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Proton and carbon-13 assignments from sensitivity-enhanced detection of heteronuclear multiple-bond connectivity by 2D multiple quantum NMR

Ad Bax, +1 more
- 01 Apr 1986 - 
- Vol. 108, Iss: 8, pp 2093-2094
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This article is published in Journal of the American Chemical Society.The article was published on 1986-04-01. It has received 2528 citations till now. The article focuses on the topics: Heteronuclear molecule & Nuclear magnetic resonance spectroscopy.

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NMR spectroscopy in the structural elucidation of oligosaccharides and glycosides.

TL;DR: The potential of one- and two-dimensional NMR techniques for the identification of individual sugar residues, their anomeric configuration, interglycosidic linkages, sequencing and the site of any appended group in establishing the structures of naturally occurring oligosaccharides and glycosides is presented.
Journal ArticleDOI

13C NMR spectra of pentacyclic triterpenoids--a compilation and some salient features

TL;DR: In this paper, a compilation of the 13C NMR data of a selected variety of naturally occurring pentacyclic triterpenoids, arranged skeletonwise, is provided.
Journal ArticleDOI

The analysis of onion and garlic.

TL;DR: The literature about the major volatile and non-volatile phytoconstituents of onion and garlic has been reviewed, with particular attention given to the different methodology developed to perform chemical analysis, including separation and structural elucidation.
Journal ArticleDOI

Lignin-ferulate cross-links in grasses: active incorporation of ferulate polysaccharide esters into ryegrass lignins

TL;DR: In this article, NMR spectroscopy of uniformly 13 C-labeled ryegrass lignins was used to demonstrate the involvement of ferulate polysaccharide esters in the cross-coupling of lignin.
Journal ArticleDOI

Identification and synthesis of new ferulic acid dehydrodimers present in grass cell walls

TL;DR: In this paper, seven isomeric dehydrodimers of ferulic acid (4-hydroxy-3-methoxycinnamic acid) have been synthesized and identified in extracts of saponified cell walls of cocksfoot, switchgrass, and suspension-cultured corn.
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