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An Electrochemical and Electron Microscopic Study of Activation and Roughening of Platinum Electrodes

T. Biegler
- 01 Aug 1969 - 
- Vol. 116, Iss: 8, pp 1131-1137
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This article is published in Journal of The Electrochemical Society.The article was published on 1969-08-01. It has received 67 citations till now. The article focuses on the topics: Electron beam-induced deposition & Platinum.

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A study of the dissolution of platinum, palladium, rhodium and gold electrodes in 1 m sulphuric acid by cyclic voltammetry

TL;DR: In this paper, it is emphasized that metal dissolution currents should not be ignored when examining electrochemical processes on noble metals at anodic potentials, and evidence in support of an anodic mechanism for noble metal corrosion has been obtained from studies of the variation of dissolution rate with both potential and temperature.
Journal ArticleDOI

The nature of adsorbed oxygen on rhodium, palladium and gold electrodes

TL;DR: In this paper, a basis for distinguishing between chemisorption and phase formation is presented, which can be used for accurate measurement of real surface area of rhodium and palladium electrodes.
Journal ArticleDOI

Hydrogen adsorption on platinum, iridium and rhodium electrodes at reduced temperatures and the determination of real surface area

TL;DR: In this article, the saturation hydrogen coverage and the real surface area of an electrode were determined directly from the voltammogram of platinum and iridium electrodes in 5 M sulphuric acid at −72°C.
Journal ArticleDOI

Vacuum-deposited gold films: I. Factors affecting the film morphology

TL;DR: Gold sputtering produces pebble-type structures with very small grains and no crystallographic texture, while evaporation of gold onto glass or mica produces large, flat crystallites, with a pronounced {111} texture.
Journal ArticleDOI

Determination of the surface composition of smooth noble metal alloys by cyclic voltammetry

TL;DR: In this paper, the potential of the oxygen desorption peak on a voltammogram was found to vary linearly with surface composition of homogeneous platinum-rhodium, palladium rhodium and palladium-gold alloy surfaces.
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