THE DESIGN AND ANALYSIS OF EXPERIMENTS. By Oscar Kempthorne. New York, John Wiley and Sons, Inc., 1952. 631 pp. $8.50. This book by a teacher of statistics (as well as a consultant for \"experimenters\") is a comprehensive study of the philosophical background for the statistical design of experiment. It is necessary to have some facility with algebraic notation and manipulation to be able to use the volume intelligently. The problems are presented from the theoretical point of view, without such practical examples as would be helpful for those not acquainted with mathematics. The mathematical justification for the techniques is given. As a somewhat advanced treatment of the design and analysis of experiments, this volume will be interesting and helpful for many who approach statistics theoretically as well as practically. With emphasis on the \"why,\" and with description given broadly, the author relates the subject matter to the general theory of statistics and to the general problem of experimental inference. MARGARET J. ROBERTSON

The Design and Analysis of Experiments

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3D printing, more formally known as Additive Manufacturing (AM), is already being adopted for rapid prototyping and soon rapid manufacturing. This review provides a brief discussion about AM and also the most employed AM technologies for polymers. The commonly-used ASTM and ISO mechanical test standards which have been used by various research groups to test the strength of the 3D-printed parts have been reported. Also, a summary of an exhaustive amount of literature regarding the mechanical properties of 3D-printed parts is included, specifically, properties under different loading types such as tensile, bending, compressive, fatigue, impact and others. Properties at low temperatures have also been discussed. Further, the effects of fillers as well as post-processing on the mechanical properties have also been discussed. Lastly, several important questions to consider in the standardization of mechanical test methods have been raised.

Mechanical characterization of 3D-printed polymers

Fused deposition modeling (FDM) is a rapidly growing 3D printing technology. However, printing materials are restricted to acrylonitrile butadiene styrene (ABS) or poly (lactic acid) (PLA) in most Fused deposition modeling (FDM) equipment. Here, we report on a new high-performance printing material, polyether-ether-ketone (PEEK), which could surmount these shortcomings. This paper is devoted to studying the influence of layer thickness and raster angle on the mechanical properties of 3D-printed PEEK. Samples with three different layer thicknesses (200, 300 and 400 μm) and raster angles (0°, 30° and 45°) were built using a polyether-ether-ketone (PEEK) 3D printing system and their tensile, compressive and bending strengths were tested. The optimal mechanical properties of polyether-ether-ketone (PEEK) samples were found at a layer thickness of 300 μm and a raster angle of 0°. To evaluate the printing performance of polyether-ether-ketone (PEEK) samples, a comparison was made between the mechanical properties of 3D-printed polyether-ether-ketone (PEEK) and acrylonitrile butadiene styrene (ABS) parts. The results suggest that the average tensile strengths of polyether-ether-ketone (PEEK) parts were 108% higher than those for acrylonitrile butadiene styrene (ABS), and compressive strengths were 114% and bending strengths were 115%. However, the modulus of elasticity for both materials was similar. These results indicate that the mechanical properties of 3D-printed polyether-ether-ketone (PEEK) are superior to 3D-printed ABS.

https://www.mdpi.com/1996-1944/8/9/5271/pdf

Influence of Layer Thickness and Raster Angle on the Mechanical Properties of 3D-Printed PEEK and a Comparative Mechanical Study between PEEK and ABS

FDM process parameters influence over the mechanical properties of polymer specimens: A review

Purpose – The mechanical properties and surface finish of functional parts are important consideration in rapid prototyping, and the selection of proper parameters is essential to improve manufacturing solutions. The purpose of this paper is to describe how parts manufactured by fused deposition modelling (FDM), with different part orientations and raster angles, were examined experimentally and evaluated to achieve the desired properties of the parts while shortening the manufacturing times due to maintenance costs. Design/methodology/approach – For this purpose, five different raster angles (0°, 30°, 45°, 60° and 90°) for three part orientations (horizontal, vertical and perpendicular) have been manufactured by the FDM method and tested for surface roughness, tensile strength and flexural strength. Also, behaviour of the mechanical properties was clarified with scanning electron microscopy images of fracture surfaces. Findings – The research results suggest that the orientation has a more significant in...

Experimental investigation of FDM process for improvement of mechanical properties and production cost

An experimental study on the effects of manufacturing parameters on the tribological properties of brake lining materials

In this study, the high-temperature ductility behaviour of an Al–Si-coated 22MnB5 sheet was investigated. The mechanical properties of Al–Si-coated 22MnB5 boron steel were examined via hot tensile tests performed at temperatures ranging from 400 to 900 °C at a strain rate of 0.083 s −1 . The deformation and fracture mechanisms under hot tensile testing were considered in relation to the testing data and to the fracture-surface observations performed via SEM. The hot ductility of the tested boron steel was observed as a function of increasing temperature and the Al–Si-coated 22MnB5 boron steel exhibited a ductility loss at 700 °C.

Investigation of the hot ductility of a high-strength boron steel

Purpose – The purpose of this paper is to investigate the role of solid lubricants (graphite, coke, ZnS) on brake performance.Design/methodology/approach – In this study, the tribological and surface characteristic of non‐asbestos organic type brake friction materials containing three different solid lubricants (graphite, coke, and ZnS) in different proportions were examined and evaluated experimentally. The coefficient of friction (COF) and wear behavior of the samples were tested on a chase‐type friction tester, and particular emphases were given to the effect of temperature and number of braking cycles on the COF. Each of the lubricants was added to the mixtures in different amounts and seven different brake linings were manufactured, provided that the total amount of solid lubricants and other ingredients were not changed. The worn surfaces of the specimens were analyzed using a scanning electron microscope with energy‐dispersive X‐ray microanalysis.Findings – The experimental results indicate that gr...

The effects of graphite, coke and ZnS on the tribological and surface characteristics of automotive brake friction materials

The flexural behavior of the 3D integrated woven spacer composites with carbon fiber-reinforced polymer face sheets are performed with epoxy and polyester matrix in the warp direction. The static loading of foam core carbon/epoxy and carbon/polyester composite sandwich panels in three-point flexural test was characterized at room temperature (23℃) and at liquid nitrogen temperature (−40℃). Macro-fracture morphology and progress have been examined to understand the deformation and failure mechanism. Significant increases in the flexural strength with brittle type core shear failure were observed at low temperatures as compared with the corresponding room temperature behavior. The performance of the epoxy-based composite is compared to the polyester one. Significant changes in the flexural properties of the composites have been found, first related to the temperature and then to the resin type. The flexural properties of the epoxy-based composites were affected greatly by temperature and exhibited higher fl...

Rukiye Ertan

Papers

Experimental investigation of FDM process for improvement of mechanical properties and production cost

An experimental study on the effects of manufacturing parameters on the tribological properties of brake lining materials

Investigation of the hot ductility of a high-strength boron steel

The effects of graphite, coke and ZnS on the tribological and surface characteristics of automotive brake friction materials

Experimental study on the flexural properties of 3D integrated woven spacer composites at room and subzero temperatures