 5 The Second Law of Thermodynamics. 5.1 Introducing the Second Law. 5.2 Statements of the Second Law. 5.3 Identifying Irreversibilities. 5.4 Interpreting the Kelvin-Planck Statement. 5.5 Applying the Second Law to Thermodynamic Cycles. 5.6 Second Law Aspects of Power Cycles Interacting with Two Reservoirs. Chapter Summary and Study Guide. 6 Using Entropy. 6.1 Entropy-A System Property. 6.2 Retrieving Entropy Data. 6.3 Introducing the T dS Equations. 6.4 Entropy Change of an Incompressible Substance. 6.5 Entropy Change of an Ideal Gas. 6.6 Entropy Change in Internally Reversible Processes of Closed Systems. 6.7 Entropy Balance for Closed Systems. 6.8 Directionality of Processes. 6.9 Entropy Rate Balance for Control Volumes. Steady-State Flow Processes. Chapter Summary and Study Guide. 7 Exergy Analysis. 7.1 Introducing Exergy. 7.2 Conceptualizing Exergy. 7.3 Exergy of a System. 7.4 Closed System Exergy Balance. 7.5 Exergy Rate Balance for Control Volumes at Steady State. 7.6 Exergetic (Second Law) Efficiency. 7.7 Thermoeconomics. Chapter Summary and Study Guide. 8 Vapor Power Systems. 8.1 Modeling Vapor Power Systems. 8.2 Analyzing Vapor Power Systems-Rankine Cycle. 8.3 Improving Performance-Superheat and Reheat. 8.4 Improving Performance-Regenerative Vapor Power Cycle. 8.5 Other Vapor Cycle Aspects. 8.6 Case Study: Exergy Accounting of a Vapor Power Plant. Chapter Summary and Study Guide. 9 Gas Power Systems. Internal Combustion Engines. 9.1 Introducing Engine Terminology. 9.2 Air-Standard Otto Cycle. 9.3 Air-Standard Diesel Cycle. 9.4 Air-Standard Dual Cycle. Gas Turbine Power Plants. 9.5 Modeling Gas Turbine Power Plants. 9.6 Air-Standard Brayton Cycle. 9.7 Regenerative Gas Turbines. 9.8 Regenerative Gas Turbines with Reheat and Intercooling. 9.9 Gas Turbines for Aircraft Propulsion. 9.10 Combined Gas Turbine-Vapor Power Cycle. Chapter Summary and Study Guide. 10 Refrigeration and Heat Pump Systems. 10.1 Vapor Refrigeration Systems. 10.2 Analyzing Vapor-Compression Refrigeration Systems. 10.3 Refrigerant Properties. 10.4 Cascade and Multistage Vapor-Compression Systems. 10.5 Absorption Refrigeration. 10.6 Heat Pump Systems. 10.7 Gas Refrigeration Systems. Chapter Summary and Study Guide. 11 Thermodynamic Relations. 11.1 Using Equations of State. 11.2 Important Mathematical Relations. 11.3 Developing Property Relations. 11.4 Evaluating Changes in Entropy, Internal Energy, and Enthalpy. 11.5 Other Thermodynamic Relations. 11.6 Constructing Tables of Thermodynamic Properties. Charts for Enthalpy and Entropy. 11.8 p-v-T Relations for Gas Mixtures. 11.9 Analyzing Multicomponent Systems. Chapter Summary and Study Guide. 12 Ideal Gas Mixture and Psychrometric Applications. Ideal Gas Mixtures: General Considerations. 12.1 Describing Mixture Composition. 12.2 Relating p, V, and T for Ideal Gas Mixtures. 12.3 Evaluating U, H, S, and Specific Heats. 12.4 Analyzing Systems Involving Mixtures. Psychrometric Applications. 12.5 Introducing Psychrometric Principles. 12.6 Psychrometers: Measuring the Wet-Bulb and Dry-Bulb Temperatures. 12.7 Psychrometric Charts. 12.8 Analyzing Air-Conditioning Processes. 12.9 Cooling Towers. Chapter Summary and Study Guide. 13 Reacting Mixtures and Combustion. Combustion Fundamentals. 13.1 Introducing Combustion. 13.2 Conservation of Energy-Reacting Systems. 13.3 Determining the Adiabatic Flame Temperature. 13.4 Fuel Cells. 13.5 Absolute Entropy and the Third Law of Thermodynamics. Chemical Exergy. 13.6 Introducing Chemical Exergy. 13.7 Standard Chemical Exergy. 13.8 Exergy Summary. 13.9 Exergetic (Second Law) Efficiencies of Reacting Systems. Chapter Summary and Study Guide. 14 Chemical and Phase Equilibrium. Equilibrium Fundamentals. 14.1 Introducing Equilibrium Criteria. Chemical Equilibrium. 14.2 Equation of Reaction Equilibrium. 14.3 Calculating Equilibrium Compositions. 14.4 Further Examples of the Use of the Equilibrium Constant. Phase Equilibrium. 14.5 Equilibrium Between Two Phases of a Pure Substance. 14.6 Equilibrium of Multicomponent, Multiphase Systems. Chapter Summary and Study Guide. Appendix Tables, Figures, and Charts. Index to Tables in SI Units. Index to Tables in English Units. Index to Figures and Charts. Index. Answers to Selected Problems: Visit the student.
2,775 citations
Book•
05 Dec 1995TL;DR: Phenolics in Food and Nutraceuticals as mentioned in this paper is the first single-source compendium of essential information concerning food phenolics, which reports the classification and nomenclature of phenolics and their occurrence in food and nutraceuticals.
Abstract: Phenolics in Food and Nutraceuticals is the first single-source compendium of essential information concerning food phenolics. This unique book reports the classification and nomenclature of phenolics, their occurrence in food and nutraceuticals, chemistry and applications, and nutritional and health effects. In addition, it describes antioxidant activity of phenolics in food and nutraceuticals as well as methods for analysis and quantification. Each chapter concludes with an extensive bibliography for further reading. Food scientists, nutritionists, chemists, biochemists, and health professionals will find this book valuable.
1,252 citations
TL;DR: In this article, the authors provide an updated overview on the principal applications of two clean processes, supercritical fluid extraction and subcritical water extraction, used to isolate natural products from different raw materials, such as plants, food by-products, algae and microalgae.
1,090 citations
TL;DR: A high-performance liquid chromatographic (HPLC) method with diode-array detection (DAD) was used to identify and quantify free and total phenolic acids in plant foods, and the methods developed were effective for the determination of phenolic acid in plant Foods.
Abstract: A high-performance liquid chromatographic (HPLC) method with diode-array detection (DAD) was used to identify and quantify free and total phenolic acids (m-hydroxybenzoic acid, p-hydroxybenzoic acid, protocatechuic acid, gallic acid, vanillic acid, syringic acid, o-coumaric acid, m-coumaric acid, p-coumaric acid, caffeic acid, ferulic acid, sinapic acid, chlorogenic acid, and ellagic acid) in plant foods. Free phenolic acids were extracted with a mixture of methanol and 10% acetic acid. Bound phenolic acids were liberated using first alkaline and then acid hydrolysis followed by extraction with diethyl ether/ethyl acetate (1:1). All fractions were quantified separately by HPLC. After HPLC quantification, results of alkali and acid hydrolysates were calculated to represent total phenolic acids. Ellagic acid was quantified separately after long (20 h) acid hydrolysis. The methods developed were effective for the determination of phenolic acids in plant foods. DAD response was linear for all phenolic acids within the ranges evaluated, with correlation coefficients exceeding 0.999. Coefficients of variation for 4-8 sample replicates were consistently below 10%. Recovery tests of phenolic acids were performed for every hydrolysis condition using several samples. Recoveries were generally good (mean >90%) with the exceptions of gallic acid and, in some cases, caffeic acid samples.
398 citations