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Active alumina catalyst, and its preparation method and use

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TLDR
The active alumina catalyst can improve selectivity and yield of compound alkyl sulfide and methanethiol as mentioned in this paper, and can be used to improve the selectivity of compounds such as dimethyl sulfide.
Abstract
The invention relates to a catalyst technology, concretely, an active alumina catalyst and its producing method. Components of the active alumina catalyst are: Na 0.8-0.1 percents, Fe<0.1 percent the others are alumina whose purity is over 99 percent. The producing approach is: using aluminium hydroxide powder or (and) bodhmite powder as material; evenly mixing aluminium hydroxide powder or (and) bodhmite with aqua fortis solution deployed by deionized water; forming, drying in 100-150deg.C for 2-8 hours, baking in 400-600deg.C for 3-20 hours, bolstering and getting production. Adopting the invention can improve selectivity and yield of compound alkyl sulfide and alkyl sulfhydrate, esp. dimethyl sulfide and methanethiol.

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Alpha- alumina supporter and preparation method thereof and application

TL;DR: In this article, a mixture is prepared from (a), 10-80% of bayerite with granularity of not more than 150 meshes based on total weight of the total mixture; (b), 20-90% of boehmite with granular of 150 meshes, and (c), 0-3.0% of fluoride based on the total amount of total mixture according to alkaline-earth metal element.
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Alumina carrier and preparation method and application thereof

TL;DR: In this article, a preparation method for an alpha-alumina carrier is described, which comprises the following steps: I) uniformly kneading the mixture obtained in the step I) and carrying out molding by using a screw mold-pressing structured-carrier molding machine.
Patent

Preparation method of aluminum oxide catalyst and application of aluminum oxide catalyst to butyl rubber

Hu Zhaoyang
TL;DR: In this article, a preparation method of an aluminum oxide catalyst for butyl rubber is described. But the preparation method is simple in process and low in cost, the application of the obtained aluminum oxide catalysts to the butyl Rubber process indicates that the content of dimethyl ether is decreased to 0.1% or below, the situation that moisture exceeds the standard is avoided in the whole process, and the prepared Butyl Rubber is good in quality.
Patent

Phosphorous catalyst for synthesizing methyl mercaptan and preparation method thereof

TL;DR: In this article, the authors proposed a method for synthesizing methyl mercaptan using a phosphorous catalyst with higher methyl sulfide transformation rate and selectivity, and a preparation method thereof, which comprises the following steps of: dissolving a metered aluminum precursor by using water to prepare an aluminum solution; heating the aluminum solution, and then adding an metered phosphorus precursor solution and a dispersing agent, stirring, and adding a precipitator to form a gel solution at the same time; regulating the pH value of the gel solution to 5-9, and drying the
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Process for preparation of dimethyl thio-ether and methylthio-alcohol

Tian Xiyi, +1 more
TL;DR: The preparation method of dimethyl sulfide and methyl mercaptan is characterized by that it uses the sulfide containing 30-99% (mol%) hydrogen sulfide, methyl alcohol and methyl alcohol as raw materials, under the action of r-Al2O3 or alumino silica gel catalyst as mentioned in this paper.