Ultrasound-assisted extraction and analysis of maidenhairtree polysaccharides.

This review elaborates on current advances in the extraction, purification, and antioxidant activity of plant leaf‐extract polysaccharides. Polysaccharides are widely used as important ingredients in the food, pharmaceutical, and cosmetic industries. Researchers have been investigating useful sources of natural polysaccharides and developing green and feasible extraction procedures for polysaccharides. This review examines different methods for extracting polysaccharides from leaves, and discusses their advantages and limitations. Purification techniques for plant leaf‐based polysaccharides were also highlighted, together with their antioxidant effects. Among different extraction methods, pressurized‐liquid extraction and enzyme‐assisted extraction are considered to be better for large‐scale extraction of polysaccharides from plant leaves. This review could contribute to the design of leaf waste processes at a commercial level for the sustainable recovery of polysaccharides. © 2022 The Authors. Biofuels, Bioproducts and Biorefining published by Society of Industrial Chemistry and John Wiley & Sons Ltd.

https://eprints.ncl.ac.uk/fulltext.aspx?url=286556/32A56542-5D2B-489F-AB13-E551C78CE484.pdf&pub_id=286556

Recent trends in extraction, purification, and antioxidant activity evaluation of plant leaf‐extract polysaccharides

Pulsed electric fields (PEF) and ultrasonic-assisted extraction (UE) were applied to improve the extraction performance of selenium-enriched tea polysaccharides (Se−TPSs) in mild conditions. Two combined extraction processes were investigated: (1) PEF strength at 10 kV/cm followed by conventional extraction (CE) at 50 °C for 60 min and (2) PEF+UE (PEF strength at 10 kV/cm followed by UE at 400 W for 60 min). The optimal extraction yields, and energy consumption rates were obtained at 36.86% and 41.53% and 78.78 kJ/mg and 133.91 kJ/mg, respectively. The Se−TPSs were analyzed and characterized by GPC, UV, and FT-IR, which evidenced the structural stability of the Se−TPSs during the extraction processes. It was found that PEF and UE could reduce the particle size diameter of the Se−TPS extract, as well as the proportion of uronic acid. Moreover, PEF could increase the selenium content in the Se−TPS extract by 160.14% due to a lower extraction temperature compared to conventional extraction. The antioxidant activities of the Se−TPSs in vitro were investigated using OH, O2−, and ABTS+ scavenging experiments, as well as a total antioxidant ability evaluation. It was found that the antioxidant activity of the Se−TPSs obtained using PEF2+CE2 was relatively high due to the potential synergistic effect between the selenium and polysaccharides. Based on these results, we speculate that PEF2+CE2 was the best extraction process for the Se−TPSs. Furthermore, this research indicates the application of selenium-enriched tea for functional food production.

/pdf/polysaccharides-in-selenium-enriched-tea-extraction-t5sglqwg.pdf

Polysaccharides in Selenium-Enriched Tea: Extraction Performance under Innovative Technologies and Antioxidant Activities

https://doi.org/10.1016/j.ultsonch.2022.106121

Prospects of ultrasonically extracted food bioactives in the field of non-invasive biomedical applications – A review

Abstract Inhalation-administrated drugs remain an interesting possibility of addressing pulmonary diseases. Direct drug delivery to the lungs allows one to obtain high concentration in the site of action with limited systemic distribution, leading to a more effective therapy with reduced required doses and side effects. On the other hand, there are several difficulties in obtaining a formulation that would meet all the criteria related to physicochemical, aerodynamic and biological properties, which is the reason why only very few of the investigated systems can reach the clinical trial phase and proceed to everyday use as a result. Therefore, we focused on powders consisting of polysaccharides, lipids, proteins or natural and synthetic polymers in the form of microparticles that are delivered by inhalation to the lungs as drug carriers. We summarized the most common trends in research today to provide the best dry powders in the right fraction for inhalation that would be able to release the drug before being removed by natural mechanisms. This review article addresses the most common manufacturing methods with novel modifications, pros and cons of different materials, drug loading capacities with release profiles, and biological properties such as cytocompatibility, bactericidal or anticancer properties.

/pdf/inhalable-microparticles-as-drug-delivery-systems-to-the-3e10gfo5.pdf

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Papers

Current emerging trends in antitumor activities of polysaccharides extracted by microwave- and ultrasound-assisted methods