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Calorimeter
About: Calorimeter is a research topic. Over the lifetime, 5878 publications have been published within this topic receiving 77157 citations.
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TL;DR: In this paper, a new method that fits the whole temperature response of a heat-pulse calorimeter for heat capacity is developed, which is capable of measuring heat capacity regardless if the sample is adiabatically or nonadiabatically isolated.
Abstract: A new method that fits the whole temperature response of a heat-pulse calorimeter for heat capacity is developed. Analyzing the thermal response of a heat-pulse calorimeter on a model that was used by the relaxation method, the authors derived some useful relations and further utilized the numeric method of the general linear least squares to determine the heat capacity of a sample. Absolute accuracy of the proposed method was verified by determining the heat capacity of a 0.249 76 g copper sample (purity 99.999%) on a self-designed and fully automated calorimetric system from 4.5 to 80 K. Comparing the result with the literature, the deviation in average was 1.2% from 4.5 to 20 K and 2.0% from 20 to 80 K. It is found that the proposed method is capable of measuring heat capacity regardless if the sample is adiabatically or nonadiabatically isolated. The size of the specimen is not critical for the application of the method and the temperature range of measurement can be expanded. It also deals with the τ...
238 citations
01 Nov 1991-Nuclear Instruments & Methods in Physics Research Section A-accelerators Spectrometers Detectors and Associated Equipment
TL;DR: The forward and rear calorimeters of the ZEUS experiment are made of 48 modules with maximum active dimensions of 4.6 m height, 0.2 m width, 7 λ depth and maximum weight of 12 t as mentioned in this paper.
Abstract: The forward and rear calorimeters of the ZEUS experiment are made of 48 modules with maximum active dimensions of 4.6 m height, 0.2 m width, 7 λ depth and maximum weight of 12 t. It consists of 1 X 0 uranium plates interleaved with plastic scintillator tiles read out via wavelength shifters and photomultipliers. The mechanical construction, the achieved tolerances as well as the optical and electronics readout are described. Ten of these modules have been tested with electrons, hadrons and muons in the momentum range 15–100 GeV/ c . Results on resolution, uniformity and calibration are presented. Our main result is the achieved calibration accuracy of about 1% obtained by using the signal from the uranium radioactivity.
234 citations
TL;DR: In this article, the authors measured the heat capacity of oterphenyl with an adiabatic calorimeter for the crystal from 2°K to Tm (329.35°K) and for the liquid from Tg to 360°K, on a sample with less than 0.005 mole % impurity.
Abstract: The heat capacity of o‐terphenyl has been measured with an adiabatic calorimeter for the crystal from 2°K to Tm (329.35°K), for the glasses from 2°K to Tg (around 240°K) and for the liquid from Tg to 360°K, on a sample with less than 0.005 mole % impurity. The heat of fusion and the entropy of fusion are 17 191 J mole−1 and 52.20 J°K−1· mole−1, respectively. The residual entropy of the glasses at 0°K is about 15 J°K−1· mole−1. Above 170°K, the heat capacity of the o‐terphenyl crystal is nearly proportional to the temperature to within 1%. Configurational entropy of the supercooled liquid, estimated from the result of this investigation, is used to relate the relaxation properties of glass‐forming liquids according to the theory of Adam and Gibbs. Good agreement is found for both viscosity and NMR correlation frequency data.
218 citations
01 Nov 1991-Nuclear Instruments & Methods in Physics Research Section A-accelerators Spectrometers Detectors and Associated Equipment
TL;DR: In this article, the mechanical design and construction techniques used in building the barrel calorimeter for the ZEUS detector were described, which is currently under construction for use at the HERA electron-proton colliding beam facility.
Abstract: We present the mechanical design and construction techniques used in building the barrel calorimeter for the ZEUS detector. The latter is currently under construction for use at the HERA electron-proton colliding beam facility. The calorimeter consists of 32 wedge shaped modules with approximate dimensions of 3×0.5×1.7 m 3 . The modules use alternate layers of depleted uranium and scintillator with one radiation length sampling. The light is collected via wavelength shifter plates placed on the sloping sides of the modules and read out by photomultiplier tubes located at the outer radius. The unit cell dimensions result in a ratio e h = 1 which yields an optimal energy resolution for hadronic jets. The placing of the structural components and the arrangement of the cracks between modules were chosen to maximize the uniformity of the response. Details of the construction and assembly effort needed to realize the total calorimeter are given. We finally describe the procedures used for transporting the completed modules to DESY and to install them on ZEUS.
212 citations
TL;DR: The average values of the enthalpy of solution of potassium chloride in water at 298.15 K have been found to be (17521 ± 13) J mol−1 when using an isoperibol L.K.B.
201 citations