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Submicron X-ray diffraction and its applications to problems in materials and environmental science.

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TLDR
The availability of high brilliance third generation synchrotron sources together with progress in achromatic focusing optics allows us to add submicron spatial resolution to the conventional century-old x-ray diffraction technique as discussed by the authors.
Abstract
The availability of high brilliance third generation synchrotron sources together with progress in achromatic focusing optics allows us to add submicron spatial resolution to the conventional century-old x-ray diffraction technique. The new capabilities include the possibility to map in situ, grain orientations, crystalline phase distribution, and full strain/stress tensors at a very local level, by combining white and monochromatic x-ray microbeam diffraction. This is particularly relevant for high technology industry where the understanding of material properties at a microstructural level becomes increasingly important. After describing the latest advances in the submicron x-ray diffraction techniques at the Advanced Light Source, we will give some examples of its application in material science for the measurement of strain/stress in metallic thin films and interconnects. Its use in the field of environmental science will also be discussed.

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References
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Quantitative zn speciation in smelter-contaminated soils by exafs spectroscopy

TL;DR: In this article, a combination of X-ray diffraction, texture goniomom- etry, and powder and polarized extended Xray absorption fine structure (EXAFS) spectra were used to investigate quantitatively the speciation of Zn in soils contaminated by three smelters.

Materials reliability issues in microelectronics

TL;DR: The proceedings of a MRS Symposium on Materials Reliability in microelectronics were discussed in this article, including electromigration, stress effects on reliability, stress and packaging, metallization, device, oxide and dielectric reliability; new investigative techniques; and corrosion.
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Structure of H-exchanged hexagonal birnessite and its mechanism of formation from Na-rich monoclinic buserite at low pH.

TL;DR: The structural transformation of high pH Na-rich buserite (NaBu) to H-exchanged hexagonal birnessite (HBi) at low pH was studied by simulation of experimental X-ray diffraction patterns.
Journal ArticleDOI

New avenues in x-ray microbeam experiments

TL;DR: The high brilliance of third-generation synchrotron radiation sources allows new applications in x-ray microdiffraction and micro-small-angle scattering as discussed by the authors, and beam sizes down to about one µm are routinely used and sub-µm beam sizes are becoming available.
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