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Tantalpulver mit glatter Oberfläche und Verfahren zur Herstellung desselben

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TLDR
In this paper, a Tantalpulver zu einer Anode eines Elektrolytkondensators is shown to have a Kapazitat of 450.000 bis 800.000 μFV/g, with a Konzentration of 0.1 Vol.-% unter einer Spannung of 1.6 V and a Strom of 90 mA/g.
Abstract
Tantalpulver, wobei, wenn das Tantalpulver zu einer Anode eines Elektrolytkondensators geformt wird, die Anode eine Kapazitat von 450.000 bis 800.000 μFV/g aufweist, gemessen durch das Pressen des Tantalpulvers zu Pellets mit Tantalzuleitungsdrahten, mit einer Pressdichte von 4,5 g/cm 3 , Sintern der Pellets, Anodisieren der gesinterten Pellets in einer wassrigen Phosphorsaurelosung mit einer Konzentration von 0,1 Vol.-% unter einer Spannung von 6 V und einem Strom von 90 mA/g, um anodisierte Pellets zu bilden und Prufen der Kapazitat in einer wassrigen Schwefelsaurelosung mit einer Konzentration von 30,5 Vol.-% bei einer Temperatur von 25°C unter einer Frequenz von 120 Hz und einer Spannung von 1,5 V.

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Methods to partially reduce a niobium metal oxide and oxygen reduced niobium oxides

James A. Fife
TL;DR: In this article, the process of heat treating the niobium oxide in the presence of a getter material and in an atmosphere which permits the transfer of oxygen atoms from the niibium oxide to the getter materials, and for a sufficient time and at a sufficient temperature to form an oxygen reduced Niobium oxides and/or suboxides is described.
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TL;DR: In this article, the process of heat treating the niobium oxide in the presence of a getter material and in an atmosphere which permits the transfer of oxygen atoms from the niibium oxide to the getter materials, and for a sufficient time and at a sufficient temperature to form an oxygen reduced Niobium oxides and/or suboxides is described.
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TL;DR: In this paper, the authors describe methods to at least partially reduce valve metal oxides, wherein the process includes heat treating the valve metal oxide in the presence of a getter material, in an atmosphere which permits the transfer of oxygen atoms from the starting valve metal Oxide to the getter Material, and for a sufficient time and at a sufficient temperature to form an oxygen reduced valve Metal Oxide.
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