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Preparation method of precipitated silica reinforced silicon rubber

Zang Zhanzhan
TLDR
In this paper, a preparation method of precipitated silica reinforced silicon rubber is described, in which the silicon rubber material is prepared from the following raw materials in parts by weight: 100 parts of raw rubber of methyl vinyl silicone rubber, 40 to 50 parts of white carbon black, 3 to 3.6 parts of structurized controlling agents, 0.3 to 0.8 part of hydrogen-containing silicone oil and 0.4 part of mold releasing agents.
Abstract
The invention discloses a preparation method of precipitated silica reinforced silicon rubber. The preparation method is characterized in that the silicon rubber is prepared from the following raw materials in parts by weight: 100 parts of raw rubber of methyl vinyl silicone rubber, 40 to 50 parts of precipitated silica reinforced white carbon black, 3 to 3.6 parts of structurized controlling agents, 0.3 to 0.8 part of hydrogen-containing silicone oil and 0.2 to 0.4 part of mold releasing agents. According to the preparation method, firstly, the weighed raw materials of 100 parts of raw rubberof raw rubber of methyl vinyl silicone rubber, 0.2 to 0.4 part of mold releasing agents and 0.3 to 0.8 part of hydrogen-containing silicone oil are fed into an internal mixer; then, 40 to 50 parts ofwhite carbon black are added into the internal mixer in three to five times; 3 to 3.6 parts of hydroxyl silicone oil are added; then, mixing and kneading are performed; the temperature is controlledto be 50 to 80 DEG C; after the internal mixing conglobation and still standing, the temperature is raised; vacuum pumping is performed; finally, the silicon rubber materials subjected to the vacuum pumping are subjected to remilling on a milling machine; after the rubber materials are smooth, filtering and packaging are performed to obtain a product. The preparation method has the advantages thatthe production process is simple; the tearing intensity is high; the effect is good, and the like.

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Patent

Method for improving dispersion of white carbon black in rubber

Wang Yongqing
TL;DR: In this paper, a method for improving dispersion of white carbon black in rubber was proposed, which comprises the following steps that natural rubber, nanoscale white carbon-black particles and hydroxyl silicone oil are mixed to be uniform in the weight ratio of (80-95):(32-45):(1-3) and then injected into an internal mixer.
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High-tear-resistance precipitated silicone rubber and preparation method thereof

TL;DR: In this paper, a high-tear-resistance precipitated silicone rubber and a preparation method for precipitated liquid silicone rubbers is described, and the preparation method consists of the following steps: adding raw rubber, high-hydrogen silicone oil and zinc stearate into an internal mixer; controlling the temperature in the internal mixer to be 60-80 DEG C, and starting internal mixing and kneading; adding high-oxyl silicone oil; adding white carbon black for 5-7 times within 90-180 min, and fully mixing the raw rubber and
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Formula and preparation method of extrusion type mixed silicone rubber

Wu Chengdong
TL;DR: The extrusion type mixed silicone rubber is good in stability, possesses high temperature resistance, high in oxidation resistance, is easy to shape, is non-sticky, easy to demold, is capable of being well extruded and formed in an extrusion mold, is high in formed product quality, is beneficial for production of silicone rubber products, is simple in preparation process, is inexpensive to produce, is low in production efficiency, and is convenient to use and convenient to popularize as mentioned in this paper.
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Preparation method of high-tear-resistance silicon compounded rubber

TL;DR: In this paper, a preparation method of high-tear-resistance silicon compounded rubber, which comprises the following steps: mixing 110-0 methylvinyl silicone rubber and 112 methylvinyel silicone rubber, adding precipitated white carbon black, zinc stearate, hydroxy silicon oil, hydrogen-containing silicon oil and vinyl silicon oil.
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TL;DR: In this paper, a silicone rubber composition consisting of polydimethylvinylsiloxane, a silica filler, a polymethylvinyl siloxane oil, a hydrogen-modified polyorganosiloxane and a platinum-based catalyst was described.