scispace - formally typeset
Search or ask a question
Topic

Differential scanning calorimetry

About: Differential scanning calorimetry is a research topic. Over the lifetime, 50315 publications have been published within this topic receiving 1152335 citations. The topic is also known as: DSC.


Papers
More filters
Journal ArticleDOI
01 Feb 1997-Polymer
TL;DR: In this paper, the trialkoxysilyl-functionalized PMMA/SiO2 hybrid has been successfully prepared without the use of the tri-alkoxynyl-functionalised polymer as a precursor which is hydrolytically unstable in the air.

151 citations

Journal ArticleDOI
TL;DR: Results of X-ray diffraction analyses indicated that the intensity of diffraction peak at 19 degrees of PVA became lower and broader with increasing the amount of GA in the CS/PVA/GA ternary blend film.

151 citations

Journal ArticleDOI
TL;DR: In this paper, the authors investigated the crystallization behavior of milk fat by varying the cooling rate and by isothermal solidification at various temperatures while monitoring the formation of crystals by differential scanning calorimetry (DSC) and X-ray powder diffraction (XRD).
Abstract: The crystallization behavior of milk fat was investigated by varying the cooling rate and by isothermal solidification at various temperatures while monitoring the formation of crystals by differential scanning calorimetry (DSC) and X-ray powder diffraction (XRD). Three different polymorphic crystal forms were observed in milk fat: γ, α, and β′. The β-form, occasionally observed in previous studies, was not found. The kind of polymorph formed during crystallization of milk fat from its melted state was dependent on the cooling rate and the final temperature. Moreover, transitions between the different polymorphic forms were shown to occur upon storing or heating the milk fat. The characteristic DSC heating curve of milk fat is interpreted on the basis of the XRD measurements, and appears to be a combined effect of selective crystallization of triglycerides and polymorphism.

151 citations

Journal ArticleDOI
TL;DR: The electrochemical impedance spectroscopy and differential scanning calorimetry indicated that solid electrolyte interphase can be confined in pores of as-prepared hollow structured SnO2@Si.
Abstract: A novel design of hollow structured SnO2@Si nanospheres was presented, which not only demonstrates high volumetric capacity as anode of LIBs, but also prevents aggregation of Sn and confines solid electrolyte interphase thickening. An impressive volumetric specific capacity of 1030 mAh cm–3 was maintained after 500 cycles. The electrochemical impedance spectroscopy and differential scanning calorimetry indicated that solid electrolyte interphase can be confined in pores of as-prepared hollow structured SnO2@Si.

151 citations

Journal ArticleDOI
TL;DR: The overall crystallization rates and mean relaxation times of amorphous nifedipine and phenobarbital in the presence of poly(vinylpyrrolidone) (PVP) were determined at various temperatures to gain further insight into the effect of molecular mobility on the crystallization rate of areorphous drugs and the possibility of predicting stability from their molecular mobility.

151 citations


Network Information
Related Topics (5)
Polymer
131.4K papers, 2.6M citations
92% related
Polymerization
147.9K papers, 2.7M citations
88% related
Aqueous solution
189.5K papers, 3.4M citations
88% related
Nanoparticle
85.9K papers, 2.6M citations
87% related
Amorphous solid
117K papers, 2.2M citations
86% related
Performance
Metrics
No. of papers in the topic in previous years
YearPapers
20231,992
20224,368
20211,646
20201,696
20191,799
20181,990