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Oxathiaphospholane approach to N- and O-phosphorothioylation of amino acids.
TL;DR: A method of highly efficient synthesis of N- and O-phosphorothioylated/phosphorylated amino acids was developed and the DBU-assisted oxathiaphospholane ring-opening process in 3 and 10 did not cause any measurable C-racemization of phosphate diesters or amidoesters.