Journal ArticleDOI
Diaquabis(N,N‐diethylnicotinamide‐κN)bis(4‐fluorobenzoato‐κO)zinc(II)
TLDR
The ZnII complex as discussed by the authors is centrosymmetric and contains two 4-fluoro-benzoate and two diethyl-nicotinamide ligands and two water molecules, all ligands being monodentate.Abstract:
The title ZnII complex, [Zn(C7H4FO2)2(C10H14N2O)2(H2O)2], is centrosymmetric. It contains two 4-fluorobenzoate and two diethylnicotinamide ligands and two water molecules, all ligands being monodentate. The four O atoms in the equatorial plane around the Zn atom form a slightly distorted square-planar arrangement, while the distorted octahedral coordination is completed by the two N atoms in the axial positions. In the crystal structure, O—H⋯O hydrogen bonds link the molecules into infinite chains.read more
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Diaquabis(2-chlorobenzoato-κO)bis(nicotinamide-κN1)nickel(II)
TL;DR: The NiII complex [Ni(C7H4ClO2) 2(C6H6N2O)2(H2O 2 ) is centrosymmetric with the Ni atom located on an inversion center as mentioned in this paper, and it contains two 2-chloro-benzoate (CB) and two nicotinamide (NA) ligands and two water molecules.
Journal ArticleDOI
Diaqua-bis-(4-bromo-benzoato-κO)bis-(nicotinamide-κN)copper(II).
TL;DR: The NiII complex as mentioned in this paper is centrosymmetric and contains two 2-bromo-benzoate (BB) ligands, two nicotinamide ligands and two water molecules, all of them being monodentate.
Journal ArticleDOI
Diaqua-bis(2-chloro-benzoato-κO)bis-(N,N-diethyl-nicotinamide-κN)manganese(II).
TL;DR: The title compound is a monomeric complex with the MnII atom lying on an inversion center that contains two 4-chlorobenzoate and two diethylnicotinamide ligands and two water molecules, all of which are monodentate.
Journal ArticleDOI
Diaquabis[4-(dimethylamino)benzoato]-κ2O,O′;κO-(isonicotinamide-κN1)cobalt(II)
TL;DR: The CoII complex as discussed by the authors contains two 4-dimethyl-amino-benzoate (DMAB) anions, one isonicotinamide (INA) ligand and two coordinated water mol-ecules.
Journal ArticleDOI
Diaquabis(2-chlorobenzoato-κO)bis(N,N-diethylnicotinamide-κN1)manganese(II)
TL;DR: In the monomeric title complex, the MnII atom is located on a crystallographic centre of inversion, the asymmetric unit contains one 2-chlorobenzoate ligand, one diethylnicotinamide (DENA) ligand and one coordinated water molecule, all ligands being monodentate.
References
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ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI)
TL;DR: L Lists of software presented and~or reviewed in the Journal of Applied Crystallography are available on the World Wide Web at the above address, together with information about the availability of the software where this is known.
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WinGX suite for small-molecule single-crystal crystallography
TL;DR: The category Computer Program Abstracts provides a rapid means of communicating up-to-date information concerning both new programs or systems and signi®cant updates to existing ones.
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A semi-empirical method of absorption correction
TL;DR: An extension of Furnas's method is described in this paper, where the variation of intensity of an axial reflection as the crystal is rotated about the goniometer axis is used to give a curve of relative transmission T against azimuthal angle ϕ for the corresponding reciprocal lattice level.
Journal ArticleDOI
Synthesis, spectroscopic and magnetic properties of mixed-ligand complexes of copper(II) with imidazole and nitrogen-protected amino acids. Crystal and molecular structure of bis(hippurate)bis(imidazole)copper(II)
Luciano Antolini,L. P. Battaglia,A. Bonamartini Corradi,Giuseppe Onofrio Marcotrigiano,Ledi Menabue,Gian Carlo Pellacani,Monica Saladini +6 more