Topic
Indentation
About: Indentation is a research topic. Over the lifetime, 13002 publications have been published within this topic receiving 340476 citations.
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TL;DR: In this paper, it is shown that a separation of the elastic film properties is possible by using a novel analytical solution for the elastic deformation of a film on a flat substrate can be used to simulate the load-depth data.
Abstract: Indentation is an important method for the determination of mechanical properties of surfaces and thin films. It is well known that the measurement results from thin layers are strongly influenced by the substrate properties. For hardness measurements it is frequently quoted that the indentation depth should be less than one-tenth of the film thickness (1/10th rule). This rule is often not practicable for thickness values below 1 μm. Therefore a correction method is required that allows the separation of substrate and film properties from the load-depth data. Moreover, the calculation is complicated if plastic deformation occurs. The use of a spherical indenter allows one to remain completely within the elastic range if the indenter radius is large enough and the load is low enough. In this case a novel analytical solution for the elastic deformation of a film on a flat substrate can be used to simulate the load-depth data. With this solution the determination of Young’s modulus of thin layers is possible independent of indentation depth and film thickness. Measurement data from a UMIS-2000 indentation system for different film substrate combinations are compared with theoretical results. It is shown, that a separation of the elastic film properties is possible. For metal films on Si the load-depth data did not differ from that of uncoated substrates. This can be explained mainly by delamination.
124 citations
TL;DR: In this article, the elastic modulus of each polymer was determined from the unloading material response using the compliance method, whereas the hardness was calculated as the maximum contact load divided by the corre-sponding projected area, obtained from the known tip shape function.
Abstract: The nanomechanical properties of various polymers were examined in light of nanoindentation experiments performed with a diamond tip of nominal radius of curvature of about 20 μm under conditions of maximum contact load in the range of 150-600 μN and loading/unloading rates between 7.5 and 600 μN/s. The elastic modulus of each polymer was determined from the unloading material response using the compliance method, whereas the hardness was calculated as the maximum contact load divided by the corre-sponding projected area, obtained from the known tip shape function. It is shown that while the elastic modulus decreases with increasing indentation depth, the polymer hard-ness tends to increase, especially for the polymers possessing amorphous microstructures or less crystallinity. Differences in the material properties, surface adhesion, and time-dependent deformation behavior are interpreted in terms of the microstructure, crystallinity, and surface chemical state of the polymers. Results obtained at different maximum loads and loading rates demonstrate that the nanoindentation technique is an effective method of differentiating the mechanical behavior of polymeric materials with different microstructures.
124 citations
TL;DR: In this article, a phenomenological approach was used to describe the dependence of nanohardness H (P ) and H ( h ) on the indenter displacement of h by simple equations.
123 citations
TL;DR: In this paper, the authors explore the correlations between indentation stress-strain curves and the simple compression stress-strain curves using the finite element model of indentation as a surrogate for the actual experiment.
123 citations
TL;DR: In an attempt to elucidate the processes involved in the formation of indentation impressions, Vickers hardness measurements have been made on soda-lime silica glass, fused silica, and crystalline quartz indented at room temperature and 77 K as discussed by the authors.
Abstract: In an attempt to elucidate the processes involved in the formation of indentation impressions, Vickers hardness measurements have been made on soda-lime silica glass, fused silica, and crystalline quartz indented at room temperature and 77 K. The hardness of all three materials increases by a factor of ∼2.5 on cooling to liquid nitrogen temperature. High-magnification SEM photographs revealed that the deformation and cracking patterns of the glasses changed strikingly: no shear lines were observed within the indentations, and ring cracking occurred instead of radial/median cracking. In addition, cracking occurs at much higher loads than at room temperature. The hardness results have been explained in terms of volume flow (densification) rather than shear flow (viscous or plastic) for the glasses at low temperature. The quartz crystal, on the other hand, deformed plastically at both room temperature and 77 K. Cracking differences result from changes in both flow and water activity
123 citations