Topic
Thin-layer chromatography
About: Thin-layer chromatography is a research topic. Over the lifetime, 7494 publications have been published within this topic receiving 124179 citations. The topic is also known as: TLC.
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60 citations
TL;DR: When prostaglandin A1 was incubated with a Tris/saline suspension of washed human red blood cells, a substantial amount was converted to polar metabolites, which were purified by solvent extraction, XAD-2 column, and cellulose thin layer chromatography and characterized by chromatography, amino acid analysis, and mass spectrometry.
60 citations
TL;DR: In this article, cyclohexyl carbamates of cellulose and amylose were prepared and their resolving abilities for enantiomers were evaluated as chiral stationary phases (CSPs) for high-performance liquid chromatography.
Abstract: Cyclohexylcarbamates of cellulose and amylose were prepared and their resolving abilities for enantiomers were evaluated as chiral stationary phases (CSPs) for high-performance liquid chromatography. The CSPs showed high resolving abilities, which are comparable to those of popular CSPs, tris(3,5-dimethylphenylcarbamate)s of cellulose and amylose. The cycloalkylcarbamates could also be used as CSPs for thin-layer chromatography because of the absence of a phenyl group, which causes the difficulty of detection by UV radiation. In addition, these two derivatives were soluble in chloroform and exhibited chiral discrimination to some chiral compounds in 1H NMR spectroscopy as well as in HPLC.
60 citations
TL;DR: In this article, neutral fractions of oxidation products from side chain degradations of cholesteryl acetate were separated into more than twenty constituents and some of these could be determinated semi-quantitatively.
60 citations
60 citations