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What are the common methods for preparing antimony tartrate complexes in research?

Antimony trichloride

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Common methods for preparing antimony tartrate complexes in research include leaching antimony-bearing residues, filtering the obtained slurry, and crystallizing the aqueous solution to form crystals of potassium antimony tartrate . Another method involves dissolving tartaric acid and antimony trichloride in deionized water, controlling the reaction temperature, and then heating, concentrating, and washing the resulting solid to obtain potassium antimony tartrate . Additionally, a method for preparing L-sodium antimony tartrate includes dissolving L-sodium bitartrate, adding antimonous oxide, filtering, concentrating, and precipitating the product through alcohol addition and centrifugation . Furthermore, complex metal antimony tartrates have been synthesized by evaporating aqueous solutions of potassium antimony tartrate and metal nitrates or chlorides, leading to the formation of infinite layers with M–O bonds .

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Patent Preparation method of antimony tartrate Wan Chuanyun, Shen Haiyan - Show less +1 more 16 Jul 2014	The common method for preparing antimony tartrate complexes involves dissolving tartaric acid and antimony trichloride, controlling the reaction temperature, and washing the solid with an organic solvent.
Patent Preparation method of high-yield L-sodium antimony tartrate Ding Chunyu, Li Qingjie, Lu Huasheng - Show less +2 more 23 Nov 2016	The common method for preparing L-sodium antimony tartrate involves heating L-sodium bitartrate, dissolving it in water, adding antimonous oxide, filtering, concentrating, adding alcohol, separating, centrifuging, and drying.
Patent Treatment of antimony bearing residues for production of potassium antimony tartrate Kumar Ashish, Mashruwala Sheeba, Sombhatla Sundar Saran, Rokkam Kiran Kumar, Sharma Krishna Deo - Show less +4 more 13 Jul 2017	The common method for preparing antimony tartrate complexes in research involves leaching antimony-bearing residues, filtering the slurry, and crystallizing the aqueous solution to form potassium antimony tartrate crystals.
Journal Article•DOI Layered structures based on antimony tartrate dimers Xiqu Wang, Allan J. Jacobson - Show less +1 more 11 Jul 2022-Zeitschrift für Kristallographie	The common method for preparing antimony tartrate complexes in research is by slowly evaporating aqueous solutions of potassium antimony tartrate and metal nitrates or chlorides.
Patent Method for production of potassium antimony tartrate by utilizing antimony bearing residues Kumar Ashish, Mashruwala Sheeba, Sombhatla Sundar Saran, Sharma Krishna Deo, Rokkam Kiran Kumar - Show less +4 more 31 Jul 2019	The common method for preparing potassium antimony tartrate involves leaching antimony-bearing residues, filtering the slurry, and crystallizing the aqueous solution in a jacketed crystallizer.

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