Crystal-like microstructural Finemet/FeSi compound powder core with excellent soft magnetic properties and its loss separation analysis

Fe-based amorphous powder cores with low core loss and high permeability fabricated using the core-shell structured magnetic flaky powders

We report on the structural and magnetic characterization of two nanocrystalline Finemet-type magnetic cores. The nanocrystalline structure developed after annealing the amorphous precursor alloy at 550 °C for 30 and 60 min of annealing time. Structural analysis carried out by means of X-ray diffraction providing useful information on the grain size mean and partial volume of the nanocrystalline phase. The magnetic characterization was focused mainly in the Rayleigh region which, influenced by the intergranular coupling, was found to be more efficient in the sample treated for a longer time with a finer nanocrystalline structure.

https://www.mdpi.com/1996-1944/11/11/2278/pdf

Magnetic Characterization in the Rayleigh Region of Nanocrystalline Magnetic Cores

In this study, melt-spun Finemet ribbons were coated by a thin layer of SiO2 using dip coating method. Amorphous ribbon prepared by melt spinning method and dip coating were done by using a solution of tetraethylen orthosilicate as a SiO2 precursor, ethanol as solvent and distilled water for hydrolysis. Different thicknesses of SiO2 layer, namely 304, 349, 451, 526 and 970 nm were obtained proportional to the number of dipping. Surface morphology and chemical composition of the coatings were analyzed by using Scanning Electron Microscope equipped with an energy dispersive spectroscope. The results clearly verified the presence of Si and O elements and confirmed the presence of silica layer on the surface of all coated ribbons. Microstructure and surface morphology of samples showed a smooth and brittle layer. Electrical resistivity of the samples was measured with a standard four-point probe device. The results confirmed an intense in increase of resistivity. Average value of electrical resistivity for coated samples was around 104 Ω-m compared to 10-6 Ω-m for Finemet ribbons. Capacity of the samples was evaluated by electronic parameter analyzer device in two different frequencies of 100 kHz and 1000 kHz. Impedance measurements of coated samples in 100 and 1000 kHz showed an increase about 70 and 10 times respectively.

/pdf/dip-coating-of-silica-layer-on-melt-spun-finemet-ribbons-112j6p8ifo.pdf

P. Infante

Papers

Structural, magnetic characterization (dependencies of coercivity and loss with the frequency) of magnetic cores based in Finemet