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How to make sure that the hydrochloride salts are converted into hydroxide? 


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To ensure the conversion of hydrochloride salts into hydroxide, various methods can be employed based on the processes described in the provided research contexts. One approach involves utilizing electrodialysis processes with bipolar membranes to generate high-purity NaOH and HCl from NaCl, effectively preventing proton leakage through low-proton-leakage membranes like ARA and ACM . Another method involves a nonelectrolytic process using a thermally stable cation exchanger like ZSM-5 zeolite to liberate hydrochloric acid from a sodium chloride solution and subsequently generate sodium hydroxide through cation-exchange reactions with ammonium hydroxide . Additionally, a synthesis method for hydroxylamine hydrochloride ensures high purity and yield through steps like hydrolysis, vacuum distillation, crystallization, and filtration . By following these processes, the conversion of hydrochloride salts into hydroxide can be effectively achieved with high purity and efficiency.

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Patent
Hu Jianghai, Zhang Xiaolei, Yu Fei 
13 Jun 2017
2 Citations
The production process described involves the conversion of nitromethane, water, and hydrochloric acid into hydroxylamine hydrochloride through specific steps including reaction, concentration, crystallization, and drying.
The conversion of hydrochloride salts into hydroxide is achieved by cation-exchange reactions using a thermally stable cation exchanger like ZSM-5 zeolite in a nonelectrolytic process.
Through electro-electrodialysis, HCl and NaCl from NaCl are converted into NaOH and HCl with over 99.9% purity using low proton leakage membranes, ensuring the conversion of hydrochloride salts into hydroxide.
Through bipolar membrane electrodialysis, HCl and NaCl can be converted into high-purity NaOH and HCl solutions, ensuring the conversion of hydrochloride salts into hydroxide.
The hydroxylamine hydrochloride synthesis method involves separating hydroxylamine hydrochloride crystals from the hydrochloric acid solution, ensuring the conversion from hydrochloride to hydroxide.

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