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Journal ArticleDOI

The thermokinetic reactor TKR and its possible applications in chemical research and engineering

W. Litz
- 01 May 1983 - 
- Vol. 27, Iss: 1, pp 215-228
TLDR
In this article, a reactor-calorimeter is described which makes it possible to perform accurate measurements of the thermal power (rate of heat evolution) of chemical and physicochemical processes in essentially fluid reaction systems to be carried out continuously under isothermal conditions.
Abstract
A reactor-calorimeter is described which makes it possible to perform accurate measurements of the thermal power (rate of heat evolution) of chemical and physicochemical processes in essentially fluid reaction systems to be carried out a) continuously under isothermal conditions, b) without interfering with the course of the reaction, c) using large quantities of reaction mix, d) allowing for considerable variations in the consistency and/or the volume of the mix during reaction, e) providing for conditions which are very close to those of industrial practice. In addition, the equipment provides information on the heat transmittance of the reactor and the stirring power.

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Citations
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Journal ArticleDOI

Calorimetric-state estimators for chemical reactor diagnosis and control: review of methods and applications

TL;DR: In this article, the authors present an overview of control applications that use state estimators based on calorimetric principles for the control of stirred tank ReReactor (STR).
Journal ArticleDOI

Recent Developments in Hardware Sensors For the On-Line Monitoring of Polymerization Reactions

TL;DR: The increasing demand for the production of polymers with prespecified properties has placed great emphasis on the development of accurate and robust instruments for the on-line monitoring of polym....
Journal ArticleDOI

Isothermal reaction calorimetry as a tool for kinetic analysis

TL;DR: The most important reaction calorimetric principles (heat-flow, heat-balance, power-compensation, and Peltier principle) and their applications in commercial or scientific devices are reviewed in this article.
Journal ArticleDOI

Isothermal reaction calorimeters—I. A literature review

TL;DR: In this paper, the authors present a review of the available calorimeter equipment for the measurement of heat effects in chemical and physical processes, and present a new data treatment system for a commercial bench scale isothermal reaction calorometer.
Journal ArticleDOI

Calorimetric monitoring of industrial chemical processes

TL;DR: In this paper, the most promising applications of thermal methods are found in process development: enthalpimetric process investigation on the bench scale, and applications to a pressure reaction, to a highly unstable radical reaction and to fermentations are shown.
References
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Journal ArticleDOI

Differential Thermal Analysis

M. J. Vold
- 01 Jun 1949 - 
Journal ArticleDOI

Thermoanalytische methoden in der chemischen verfahrensentwicklung

W. Regenass
- 01 Jul 1977 - 
TL;DR: In this paper, a survey of methods and instruments for heat-flow calorimeter is given, and a new Bench Scale Heat-Flow Calorimeter (BSF) is presented.
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