Showing papers on "Dichlorophenylphosphine published in 2010"
TL;DR: In this paper, a one-pot procedure for the synthesis of unsymmetrical alkyl-substituted secondary phosphine oxides is described, where the use of ionic liquids in the first step is essential and streamlined the synthesis.
44 citations
TL;DR: Zirconacyclopentenes, which are easily prepared from alkynes, alkenes, and zirconocene compounds, reacted with dichlorophenylphosphine to give 2-phospholene in high yields.
12 citations
TL;DR: In this article, open-bed chromatography was carried out on silica gel (70 ~ 230 mesh, Merck) using gravity flow, and the column was packed with slurries made from the elution solvent.
Abstract: P NMR). IR spectra were obtained on a Mattson Genesis Series FT-IR spectrophotometer. Mass spectra were obtained on a GC Mate 2, JEOL. X-ray di-ffraction data were obtained with a Bruker SMART diffracto-meter equipped with a graphite monochromated Mo Kα (λ = 0.71073 A) radiation source and a CCD detector. The open-bed chromatography was carried out on silica gel (70 ~ 230 mesh, Merck) using gravity flow. The column was packed with slurries made from the elution solvent.