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8-Hy­droxy­quinolin-1-ium hydrogen sulfate monohydrate

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TLDR
In the crystal structure of the title salt hydrate, C9H8NO+·HSO4 −·H2O, the quinoline N—H atoms are hydrogen bonded to the bisulfate anions, creating a three-dimensional network in which two R 4 4(12) rings and C 2 2(13) infinite chains can be identified.
Abstract
In the crystal structure of the title salt hydrate, C9H8NO+·HSO4−·H2O, the quinoline N—H atoms are hydrogen bonded to the bis­ulfate anions. The bis­ulfate anions and water mol­ecules are linked together by O—H⋯O hydrogen-bonding inter­actions. The cations and anions form separate layers alternating along the c axis, which are linked by N—H⋯O and O—H⋯O hydrogen bonds into a two-dimensional network parallel to (100). Further O—H⋯O contacts connect these layers, forming a three-dimensional network, in which two R44(12) rings and C22(13) infinite chains can be identified.

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Journal ArticleDOI

J. Appl. Cryst.の発刊に際して

良二 上田
Journal ArticleDOI

Intermolecular interactions in the solid state structures of neutral and N-protonated 5-alkoxymethyl-8-hydroxyquinolines

TL;DR: A series of five different alkoxymethyl substituted derivatives of 8-hydroxyquinoline was synthesised both in protonated ( 1a-1e ) and neutral ( 2a-2e ) form.
Dissertation

Synthesis of Gold Complexes From Diphosphine Ligands and Screening Reactions of Heterocyclic Acetylacetonato (ACAC) Ligands with Transitional Metal Complexes

TL;DR: In this paper, a synthesis of diphosphine gold (I) complexes from gold THT and two ligands, 4, 5-bis (diphenylphosphino)-4-cyclopenten-1, 3-dione (BPCD) and 2,3-bis(diphosphino) N-phenylmaleimide (BPPM) were done separately.
References
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Journal ArticleDOI

A short history of SHELX

TL;DR: This paper could serve as a general literature citation when one or more of the open-source SH ELX programs (and the Bruker AXS version SHELXTL) are employed in the course of a crystal-structure determination.
Journal ArticleDOI

The Cambridge Structural Database: a quarter of a million crystal structures and rising

TL;DR: The Cambridge Structural Database now contains data for more than a quarter of a million small-molecule crystal structures, and projections concerning future accession rates indicate that the CSD will contain at least 500,000 crystal structures by the year 2010.
Journal ArticleDOI

WinGX and ORTEP for Windows: an update

TL;DR: The WinGX suite provides a complete set of programs for the treatment of small-molecule single-crystal diffraction data, from data reduction and processing, structure solution, model refinement and visualization, and metric analysis of molecular geometry and crystal packing, to final report preparation in the form of a CIF.
Journal ArticleDOI

J. Appl. Cryst.の発刊に際して

良二 上田
Journal ArticleDOI

SIR2002: the program

TL;DR: Giacovazzo et al. as mentioned in this paper presented an overview of the work of the Dipartimento di Scienze della Terra Piazza UniversitaÁ, 06100 Perugia, Italy, Istituto di Cristallografia, CNR.
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