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Showing papers on "Aluminium alloy published in 1999"


Journal ArticleDOI
01 Apr 1999-Nature
TL;DR: In this article, the authors present observations of low-temperature superplasticity in nanocrystalline nickel, 1420-Al, and Ni3Al, which is the lowest normalized super-plastic temperature reported for any crystalline material.
Abstract: Superplasticity — the ability of a material to sustain large plastic deformation — has been demonstrated in a number of metallic, intermetallic and ceramic systems. Conditions considered necessary for superplasticity1 are a stable fine-grained microstructure and a temperature higher than 0.5 T m (where T m is the melting point of the matrix). Superplastic behaviour is of industrial interest, as it forms the basis of a fabrication method that canbeused to produce components having complex shapes from materials that are hard to machine, such as metal matrix composites and intermetallics. Use of superplastic forming may become even more widespread if lower deformation temperatures can be attained. Here we present observations of low-temperature superplasticity in nanocrystalline nickel, a nanocrystalline aluminium alloy (1420-Al), and nanocrystalline nickel aluminide (Ni3Al). The nanocrystalline nickel was found to be superplastic ata temperature 470 °C below that previously attained2: this corresponds to 0.36T m, the lowest normalized superplastic temperature reported for any crystalline material. The nanocrystalline Ni3Al was found to be superplastic at a temperature 450 °C below the superplastic temperature in the microcrystalline regime3.

553 citations


Journal ArticleDOI
TL;DR: A detailed study of the effects of grit blasting with different alumina grits on the surface characteristics of mild steel and aluminium alloy substractes is reported in this article, where the results indicate that the changes in joint properties associated with roughened surfaces cannot be explained simply by the increased roughness characteristics, such as mechanical keying and increased effective bond area.

278 citations


Journal ArticleDOI
TL;DR: In this article, a plasma electrolysis technique known as micro-arc discharge oxidation (MDO) was investigated; thick and hard oxide ceramic layers were fabricated on BS Al-6082 aluminium alloy by this method.
Abstract: Weight-saving materials are becoming increasingly important, especially in the automotive and aerospace industries. Design engineers would thus like to make more extensive use of light metals such as aluminium, titanium, magnesium and their alloys; however, these materials tend to have poor wear resistance. Previous treatments and coatings applied to aluminium alloys, for example by traditional processes such as hard anodising and thermal spraying, have suffered from the low load support from the underlying material and/or insufficient adhesion, which reduces their durability. Also, although TiN-, CrN- or DLC-coated aluminium alloys (using various PVD methods) can achieve a high surface hardness, in practice they often exhibit poor performance under mechanical loading, since the coatings are usually too thin to protect the substrate from the contact conditions. In the work reported here, a plasma electrolysis technique known as micro-arc discharge oxidation (MDO) was investigated; thick and hard oxide ceramic layers were fabricated on BS Al-6082 aluminium alloy by this method. The phase composition and microstructure of the MDO coatings were investigated by XRD, SEM and EDX analyses. A number of adhesion and tribological sliding and impact wear tests were also performed. It was found that Al–Si–O coatings with a hardness of up to 2400 HV and with excellent wear resistance and load support could be formed. The thickness of the coatings significantly influenced the mechanical properties. In terms of tribological performance, the thicker coatings performed best in sliding, scratch and impact tests whilst thin coatings were also surprisingly effective in both impact and low-load sliding. Coatings of intermediate thickness provided relatively poor performance in all tribological tests.

276 citations


Journal ArticleDOI
TL;DR: The tensile and compressive stress-strain behavior of closed cell aluminium alloy foams (trade name "Alulight") has been measured and interpreted in terms of its microstructure as discussed by the authors.

227 citations


Journal ArticleDOI
TL;DR: In this article, an experimental investigation was carried out to study the behavior of square aluminium extrusions filled with aluminium foam under quasi-static loading conditions, and simple relations between dimensionless numbers governing the influence of the foam on the characteristics of the crush problem were identified.

196 citations


Journal ArticleDOI
TL;DR: In this paper, the effects of several types of geometric imperfections, such as plateau borders, cell edge misalignments, fractured cell edges, missing cells, inclusions and cell size variations, on the thermal and structural fire retardance of cellular metallic foams are identified.

196 citations


Journal ArticleDOI
TL;DR: In this article, electron beam welding was performed on three different aluminium alloys, namely alloys 2024, 5005, and 6061, to establish the local microstructure-property relationships that would satisfy the service requirements for an electron beam welded aluminium alloy component with weld zone strength undermatching.
Abstract: Electron beam (EB) welding was performed on three different aluminium alloys, namely alloys 2024, 5005, and 6061 (plate thickness 5 mm except alloy 5005 which was 3 mm in thickness), to establish the local microstructure–property relationships that would satisfy the service requirements for an electron beam welded aluminium alloy component with weld zone strength undermatching. Microstructural characterisation of the weld metals was carried out by optical and scanning electron microscopy. A very low level of porosity was observed in all EB welds owing to surface cleaning before welding and the vacuum environment of the EB welding process. Extensive microhardness measurements were also conducted in the weld regions of the joints. Global tensile properties and fracture toughness properties (in terms of crack tip opening displacement, CTOD) of the EB joints were determined at room temperature. The effects of strength mismatch and local microstructure on fracture toughness of the EB joints are discuss...

120 citations


Journal ArticleDOI
TL;DR: In this paper, the process of friction welding between the aluminium alloy and the stainless steel is proposed to evolve as follows: welding progresses from the outer to the inner region, an unbonded region is retained at the centre of the weld interface with shorter friction time; longer friction time causes the formation of an intermetallic reaction layer at the weld interfaces; and the reaction layer grows as the friction time increases.
Abstract: Type 5052 aluminium alloy was joined to type 304 austenitic stainless steel via a continuous drive friction welding process. The joint strength increased, and then decreased after reaching a maximum value, with increasing friction time. Joint strength depended on the size and shape of the tensile testpiece. Friction weldability could be estimated by electrical resistmetry. The process of friction welding between the aluminium alloy and the stainless steel is proposed to evolve as follows: welding progresses from the outer to the inner region; an unbonded region is retained at the centre of the weld interface with shorter friction time; longer friction time causes the formation of an intermetallic reaction layer at the weld interface; and the reaction layer grows as the friction time increases. When the thickness of the reaction layer increased above a critical value, the joint was brittle and fractured at the weld interface. The joint was sound when there was no unbonded region and a thin reaction...

114 citations


Journal ArticleDOI
TL;DR: A European consortium is evaluating materials for the construction of a new supersonic transport aircraft that may replace Concorde as mentioned in this paper, and current designs propose to use an aluminium alloy for the fusela.
Abstract: A European consortium is evaluating materials for the construction of a new supersonic transport aircraft that may replace Concorde. Current designs propose to use an aluminium alloy for the fusela...

101 citations


Journal ArticleDOI
TL;DR: In this article, it is proposed that water vapor causes stress corrosion cracking at the Al2O3-alloy interface during cyclic oxidation, which increases the degradation rate by a factor of 2.
Abstract: Cyclic oxidation tests have been performed at 1100 °C in wet and dry air on a number of alloys and coatings that form α-Al2O3 scales upon exposure to oxidizing conditions. The alloys that were investigated included PWA 1480, PWA 1484, CMSX 4, diffusion aluminide coatings on PWA 1480 and PWA 1484, and Co-24Cr-10.5Al-0.3Y. In cases where some cracking and spalling of the alumina scales occurred in dry air, the presence of water vapor caused the degradation rate to be increased by a factor of 2. When no cracking or spalling of the alumina occurred in dry air, as was the case for low sulfur alloys, water vapor had no effect on the oxidation behavior. It is proposed that water vapor causes stress corrosion cracking at the Al2O3-alloy interface during cyclic oxidation.

86 citations


Journal ArticleDOI
TL;DR: In this paper, a comparison has been made between two samples which exhibit different propensities for roughening and a detailed microstructural characterisation of these samples has been performed in order to explain the differences.
Abstract: The development of surface roughening during uniaxial tensile deformation, with particular attention to the development of parallel ridges and valleys (ribbed profile), has been investigated for a commercial aluminium alloy. A comparison has been made between two samples which exhibit different propensities for roughening and a detailed microstructural characterisation of these samples has been performed in order to explain the differences. Microstructural characterisation techniques included polarised light microscopy, bulk texture and microtexture. In addition, yield properties were calculated from the microtexture data using polycrystal plasticity analysis. The results show that the differences in the roughening behaviour can be attributed to spatial differences in texture at the specimen surface whereby R-component colonies in a cube matrix produce differential straining, which eventually leads to strain localisation through the specimen thickness to produce a ribbed profile.

Journal ArticleDOI
01 Apr 1999-Wear
TL;DR: In this article, a series of reciprocation sliding wear experiments have been carried out under lubricated conditions and the results showed that the micro-arc oxidised (MAO) process provided the greatest wear resistance of the surface treatments investigated.


Journal ArticleDOI
TL;DR: In this article, the effect of scandium and titanium-boron (Tibor) additions on the solidification behavior of castings and welds of aluminium alloy 7108 has been investigated.
Abstract: The effect of scandium and titanium–boron (Tibor) additions on the solidification behaviour of castings and welds of aluminium alloy 7108 has been investigated. A circular patch test was adopted to evaluate the effects of these elements on the hot cracking suscepti bility of welds made on cast coupons treated with different grain refiner additions. It was observed that grain size, as well as cracking susceptibility, decreased with increasing amounts of scandium and that hot cracking was completely eliminated at scandium additions above 0·25 wt-%. A more pronounced grain refining effect in welds was observed with Tibor and, in addition, no hot cracking was observed with Tibor additions as low as 0·02 wt-%Ti (0·004 wt-%B). Castings, however, were more effectively grain refined with scandium, achieving a finer grain size than with Tibor.

Journal ArticleDOI
TL;DR: Of the examined representative step-wedges, all but the aluminium--4% copper material were satisfactory and gave results comparable with wedges of high purity, so limits should be revised for composition of aluminium radiopacity step- wedges or test blocks to a more realistic level of purity.

Journal ArticleDOI
TL;DR: In this paper, three local stress approaches, the stress averaging approach, the highly stressed volume approach and the crack propagation approach, were applied to the fatigue assessment of welded joints in AlMg 4.5 Mn aluminium alloy (AA 5083) with different stress concentrations and plate thicknesses.

Journal ArticleDOI
TL;DR: In this paper, the effect of various parameters on the surface roughness of an aluminium alloy burnished with a spherical surfaced polycrystalline diamond tool is studied experimentally with a theoretical analysis.
Abstract: The effect of various parameters on the surface roughness of an aluminium alloy burnished with a spherical surfaced polycrystalline diamond tool are studied experimentally with a theoretical analysis. Problems in selecting the optimum burnishing parameters and some burnishing mechanisms are discussed. With suitable parameters employed, the new no-chip finishing process developed can eliminate or reduce the cutting marks left on the workpiece surface by diamond cutting tools, with its surface roughness reduced to Ra=0.026 μm from the original 0.5 μm.

Journal ArticleDOI
TL;DR: In this article, a cast Al-7Si-Mg alloy with various casting defects, particularly surface or subsurface defects, was studied under four-point bending to investigate the stress-life relationship and fatigue fracture characteristics in order to understand crack initiation and growth behaviour in conjunction with the examination of surface roughness and porosity surface hollows were found to control crack initiation of as-cast specimens.
Abstract: Fatigue performance has been studied in a cast Al-7Si-Mg alloy with regard to various casting defects, particularly surface or subsurface defects Fatigue tests were carried out under four-point bending to investigate the stress-life relationship and fatigue fracture characteristics in order to understand crack initiation and growth behaviour in conjunction with the examination of surface roughness and porosity Surface hollows were found to control crack initiation of as-cast specimens The fracture surfaces of polished specimens revealed that surface or subsurface shrinkage pores replaced the hollows to act as crack initiators when the rough surface was removed The importance of oxide films in crack initiation was also demonstrated The effects of all these casting defects on fatigue life are discussed

Journal ArticleDOI
TL;DR: In this article, a single-phase model for semi-solid metal alloys is presented, which is based on the experimental data of a tin-lead alloy (Sn-15%Pb) with a similar microstructure to aluminium alloys.
Abstract: Semi-solid metal alloys, as used in thixoforming, have a special microstructure of globular grains suspended in a liquid metal matrix. The complex rheological properties are strongly influenced by the local solid fraction, particle shape, particle size and state of agglomeration. There is a high demand for models and software tools allowing the simulation of semi-solid casting processes. The material under investigation is a tin-lead alloy (Sn-15%Pb) which exhibits a similar microstructure to aluminium alloys. The experiments were performed with a concentric cylinder rheometer of the Searle type. Initially, the liquid alloy is cooled down to the semi-solid range under constant shearing and then kept under isothermal conditions for further experimentation. Based on the experimental data, a single-phase model has been derived where the semi-solid alloy is regarded as a homogeneous material with thixotropic properties and the microstructure is characterised by a structural parameter. The model consists of two parts: the equation of state, including a finite yield stress, and a rate equation for the structural parameter. The model equations are employed in numerical software and used for the simulation of characteristic filling cases and the comparison with the conventional filling.

Journal ArticleDOI
TL;DR: In this paper, the fracture behavior of closed cell aluminium-based foams (trade-name “Alulight”) is characterized for the compositions Al−Mg1−Si0.6 and Al-Mg 1−Si10 (wt%), and for a relative density in the range 0.1−0.4.

Journal ArticleDOI
TL;DR: In this article, the mechanical properties of a typical sintered aluminium alloy have been improved by the simultaneous use of trace additions of Sn, high sintering temperatures and modified heat treatments.
Abstract: The mechanical properties of a typical sintered aluminium alloy (Al-4.4Cu-0.8Si-0.5Mg) have been improved by the simultaneous use of trace additions of Sn, high sintering temperatures and modified heat treatments. Tin increases densification, but the Sn concentration is limited to less than or equal to 0.1wt% because incipient melting occurs during solution treatment at higher Sn levels. A sintering temperature of 620 degrees C increases the liquid volume over that formed at the conventional 590 degrees C sintering temperature. However, the higher sintering temperature results in the formation of an embrittling phase which can be eliminated if solution treatment is incorporated into the sintering cycle (a modified TS heat treatment). These conditions produce a tensile strength of 375 MPa, an increase of nearly 20% over the unmodified alloy. (C) 1999 Elsevier Science S.A. All rights reserved.

Journal ArticleDOI
TL;DR: The influence of strontium on the silicon modification and aluminium-copper eutectic microstructures in the 319 aluminium alloy was examined in this article, where the levels considered were between 8 and 96 p...
Abstract: The influence of strontium on the silicon modification and aluminium-copper eutectic microstructures in the 319 aluminium alloy was examined. The strontium levels considered were between 8 and 96 p...

Journal ArticleDOI
TL;DR: In this paper, the morphology and growth kinetics of α-Al2O3 scales formed during high-temperature oxidation of the Fe-Cr-Al and Fe-cr-Al-Y alloys were studied.
Abstract: The morphology and growth kinetics of protectiveα-Al2O3 scales formed duringhigh-temperature oxidation of the Fe-Cr-Al andFe-Cr-Al-Y alloys were studied. Scanning electronmicroscopy observations were focused on the oxidewrinkling phenomenonand formation of interfacial cavities in the course ofoxidation of the yttrium-free alloy. In this paper,emphasis is also placed on the effects of surface preparation and yttrium additions on the scaleand scalealloy interface structures. Several features ofalumina morphology, which have not received sufficientattention previously, are discussed in the context of existing models; some criticalissues are outlined.

Journal ArticleDOI
TL;DR: In this paper, an experimental investigation was undertaken to study the stability and ultimate strength of aluminium alloy outstands, and the experimental ultimate strength was compared with theoretical predictions, using the classical Stowell theory for plastic buckling in combination with the effective width concept, and with ultimate strength formulae recommended in the literature.
Abstract: An experimental investigation was undertaken to study the stability and ultimate strength of aluminium alloy outstands. In the tests, thin-walled cruciform aluminium extrusions were stressed into the post-buckling range in axial compression. The local buckling behaviour of the flanges of a cruciform section is the same as that of an outstand, i.e. a plate element which is free along one unloaded edge and simply supported along the other. Two tempers of alloy AA6082 with significantly different stress–strain curves were tested for five b / t ratios. The experimental ultimate strengths were compared with theoretical predictions, using the classical Stowell theory for plastic buckling in combination with the effective width concept, and with ultimate strength formulae recommended in the literature.

Patent
29 Oct 1999
TL;DR: In this article, a composite aluminium panel comprising two parallel plates and/or sheets secured to the peaks and troughs of a corrugated aluminium stiffener sheet between the parallel plates, is made from an aluminium alloy rolled sheet of composition.
Abstract: A composite aluminium panel comprising two parallel plates and/or sheets secured to the peaks and troughs of a corrugated aluminium stiffener sheet between the parallel plates and/or sheets, wherein the corrugated aluminium stiffener sheet is made from an aluminium alloy rolled sheet of composition (in weight percent): Mg 1.5-6.0, Mn 0.3-1.4, Zn 0.4-5.0, Fe up to 0.5, Si up to 0.5, Zr up to 0.30, optionally, one or more of (Cr 0.05-0.30, Ti 0.01-0.20, V 0.05-0.25, Ag 0.05-0.40, Cu up to 0.40), others up to 0.05 each, 0.15 total, Al balance, and having in an H-condition or in the O-condition a ratio of PS/UTS in the range of 0.4 to 0.9 and having good roll formability.

Journal ArticleDOI
TL;DR: In this paper, the internal-nitriding behavior of several modelalloys of the Ni-Cr-Al-Ti system in an oxygen-freenitrogen atmosphere at 800-1100°C was studied.
Abstract: The internal-nitriding behavior of several modelalloys of the Ni-Cr-Al-Ti system in an oxygen-freenitrogen atmosphere at 800-1100°C was studied.Thermogravimetry as well as various metallographic techniques (SEM and TEM) were used. It wasshown that both the nitrogen solubility and the nitrogendiffusion coefficient are strongly affected by the Crcontent of the Ni alloy. Hence, in Ni-Cr-Ti alloys a higher chromium content leads to an increaseddepth of the internal precipitation of TiN. Nitridationof the alloying element Cr takes place only at highconcentrations of Cr. In general, the nitridation rate was found to obey Wagner's parabolic ratelaw of internal oxidation. Changes in the parabolic rateconstant with alloy composition can be understood bymeans of thermodynamic calculations in combination with microstructural observations.

Journal ArticleDOI
TL;DR: In this article, the authors applied plane strain compression (PSC) testing to an Al-1% Mg alloy and found significant variations in internal microstructural parameters after different strain-rate histories to a strain of 1.0.

Patent
17 Dec 1999
TL;DR: In this paper, the authors proposed a method for manufacturing an aluminium-magnesium-lithium product, comprising the steps of subsequently: (a) providing an aluminium alloy consisting of (in weight %): Mg 3.0-6.0, Li 0.4-3.5, Fe up to 0.3, Si 0.02-0.5 selected from the group consisting of the group of (Sc 0.010-0, V 0.30, Nd 0.20, Cr 0.020-0., Y 0.005-
Abstract: Method for manufacturing of an aluminium-magnesium-lithium product, comprising the steps of subsequently: (a) providing an aluminium alloy consisting of (in weight %): Mg 3.0-6.0, Li 0.4-3.0, Zn up to 2.0, Mn up to 1.0, Ag up to 0.5, Fe up to 0.3, Si to 0.3, Cu up to 0.3, 0.02-0.5 selected from the group consisting of (Sc 0.010-0.40, Hf 0.010-0.25, Ti 0.010-0.25, V 0.010-0.30, Nd 0.010-0.20, Zr 0.020-0.25, Cr 0.020-0.25, Y 0.005-0.20, Be 0.0002-0.10), balance consisting essentially of aluminium and incidental elements and impurities; (b) casting the aluminium alloy into an ingot; (c) preheating the ingot; (d) hot rolling the preheated ingot to a hot worked intermediate product; (e) cold rolling the hot worked intermediate product to a rolled product in both the length and in the width direction with a total cold rolling reduction of at least 15 %; (f) solution heat treating the cold rolled product in the temperature range of 465 to 565°C for a soaking time in the range of 0.15 to 8 hours; (g) cooling the solution heat treated product from the solution heat treatment temperature to below 150°C with a cooling rate of at least 0.2°C/sec; (h) ageing the cooled product to provide a sheet or thin plate product having a minimum yield strength of 260 MPa or more and a minimum tensile strength of 400 MPa or more in at least the L- and LT-direction, a minimum yield strength of 230 MPa or more and a minimum tensile strength of 380 MPa or more in the 45° to the L-direction, and further having a minimum T-L fracture toughness KCO of 80 MPa.√ or more for 400 mm wide CCT-panels.

Journal ArticleDOI
TL;DR: In this article, the long-term environmental resistance of high niobium-containing Ti-22Al-25Nb, an alloy presently under consideration for titanium matrix fiber reinforced composites (TMCs), was evaluated.

Journal ArticleDOI
TL;DR: In this paper, a series of diffusion bonds were produced without using an interlayer at temperatures ranging from 950 to 1100°C with different pressure levels and holding times, and defect-free bonds were achieved for all the conditions studied.
Abstract: Intensive alloy development studies on intermetallic gamma (γ) based alloys in recent years has led to the development of several aerospace engine components using advanced γ-TiAl based alloys by ingot and powder metallurgical routes. These materials are of great interest to the aerospace industry owing to their very low density and good high temperature properties. Further application of this material will require the development of successful joining and cost effective fabrication methods. Joining of this intermetallic alloy by fusion joining processes, however, requires very careful process controlling, i.e. low cooling rates and very high preheat temperatures. On the other hand, solid state joining processes, particularly diffusion bonding, brazing, and friction welding, can readily be used to join this material. In the present work, successful application of solid state diffusion bonding to weld investment cast γ-TiAl alloys has been demonstrated. A series of diffusion bonds were produced without using an interlayer at temperatures ranging from 950 to 1100°C with different pressure levels and holding times. Bonds have been characterized using optical and scanning electron microscopy. Defect-free bonds were achieved for all the conditions studied. The bond qualities were assessed by shear testing at room temperature. Reasonable shear strength levels were obtained by bonding at 1000 and 1100°C for 3 h at pressures of 20 and 40 MPa, respectively. The bonds were also post bond heat treated at 1430°C for 30 min, which improved the bond quality in all cases.