THE DESIGN AND ANALYSIS OF EXPERIMENTS. By Oscar Kempthorne. New York, John Wiley and Sons, Inc., 1952. 631 pp. $8.50. This book by a teacher of statistics (as well as a consultant for \"experimenters\") is a comprehensive study of the philosophical background for the statistical design of experiment. It is necessary to have some facility with algebraic notation and manipulation to be able to use the volume intelligently. The problems are presented from the theoretical point of view, without such practical examples as would be helpful for those not acquainted with mathematics. The mathematical justification for the techniques is given. As a somewhat advanced treatment of the design and analysis of experiments, this volume will be interesting and helpful for many who approach statistics theoretically as well as practically. With emphasis on the \"why,\" and with description given broadly, the author relates the subject matter to the general theory of statistics and to the general problem of experimental inference. MARGARET J. ROBERTSON

The Design and Analysis of Experiments

A review of shape memory alloy research, applications and opportunities

https://zirconia.typepad.com/files/zirconia-as-a-ceramic-biomaterial---piconi---biomaterials-1999.pdf

Zirconia as a ceramic biomaterial

In the present paper, the following topics are reviewed in detail: (a) the available adhesives, as well as their recent advances, (b) thermodynamic factors affecting the surface pretreatments including adhesion theories, wettability, surface energy, (c) bonding mechanisms in the adhesive joints, (d) surface pretreatment methods for the adhesively bonded joints, and as well as their recent advances, and (e) combined effects of surface pretreatments and environmental conditions on the joint durability and performance. Surface pretreatment is, perhaps, the most important process step governing the quality of an adhesively bonded joint. An adhesive is defined as a polymeric substance with viscoelastic behavior, capable of holding adherends together by surface attachment to produce a joint with a high shear strength. Adhesive bonding is the most suitable method of joining both for metallic and non-metallic structures where strength, stiffness and fatigue life must be maximized at a minimum weight. Polymeric adhesives may be used to join a large variety of materials combinations including metal-metal, metal-plastic, metal-composite, composite-composite, plastic-plastic, metal-ceramic systems. Wetting and adhesion are also studied in some detail in the present paper since the successful surface pretreatments of the adherends for the short- and long-term durability and performance of the adhesive joints mostly depend on these factors. Wetting of the adherends by the adhesive is critical to the formation of secondary bonds in the adsorption theory. It has been theoretically verified that for complete wetting (i.e., for a contact angle θ equal to zero), the surface energy of the adhesive must be lower than the surface energy of the adherend. Therefore, the primary objective of a surface pretreatment is to increase the surface energy of the adherend as much as possible. The influence of surface pretreatment and aging conditions on the short- and long-term strength of adhesive bonds should be taken into account for durability design. Some form of substrate pretreatment is always necessary to achieve a satisfactory level of long-term bond strength. In order to improve the performance of adhesive bonds, the adherends surfaces (i.e., metallic or non-metallic) are generally pretretead using the (a) physical, (b) mechanical, (c) chemical, (d) photochemical, (e) thermal, or (e) plasma method. Almost all pretreatment methods do bring some degree of change in surface roughness but mechanical surface pretreatment such as grit-blasting is usually considered as one of the most effective methods to control the desired level of surface roughness and joint strength. Moreover, the overall effect of mechanical surface treatment is not limited to the removal of contamination or to an increase in surface area. This also relates to changes in the surface chemistry of adherends and to inherent drawbacks of surface roughness, such as void formations and reduced wetting. Suitable surface pretreatment increases the bond strength by altering the substrate surface in a number of ways including (a) increasing surface tension by producing a surface free from contaminants (i.e., surface contamination may cause insufficient wetting by the adhesive in the liquid state for the creating of a durable bond) or removal of the weak cohesion layer or of the pollution present at the surface, (b) increasing surface roughness on changing surface chemistry and producing of a macro/microscopically rough surface, (c) production of a fresh stable oxide layer, and (d) introducing suitable chemical composition of the oxide, and (e) introduction of new or an increased number of chemical functions. All these parameters can contribute to an improvement of the wettability and/or of the adhesive properties of the surface.

Adhesively-bonded joints and repairs in metallic alloys, polymers and composite materials: Adhesives, adhesion theories and surface pretreatment

An updated review of adhesively bonded joints in composite materials

Functional fatigue of Ni–Ti shape memory wires under various loading conditions

Design of adhesive joints based on peak elastic stresses

The continuous advance in mechatronics has long attracted researchers toward the development of new highly integrated actuators for automotive applications where reduced space and low weight are common constraints. In this context, Shape Memory Alloys (SMAs) offer many peculiar characteristics that make this technology very attractive for the construction of miniature mechatronic actuators. This paper presents the design, the prototype fabrication, and the functional testing of a case study, where an SMA binary actuator is used for automotive tumble flaps. The innovative solid-state actuation system is proposed as an alternative to electromagnetic and pneumatic effectors, traditionally used to drive the tumble shaft of an air intake manifold for internal combustion engines. Original features of the linear actuator involve the mechanical architecture and the control structure. On the mechanical side, two contrasting sets of SMA springs are used to actively generate the net actuating force during both out-stroke and in-stroke. On the control side, a current feedback is exploited for sensorless real-time monitoring of the working temperature of the SMA springs during electrical supply. Major shortcomings of the proposed solution are a low response time and a power consumption higher than pneumatic and electromagnetic counterparts.

Mechatronic Design of a Shape Memory Alloy Actuator for Automotive Tumble Flaps: A Case Study

Intrinsic static strength of friction interfaces augmented with anaerobic adhesives

An usual experimental observation retrieved in the technical literature is that the strength of an adhesive joint decreases by increasing the adhesive layer thickness. This well-known behaviour is still not completely understood. All works found in the literature consider a complex stress state in the adhesive with mode mixing, stress concentrations on the midplane, and stress singularities at the interface occurring at the same time. This paper aims at estimating the effect of the adhesive thickness on its intrinsic static shear strength and evaluate whether this strength can explain the behaviour of a real bonded joint. A nearly uniform shear stress distribution is obtained through an ad-hoc tubular butt joint subject to pure torsion. A standard single lap joint is considered as a benchmark, due to its complex and singular stress field into the adhesive. The experimental campaign is focused on two brittle adhesives: a modified methacrylate and high-strength epoxy. Four levels and three levels of the adh...

Eugenio Dragoni

Papers

Functional fatigue of Ni–Ti shape memory wires under various loading conditions

Design of adhesive joints based on peak elastic stresses

Mechatronic Design of a Shape Memory Alloy Actuator for Automotive Tumble Flaps: A Case Study

Intrinsic static strength of friction interfaces augmented with anaerobic adhesives

Effect of Bondline Thickness on the Static Strength of Structural Adhesives Under Nearly-Homogeneous Shear Stresses