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Showing papers on "Ultimate tensile strength published in 2002"


Journal ArticleDOI
31 Oct 2002-Nature
TL;DR: A thermomechanical treatment of Cu is described that results in a bimodal grain size distribution, with micrometre-sized grains embedded inside a matrix of nanocrystalline and ultrafine (<300 nm) grains, which impart high strength, as expected from an extrapolation of the Hall–Petch relationship.
Abstract: Nanocrystalline metals--with grain sizes of less than 100 nm--have strengths exceeding those of coarse-grained and even alloyed metals, and are thus expected to have many applications. For example, pure nanocrystalline Cu (refs 1-7) has a yield strength in excess of 400 MPa, which is six times higher than that of coarse-grained Cu. But nanocrystalline materials often exhibit low tensile ductility at room temperature, which limits their practical utility. The elongation to failure is typically less than a few per cent; the regime of uniform deformation is even smaller. Here we describe a thermomechanical treatment of Cu that results in a bimodal grain size distribution, with micrometre-sized grains embedded inside a matrix of nanocrystalline and ultrafine (<300 nm) grains. The matrix grains impart high strength, as expected from an extrapolation of the Hall-Petch relationship. Meanwhile, the inhomogeneous microstructure induces strain hardening mechanisms that stabilize the tensile deformation, leading to a high tensile ductility--65% elongation to failure, and 30% uniform elongation. We expect that these results will have implications in the development of tough nanostructured metals for forming operations and high-performance structural applications including microelectromechanical and biomedical systems.

2,531 citations


Journal ArticleDOI
TL;DR: In this article, a tensile strength of 0.15 TPa was computed for individual carbon nanotubes in-situ in a transition electron microscope, based on the force required to break the tube.
Abstract: We have conducted pulling and bending tests on individual carbon nanotubes in-situ in a transition electron microscope. Based on our observation of the force required to break the tube, a tensile strength of 0.15 TPa was computed. From corresponding bending studies on such nanotubes, the Young's modulus was estimated to be 0.9 TPa (0.8 TPa after ‘sub continuum’ corrections). These results suggest a strength that is a large fraction of the elastic modulus, although previous measurements of their elastic stiffness have yielded higher modulus values, by as much as a factor of 2. The result does indicate that individual nanotubes can fail as essentially defect-free materials. Furthermore, we observed no obvious reduction in cross-sectional area prior to the failure. In addition, the bending experiments revealed a remarkable flexibility in these tubes. These unique properties support the potential of nanotubes as reinforcement fibers in structural materials.

1,069 citations


Journal ArticleDOI
TL;DR: In this paper, the Young's modulus of a flax fiber is estimated by taking into account the composition of the fibre and the evolution of the orientation of the fibrils during a tensile test.
Abstract: The knowledge of the behaviour of flax fibres is of crucial importance for their use as a reinforcement for composites materials. Flax fibres were tested under tensile loading and in repeated loading–unloading experiments. We have shown that fibre stiffness increases with the strain. This phenomenon is attributed to the orientation of the fibrils with the axis of the fibre when a strain occurs. By using micro-mechanical equations, the Young's modulus of a flax fibre is estimated by taking into account the composition of the fibre and the evolution of the orientation of the fibrils during a tensile test. A good agreement is found between experimental and calculated results. The origin of the large spread observed in the mechanical characteristics is analysed here.

890 citations


Journal ArticleDOI
01 Jan 2002-Carbon
TL;DR: In this paper, a fusible lignin with excellent spinnability to form a fine filament was produced with a thermal pretreatment under vacuum, but at PEO levels greater than 5%, the blends could not be stabilized without the individual fibers fusing together.

722 citations


Journal ArticleDOI
TL;DR: In this article, the percolation threshold of nanotubes in poly(propylene) and poly(polystyrene) matrices was investigated and a small increase in elastic modulus and decrease in tensile strength at low nanotube loading was observed, but as the concentration was increased there was a progressive increase in both strength and stiffness.
Abstract: The dispersion of nanotubes in polymer matrices has been investigated as a means of deriving new and advanced engineering materials. These composite materials have been formed into fibers and thin films and their mechanical and electrical properties determined. The nanotube concentration at which conductivity was initiated (the percolation threshold) varied with host polymer. In poly(propylene), this was as low as 0.05 vol.-%, while higher concentrations were required for polystyrene and particularly for ABS. There was a small increase in elastic modulus and decrease in tensile strength at low nanotube loading, but as the concentration was increased there was a progressive increase in both strength and stiffness.

687 citations


Journal ArticleDOI
TL;DR: In this paper, a micro-scale twin-screw extruder was used to achieve dispersion of multi-walled carbon nanotubes in a polystyrene matrix.
Abstract: Carbon nanotubes have been the subject of considerable attention because of their exceptional physical and mechanical properties. These properties observed at the nanoscale have motivated researchers to utilize carbon nanotubes as reinforcement in composite materials. In this research, a micro-scale twin-screw extruder was used to achieve dispersion of multi-walled carbon nanotubes in a polystyrene matrix. Highly aligned nanocomposite films were produced by extruding the polymer melt through a rectangular die and drawing the film prior to cooling. Randomly oriented nanocomposites were produced by achieving dispersion first with the twin-screw extruder followed by pressing a film using a hydraulic press. The tensile behaviour of the aligned and random nanocomposite films with 5 wt.% loading of nanotubes were characterized. Addition of nanotubes increased the tensile modulus, yield strength and ultimate strengths of the polymer films, and the improvement in elastic modulus with the aligned nanotube composite is five times greater than the improvement for the randomly oriented composite.

681 citations


Journal ArticleDOI
TL;DR: In this article, the cyclic elasto-plasticity of two types of steel sheets for press-forming (an aluminum-killed mild steel and a dual-phase high strength steel of 590 MPa ultimate tensile strength) under in-plane cyclic tension-compression at large strain (up to 25% strain for mild steel, and 13% for high-strength steel) was investigated.

582 citations


Journal ArticleDOI
TL;DR: In this paper, a tougher polypropylene (PP) was compounded with nano-silica by industrial-scale twin screw extruder and injection molding machine in the presence of grafting polymers on the nanoparticles.

570 citations


Journal ArticleDOI
TL;DR: In this article, the effects of environmental aging on tensile properties of both BFRP and BGRP systems were studied by immersing samples in water for up to 1200h at 25°C.
Abstract: Short bamboo fiber reinforced polypropylene composites (BFRP) and short bamboo–glass fiber reinforced polypropylene hybrid composites (BGRP) were fabricated using a compression molding method. Maleic anhydride polypropylene (MAPP) was used as a compatibilizer to improve the adhesion between the reinforcements and the matrix material. By incorporating up to 20% (by mass) glass fiber, the tensile and flexural modulus of BGRP were increased by 12.5 and 10%, respectively; and the tensile and flexural strength were increased by 7 and 25%, respectively, compared to those of BFRP. Sorption behavior and effects of environmental aging on tensile properties of both BFRP and BGRP systems were studied by immersing samples in water for up to 1200 h at 25°C. Compared to BFRP, a 4% drop in saturated moisture level is seen in BGRP. After aging in water for 1200 h, reduction in tensile strength and modulus for BGRP is nearly two times less than that of BFRP. Use of MAPP as coupling agent in the polypropylene matrix results in decreased saturated moisture absorption level and enhanced mechanical properties for both BFRP and BGRP systems. Thus it is shown that the durability of bamboo fiber reinforced polypropylene can be enhanced by hybridization with small amount of glass fibers.

557 citations


Journal ArticleDOI
TL;DR: In this article, the microstructure of commercially available nanocrystalline (nc) electroplated Ni foils is studied by means of Xray diffraction and transmission electron microscopy.

501 citations


Journal ArticleDOI
TL;DR: In this article, the analysis of tensile, flexural and impact properties of these composites revealed that the optimum length of fibre required for banana fibre and glass fibre are different in phenol formaldehyde resole matrix.

Journal ArticleDOI
TL;DR: In this paper, the influence of water uptake on the tensile properties of short sisal/PP composites has been studied with special reference to the effect of ageing conditions like treatment with water and UV radiation.

Journal ArticleDOI
TL;DR: In this paper, the impact strength and the density of the composites showed similar trends with an increase in fibre loading, however, elongation at break and flexural modulus are found to decrease beyond 40 wt% fibre loading.

Journal ArticleDOI
01 Jun 2002-Polymer
TL;DR: The mechanisms of deformation and fracture of isotactic polypropylene filled with CaCO3 particles were studied in this paper, where three types of particles with average diameters of 007, 07, and 35μm were used at filler volume fraction from 005 to 030.

Journal ArticleDOI
N. Chikhi1, S. Fellahi1, M. Bakar1
TL;DR: In this article, liquid amine-terminated butadiene acrylonitrile (ATBN) copolymers were added at different contents to improve the toughness of diglycidyl ether of bisphenol A epoxy resins using polyaminoimidazoline as a curing agent.

Journal ArticleDOI
TL;DR: In this paper, the microstructures and tensile properties of three typical Sn-Ag-Cu alloys, Sn-30wt%Ag-05wt%Cu and Sn-39Ag-06Cu, were evaluated after casting under three different cooling conditions.
Abstract: The microstructures and tensile properties of three typical Sn–Ag–Cu alloys, Sn–30wt%Ag–05wt%Cu, Sn–35wt%Ag–07wt%Cu and Sn–39wt%Ag–06wt%Cu, prepared under three different cooling conditions were evaluated after casting The microstructures of all rapidly cooled specimens consisted of the eutectic phase of β-Sn with fine fibrous Ag3Sn dispersion surrounding primary β-Sn grains The slowly cooled Sn–35Ag–07Cu and Sn–39Ag–06Cu alloys exhibited additional large primary Ag3Sn platelets, while the Sn–30Ag–05Cu did not For all alloys, both ultimate tensile strength and 02% proof stress increased with increasing strain-rates in tensile tests Lowering cooling speed decreased tensile strength Elongation increased with an increasing strain rate from 10−5 to 10−2 s−1, and decreased slightly at 10−1 s−1 for the rapidly cooled specimens Elongation remarkably decreased for the slowly cooled Sn–35Ag–07Cu and Sn–39Ag–06Cu alloys, a degradation attributable to the formation of large primary Ag3Sn platelets

Journal ArticleDOI
TL;DR: ACI Structural Journal, V. 99, No. 4, July-August 2002 as discussed by the authors, was reviewed under Institute publication policies, and a discussion was published in the May-June 2003 ACI structural journal if received by January 1, 2003.
Abstract: ACI Structural Journal/July-August 2002 ACI Structural Journal, V. 99, No. 4, July-August 2002. MS No. 01-402 received November 27, 2001, and reviewed under Institute publication policies. Copyright © 2002, American Concrete Institute. All rights reserved, including the making of copies unless permission is obtained from the copyright proprietors. Pertinent discussion will be published in the May-June 2003 ACI Structural Journal if received by January 1, 2003. ACI STRUCTURAL JOURNAL TECHNICAL PAPER

Journal ArticleDOI
TL;DR: In this paper, a step-by-step comparison of the mechanical performance of injection moulded "long" (LF-PP) and "short" (SF-PP), glass fibre-polypropylene compounds is presented.
Abstract: We present results of a step by step comparison of the mechanical performance of injection moulded ‘long’ (LF-PP) and ‘short’ (SF-PP) glass fibre-polypropylene compounds. The study allows direct comparison of the mechanical performance of long and short fibre systems in the same resin at the same fibre diameter, and the effect of fibre diameter in short fibre compounds. Furthermore, the comparison of these three systems has been made over the 0–40 wt% fibre content range. At the same fibre diameter and fibre content LF-PP gives significant improvements in room temperature tensile and flexural strength, notched and unnotched impact resistance. The improvement in impact resistance is higher still at lower test temperature. LF-PP also gives increasingly higher modulus over SF-PP as the strain is increased. The effect of lowering the fibre diameter in SF-PP has been shown to increase both strength and unnotched impact, but not to the levels obtained with LF-PP at higher fibre diameter. Notched impact and modulus of SF-PP were relatively unaffected by reduction of the fibre diameter. The relative mechanical data are shown to conform well to available models. The results are discussed in terms of the relevant micro-mechanical parameters of these materials.

Journal ArticleDOI
TL;DR: In this paper, the tensile strength of technical fiber bundles was found to depend strongly on the clamping length of the fiber bundles, and the failure behavior of elementary flax fibres under compression can be described as similar to the failure behaviour of a stranded wire.
Abstract: Mechanical properties of standard decorticated and hand isolated flax bast fibres were determined in tension as well as in compression. The tensile strength of technical fibre bundles was found to depend strongly on the clamping length. The tensile strength of elementary flax fibres was found to range between 1500 MPa and 1800 MPa, depending on the isolation procedure. The compressive strength of elementary flax fibres as measured with a loop test lies around 1200 MPa. However, the compressive strength can be lowered severely by the decortication process. The standard decortication process induces kink bands in the fibres. These kink bands are found to contain cracks bridged by microfibrils. The failure behaviour of elementary flax fibres under compression can be described as similar to the failure behaviour of a stranded wire.

Journal ArticleDOI
TL;DR: In this article, the benefit of using randomly distributed polyethylene terephthalate fiber, obtained from recycling waste plastic bottles, alone or combined with rapid hardening Portland cement to improve the engineering behavior of a uniform fine sand was evaluated.
Abstract: Unconfined compression tests, splitting tensile tests, and saturated drained triaxial compression tests with local strain mea- surement were carried out to evaluate the benefit of utilizing randomly distributed polyethylene terephthalate fiber, obtained from recycling waste plastic bottles, alone or combined with rapid hardening Portland cement to improve the engineering behavior of a uniform fine sand. The separate and the joint effects of fiber content~up to 0.9 wt %!, fiber length ~up to 36 mm!, cement content ~ from 0t o 7 wt %!, and initial mean effective stress ~20, 60, and 100 kN/m 2 ! on the deformation and strength characteristics of the soil were investigated using design of experiments and multiple regression analysis. The results show that the polyethylene terephthalate fiber reinforcement improved the peak and ultimate strength of both cemented and uncemented soil and somewhat reduced the brittleness of the cemented sand. In addition, the initial stiffness was not significantly changed by the inclusion of fibers.

Journal ArticleDOI
TL;DR: In this article, a comprehensive model for kinetic spray coating formation is proposed based on observations reported in this paper, and four velocity-dependent stages of coating formation are proposed based upon observations reported here, which are consistent with a metallic form for tensile tests on Al coatings removed from the substrate.
Abstract: Coatings have been produced by entraining relatively large diameter metal powders in a supersonic airflow. For the first time, most of the particles in the powders have diameters >50 μm. Substantial plastic deformation is involved in the conversion of the particle's kinetic energy into heat and strain energy in this kinetic spray process. As suggested by simple estimates and confirmed by coating grain structures, the particles are not melted or thermally softened in this coating process. These coatings have a relatively low oxide content, low thermal stress, high adhesion, low porosity and hardness somewhat higher than those of corresponding bulk materials. Threshold or critical velocities for coating formation are discussed. Critical velocities for the relatively large particles were observed to be substantially less than have been reported earlier for smaller diameter (<50 μm) particles. Coating particle rotation and deformation due to particle impact resulted in a corresponding decrease in porosity. Bond formation, particle deformation and grain deformation were found to be highly anisotropic, depending on the direction of the incident particle velocity. At higher incident velocities, increasing metallic bond formation between particles was observed. This is consistent with a metallic form for stress/strain curves obtained via tensile tests on Al coatings removed from the substrate. The coating elastic modulus was found to be less than half that of bulk Al. Measured ultimate tensile strengths and yield points of Al coatings were comparable to those of bulk Al. This may be due to work hardening resulting from the plastic deformation necessary for coating formation. These tensile test results are consistent with coating cohesive strengths as measured by stud pull tests. Higher powder feed rates produced coatings with higher failure loads in three point bending, higher coating cohesion and lower coating strength anisotropy, presumably due to a peening effect. Four velocity-dependent stages of coating formation are proposed based on observations reported here. Coating properties arise from a competition between these stages. Parallels with models of dynamic (explosive) powder compaction are made. This is the first comprehensive model for kinetic spray coating formation.

Journal ArticleDOI
TL;DR: In this paper, two series of composites with and without the presence of a bonding agent were studied and the properties of the composites such as tensile strength, tensile modulus, tear strength, elongation at break and hardness were studied.

Journal ArticleDOI
TL;DR: In this article, a FE analysis of the stress state in a ball on three balls tested disc is performed, where the stress field scales with the maximum principle stress, which occurs in the centre of the tensile surface.
Abstract: Biaxial strength testing of brittle materials is claimed to have some benefits compared to uniaxial testing, e.g. the much simpler specimen preparation, the avoiding of tensile loaded edges, the similarity of the stress state to those from typical loading (e.g. during a thermal shock loading) and the fact, that biaxial stress states are more revealing of defects than uniaxial stress states. The experience of the past showed, that biaxial strength testing has its own problems, to avoid these led to the development of several variants. One of these variants, the ball on three balls test, seems to be extremely simple: a disc is supported by three balls and then axially loaded from the opposite side via a fourth ball. In this system small deviations from the requested geometry, especially some out of flatness of the disc, are mentioned to be tolerable, but the threefold bending symmetry makes an exact analytical assessment of the stress state in the loaded disc extremely difficult. A numerical approach has yet not been performed. In this paper a FE analysis of the stress state in a ball on three balls tested disc is performed. The stress field scales with the maximum principle stress, which occurs in the centre of the tensile surface. For this stress an analytical approximation (which has been fitted to the numerical results) is given, which accounts for the influence of all relevant geometrical and material parameters. The investigated range of parameters considers the values typical for testing of brittle materials.

Journal ArticleDOI
TL;DR: In this article, the nano-silica element neither existed at the surfaces nor existed at interfaces of acrylic-based polyurethane coatings, and the silicon atoms intend to reside inside the coatings.

Journal ArticleDOI
TL;DR: In this article, a poly(ether ether ketone) nanocomposites containing vapour-grown carbon nanofibres (CNF) were produced using standard polymer processing techniques.
Abstract: Poly(ether ether ketone) nanocomposites containing vapour-grown carbon nanofibres (CNF) were produced using standard polymer processing techniques. Evaluation of the mechanical composite properties revealed a linear increase in tensile stiffness and strength with nanofibre loading fractions up to 15 wt% while matrix ductility was maintained up to 10 wt%. Electron microscopy confirmed the homogeneous dispersion and alignment of nanofibres. An interpretation of the composite performance by short-fibre theory resulted in rather low intrinsic stiffness properties of the vapour-grown CNF. Differential scanning calorimetry showed that an interaction between matrix and the nanoscale filler could occur during processing. Such changes in polymer morphology due to the presence of a nanoscale filler need to be considered when evaluating the mechanical properties of such nanocomposites.

Journal ArticleDOI
TL;DR: In this article, both particle size and particle volume fraction were systematically varied to investigate their effects on the fracture behavior and the fracture toughness of a highly-crosslinked, nominally brittle, thermosetting unsaturated polyester resin.
Abstract: Micron- and nanometer-sized aluminum particles were used as reinforcements to enhance the fracture toughness of a highly-crosslinked, nominally brittle, thermosetting unsaturated polyester resin. Both particle size and particle volume fraction were systematically varied to investigate their effects on the fracture behavior and the fracture toughness. It was observed that, in general, the overall fracture toughness increased monotonically with the volume fraction of aluminum particles, for a given particle size, provided particle dispersion and deagglomeration was maintained. The fracture toughness of the composite was also strongly influenced by the size of the reinforcement particles. Smaller particles led to a greater increase in fracture toughness for a given particle volume fraction. Scanning electron microscopy of the fracture surfaces was employed to establish crack front trapping as the primary extrinsic toughening mechanism. Finally, the effects of particle volume fraction and size on the tensile properties of the polyester-aluminum composite were also investigated. The measured elastic modulus was in accordance with the rule-of-mixtures. Meanwhile, the tensile strength was slightly reduced upon the inclusion of aluminum particles in the polyester matrix.

Journal ArticleDOI
TL;DR: The tensile behavior of composites produced by infiltrating ceramic particle beds with high purity (99.99%) is studied as a function of reinforcement size and chemistry (Al2O3 and B4C) as mentioned in this paper.

01 Jan 2002
TL;DR: In this article, two series of composites with and without the presence of a bonding agent were studied and the properties of the composites such as tensile strength, tensile modulus, tear strength, elongation at break and hardness were studied.
Abstract: Bamboo fibre reinforced natural rubber composites were prepared by incorporation of different loadings of bamboo fibre. Two series of composites were studied i.e. composites with and without the presence of a bonding agent. The curing characteristics of the composites were determined and the composites were vulcanized at 150°C using a hot press. The properties of the composites such as tensile strength, tensile modulus, tear strength, elongation at break and hardness were studied. The adhesion between the bamboo fibre and the natural rubber were enhanced by the addition of bonding agent as exhibited by the tensile fracture surfaces of the composites using scanning electron microscopy (SEM). The presence of bonding agent also gave shorter curing time and enhanced mechanical properties.  2001 Elsevier Science Ltd. All rights reserved.

Journal ArticleDOI
TL;DR: In this paper, a split Hopkinson tension bar was modified for the dynamic tensile stress-strain behavior of the low-strength and low-mechanical-impedance specimens.

Journal ArticleDOI
TL;DR: In this article, the strain rate dependent behavior of IM7/977-2 carbon/epoxy matrix composite in tension is studied by testing the resin and various laminate configurations at different strain rates.