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Showing papers on "Aluminium hydroxide published in 2018"


Journal ArticleDOI
TL;DR: In this paper, the case of Fe2+ ions removal from a synthetic aqueous solution by electrocoagulation with aluminium electrodes was investigated and the significance of the various physicochemical phenomena encountered e.g., formation of divalent iron hydroxide, adsorption of Fe species on Al(III) flocs formed and oxidation phenomena.

35 citations


Journal ArticleDOI
TL;DR: In this article, anion was designed by Solvay Specialty Polymers with the purpose to confer to the ionic liquids strong hydrophobic properties that facilitate the aluminium deposition in ambient conditions.

13 citations


Journal ArticleDOI
L. Zhang1, Awais Ullah Ihsan1, Y. Cao1, Y. Cheng1, Xiaohui Zhou1 
TL;DR: T2 in aluminium hydroxide adjuvant subcutaneous injection could successfully set up experimental autoimmune prostatitis in C57BL/6 mice, and the expression levels of IL‐1β in the prostate were more obvious than control groups.
Abstract: A mouse model was developed to simulate the clinical features of chronic prostatitis/chronic pelvic pain syndrome using peptide (T2 ). Forty C57BL/6 mice were divided into four groups of 10 mice each, averagely and randomly. T2 plus aluminium hydroxide adjuvant group was given subcutaneous injection with the emulsion mixture of T2 and aluminium hydroxide adjuvant, the T2 group with T2 , the aluminium hydroxide adjuvant group with aluminium hydroxide adjuvant and the normal control group with 0.9/% NaCl solution. Haematoxylin andeosin staining was used to observe the inflammation of the prostate. Plasma levels of TNF-α and CRP were detected by ELISA kit. The expression of IL-1βin the prostate was investigated by immunohistochemistry. The statistical differences between the groups were compared by t test. Histopathological analyses demonstrated that prostate lesions were most severe in the group immunised with T2 plus aluminium hydroxide adjuvant. Plasma levels of TNF-α and CRP were statistically elevated compared with control groups. The expression levels of IL-1β in the prostate were more obvious than control groups. T2 in aluminium hydroxide adjuvant subcutaneous injection could successfully set up experimental autoimmune prostatitis in C57BL/6 mice. This murine model would be greatly beneficial to further comprehend the aetiology, pathogenesis and explicit treatment of CP/CPPS.

13 citations


Journal ArticleDOI
TL;DR: In this paper, the authors proposed that the iron-rich gibbsitic bauxite experienced the deposition of a primary layer of a mixture of clay and gibbsite which later become mixed with the ferrallitic soil to form the nodules and clayey soil.

13 citations


Patent
10 Jul 2018
TL;DR: In this paper, a graphene-type high temperature-resistant phosphate anticorrosion paint is composed of modified aluminium dihydrogen phosphate and a curing agent, and comprises the following raw materials by mass percentage: 10-50% of a phosphoric acid solution, 0.5-15% of aluminium hydroxide, 0 5-10% of sodium tungstate, 0 3-15%, 0.1-8.0% of zirconia, and 10-80% of the curing agent.
Abstract: The invention relates to a graphene-type high temperature-resistant phosphate adhesive, and concretely relate to a graphene-type high temperature-resistant phosphate adhesive and a preparation methodthereof. A graphene-type high temperature-resistant phosphate anticorrosion paint is composed of modified aluminium dihydrogen phosphate and a curing agent, and comprises the following raw materials by mass percentage: 10-50% of a phosphoric acid solution, 0.5-15% of aluminium hydroxide, 0.5-10% of sodium tungstate, 0.3-15% of zirconia, 0.1-8.0% of a graphene oxide solution, and 10-80% of a curingagent. The graphene-type high temperature-resistant phosphate adhesive can be solidified at room temperature (greater than 20 DEG C) for 30-40 h or solidified at the temperature of 120 DEG C for 4 h,the shearing intensity of the solidified adhesive under high temperature of lower than 1300 DEG C with long term (at temperature of lower than 1800 DEG C with short term) cannot be changed, due to addition of graphene oxide, after adhesive solidification, when the usage temperature is greater than 400 DEG C, the graphene oxide is reduced to graphene. The existence of graphene can increase the shearing intensity of the adhesive at high temperature, and can shorten the solidification time. The graphene-type high temperature-resistant phosphate adhesive can be used for bonding metal, ceramic andglass, and can be used as a matrix of a composite material, a refractory material and a paint.

7 citations


Patent
Lu Sidi, Wang Wei, Lu Huaining, Zuo Zhen, Wang Zhe 
23 Feb 2018
TL;DR: In this article, a smoke suppression type dry powder extinguishing agent was proposed, which consisted of 60-70 parts of ammonium phosphate, 10-15 parts of bentonite, 12-14 parts of aluminium hydroxide, 8-9 parts of magnesium hydrate, 2-4 parts of C6-Fluoroketone and 2-3 parts of diphosphopyridine nucleotide.
Abstract: The invention discloses a smoke suppression type dry powder extinguishing agent. The smoke suppression type dry powder extinguishing agent comprises, by weight, 60-70 parts of ammonium phosphate, 10-15 parts of bentonite, 12-14 parts of aluminium hydroxide, 8-9 parts of magnesium hydrate, 2-4 parts of C6-Fluoroketone, 2-3 parts of diphosphopyridine nucleotide, 2-3 parts of nitric acid dyhydroxy bismuth, 2-3 parts of graphite powder and 1-2 parts of inorganic silica gel. The invention further discloses a preparation method of the smoke suppression type dry powder extinguishing agent. By means of the dry powder extinguishing agent, the defect that an existing dry powder extinguishing agent is used for putting out of fire, the amount of smoke is large can be overcome.

4 citations


Patent
02 Oct 2018
TL;DR: In this article, a method for producing aluminium hydroxide by adopting a waste aluminum material is described, in which non-aluminum materials attached to the waste aluminum materials are detached, removed and classified; the same type of waste aluminium material is placed into a smelting furnace to be molten; next, according to needed aluminum fuel components, matched alloy elements are added to be fully stirred and mixeduniformly, and after thermal insulation is performed, the product is casted into a die to prepare into an aluminum fuel ingot and to preparing into the aluminum fuel with
Abstract: Disclosed is a method for producing aluminium hydroxide by adopting a waste aluminum material. Non-aluminum materials attached to the waste aluminum material are detached, removed and classified; thesame type of waste aluminum material is placed into a smelting furnace to be molten; next, according to needed aluminum fuel components, matched alloy elements are added to be fully stirred and mixeduniformly, and after thermal insulation is performed, the product is casted into a die to prepare into an aluminum fuel ingot and to prepare into the aluminum fuel with a needed power generation shape; the aluminum fuel taken as a negative electrode is placed into an aluminum fuel cell system, the aluminum fuel cell is started to realize power generation, and aluminium hydroxide is generated in anelectrolyte of the aluminum fuel cell system; and separating, cleaning and drying are performed on aluminium hydroxide in the electrolyte of the aluminum fuel cell system to produce aluminium hydroxide. By adoption of the method, the waste aluminum material is changed into useful materials, so that pollution to the environment caused by a large amount of waste aluminium materials can be solved completely, and sustainable development of the aluminium source can be realized.

4 citations


Journal ArticleDOI
TL;DR: A direct reactive method to prepare transparent dispersions of pseudo-boehmite nanoparticles without any surface modification, and with an average particle size of 80 nm in length and 10 nm in width, as well as excellent optical transparency over 94% in the visible range is reported.
Abstract: Transparent dispersions of inorganic nanoparticles are attractive materials in many fields. However, a facile method for preparing such dispersions of aluminium hydroxide nanoparticles is yet to be realized. Here, we report a direct reactive method to prepare transparent dispersions of pseudo-boehmite nanoparticles (1 wt%) without any surface modification, and with an average particle size of 80 nm in length and 10 nm in width, as well as excellent optical transparency over 94% in the visible range. Furthermore, transparent dispersions of boehmite nanoparticles (1.5 wt%) were also achieved after an additional hydrothermal treatment. However, the optical transparency of dispersions decreased with the rise of hydrothermal temperature and the shape of particles changed from rhombs to hexagons. In particular, monodisperse hexagonal boehmite nanoplates with an average lateral size of 58 nm and a thickness of 12.5 nm were obtained at a hydrothermal temperature of 220 °C. The selectivity of crystal growth direction was speculated as the possible formation mechanism of these as-prepared aluminium hydroxide nanoparticles. Besides, two values of 19.6 wt% and 14.64 wt% were separately measured for the weight loss of pseudo-boehmite and boehmite nanoparticles after a continuous heating, indicating their potential flame-resistant applications in the fabrication of plastic electronics and optical devices with high transparency.

4 citations


Patent
30 Nov 2018
TL;DR: In this article, a macromolecular compound with constitution water can be formed in a reaction process, so that the finally prepared phosphate binder has higher stability and higher moisture absorption performance.
Abstract: The invention discloses a ferrous sulfate modified phosphate binder and a preparation method thereof. The ferrous sulfate modified phosphate binder is prepared from raw materials as follows: 53.74%-53.81% of phosphoric acid for industrial use, 10.81%-10.83% of aluminium hydroxide powder, 1.908%-1.910% of boric acid, 0.318% of silicic acid, 1.272%-1.274% of magnesium oxide, 0.02%-0.159% of ferroussulfate and 31.8%-31.84% of water. The preparation method comprises following steps: the raw materials are added in specific sequence, and with addition of ferrous sulfate, a macromolecular compound with constitution water can be formed in a reaction process, so that the finally prepared phosphate binder has higher stability and higher moisture absorption performance. A test indicates that a sandmold prepared from the binder has higher instant strength and constant-humidity room (RH40%) 6h strength, the maximum instant strength can reach 1.86 MPa, and the maximum constant-humidity room (RH40%) 6h strength can reach 1.76 MPa.

4 citations


Patent
18 Dec 2018
TL;DR: In this article, a method for preparing flower-like structure zinc oxide powder from low-and medium-grade zinc oxide ores is described. But this method is not suitable for the extraction of valuable components such as lead, strontium and silicon.
Abstract: The invention relates to the technical field of hydrometallurgy, in particular to a method for preparing flower-like structure zinc oxide powder from low-and medium-grade zinc oxide ores. The method comprises grinding the low-and medium-grade zinc oxide ores, and mixing the low-and medium-grade zinc oxide ores with ammonium bisulfate evenly for roasting to obtain a roasted material, adding water for dissolving the roasted material, filtering the roasted material, using filter residue to extract valuable components such as lead, strontium and silicon, precipitating iron by an ammonium jarositemethod and precipitating aluminium by an aluminium hydroxide form to obtain a purified solution with the iron and the aluminium removed; mixing the purified solution with an alkali solution in a molarratio of Zn : OH of 1:2-10, and placing the purified solution and the alkali solution in a hydrothermal reactor, and adding a PEG 20000 or SDBS solution with a mass concentration of 5-15% to the hydrothermal reactor, homogeneously stirring, reacting at 120-220 DEG C for 4-12 h, filtering, washing and drying to obtain the flower-like structure zinc oxide powder.

4 citations


Journal ArticleDOI
TL;DR: In this article, a modification of the raw materials composition and autoclave regime of aerated concrete using aluminium hydroxide in order to improve final mechanical properties and mineralogical composition is proposed.
Abstract: Aerated concrete is lightweight building material with excellent thermos-technical properties compared to its strengths, easy workability and economic efficiency. It is material with long tradition of manufacturing since 1924 but its potential is yet possible to be extended. Since the beginning pure ingredients such as lime and silica sand has been used. Nowadays we are looking for ways to replace these expensive raw materials with cheaper alternatives. One of the most important mechanical properties of each material is its strength. In case of aerated concrete the bearer of strength is mineral tobermorite. It is created by reaction of silicon oxides and lime at hydrothermal conditions. It belongs to the group of calcium hydrosilicates with chemical formula Ca5Si6O16(OH)2·4H2O. Main goal of this paper is proposal for modification of the raw materials composition and autoclave regime of aerated concrete using aluminium hydroxide in order to improve final mechanical properties and mineralogical composition.

Journal ArticleDOI
01 Sep 2018
TL;DR: In this paper, the synthesis process of γ-alumina/SiO2 composite from aluminium powders and amorphous nanosilica through the means of tetra-methyl-ammonium hydroxide (TMAH) as the mixing medium was reported.
Abstract: This article reports the synthesis process of γ-alumina/SiO2 composite from aluminium powders and amorphous nanosilica through the means of tetra-methyl-ammonium hydroxide (TMAH) as the mixing medium which produced aluminium hydroxide Al(OH)3 in the form of white powders. The crystal structures, microstructures, and mapping of the atomic constituent of γ-Al2O3 and γ-Al2O3/SiO2 samples were respectively analyzed via X-ray diffraction (XRD), and scanning electron microscopy-energy dispersive X-ray SEM-EDX. At the calcination temperature to 300 °C, the samples still had boehmite phase, and the boehmite phase transformation to γ-alumina phase occurred at temperature of 700-900 °C. The γ-alumina phase began to form at the calcination temperature of 500-700 °C with the crystal structure of (440), (511), (400), (222), (311), and (111). The similar diffraction pattern was also shown by the γ-Al2O3/SiO2 composite for the calcination temperature of 700 °C and 900 °C. The microstructure analysis of the γ-Al2O3/SiO2 showed that SiO2 particles were smaller and round while the γ-Al2O3 particles were bigger and elongated. Additionally, the mapping results showed SiO2 and γ-Al2O3 particles were homogenously distributed.

Patent
08 Feb 2018
TL;DR: In this paper, a method for manufacturing a cracking catalyst is described, which includes carrying out ion exchanges for cations of rare-earth elements and ammonium in NaY zeolite, two stages of ultrastabilization of the zeolisolite in an environment of water vapour, mixing the zeolites with a matrix comprised of bentonite clay, aluminium hydroxide and amorphous aluminium silicate, producing a composition, spray drying said composition, and subsequently calcining and producing a catalyst, wherein the catalyst contains 0.1-1.
Abstract: The invention relates to the field of the petroleum refining and petrochemical industry, and more particularly to methods for manufacturing catalysts of the catalytic cracking of petroleum fractions. The invention solves the problem of producing an effective cracking catalyst. A method for manufacturing a cracking catalyst includes carrying out ion exchanges for cations of rare-earth elements and ammonium in NaY zeolite, two stages of ultrastabilization of the zeolite in an environment of water vapour, mixing the zeolite with a matrix comprised of bentonite clay, aluminium hydroxide and amorphous aluminium silicate, producing a composition, spray drying said composition, and subsequently calcining and producing a catalyst, wherein prior to the first stage of ultrastabilization, additional ion exchange of sodium cations in the zeolite for magnesium cations or calcium cations is carried out without intermediate filtration to produce Y zeolite, containing: not more than 0.6 mass% sodium oxide; 0.5-5.5 mass% rare earth element oxides; 0.5-4.0 mass% magnesium oxide; 1.0-7.0 mass% calcium oxide; wherein the catalyst contains 0.1-1.1 mass% rare earth element oxides; 0.23 mass% sodium oxide; 0.1-0.8 mass% magnesium oxide from the zeolite component or 0.2-1.4 mass% calcium oxide from the zeolite component.

Patent
19 Oct 2018
TL;DR: In this article, a preparation method of low-sodium submicron alpha-alumina is described in which industrial alumina is used as a raw material in the preparation process.
Abstract: The invention relates to a preparation method of low-sodium submicron alpha-alumina. The preparation method is characterized in that industrial alumina is used as a raw material in the preparation process. The industrial alumina is obtained by flash-roasting metallurgical-grade aluminium hydroxide produced by Bayer process at 1100-1300 DEG C through a suspension roaster. The principal crystallinephase is gamma phase; BET specific surface area is 60-100 m /g; content of sodium oxide is less than 0.5 wt%; content of iron oxide is less than 0.015 wt%; and content of silica is less than 0.015 wt%. the preparation method comprises the following steps: blending industrial alumina with pure water and a crystalline form regulator to prepare slurry; carrying out wet impurity removal treatment toobtain wet alumina; and finally calcining to obtain a low-sodium submicron alpha-alumina product, and dispersing and dispersing through an agitator mill, a ceramic ball mill or a sand mill to obtainlow-sodium submicron alpha-alumina powder.

Patent
Zhao Fei, Tiezhu Ge, Zhao Hua, Enxia Xu, Jinxing Gao 
21 Sep 2018
TL;DR: In this paper, a preparation method of a light-weight high-strength calcium hexaluminate fire resistant material is described, which is characterized by comprising of the following steps that (1) 38-60% of calcarea carbonica raw material and 40-62% of aluminium hydroxide are mixed by weight and mixed with, by weight, 80-120% of water, 0.02-0.05% of dispersing agent and 1-4% of binding agent, and ball-milling is carried out for 3-5 hours to obtain
Abstract: The invention provides a preparation method of a light-weight high-strength calcium hexaluminate fire resistant material. The method is characterized by comprising the following steps that (1) 38-60%of calcarea carbonica raw material and 40-62% of aluminium hydroxide are mixed by weight and mixed with, by weight, 80-120% of water, 0.02-0.05% of dispersing agent and 1-4% of binding agent, and ball-milling is carried out for 3-5 hours to obtain a mixed slurry; (2) spray granulation is carried out on the mixed slurry to obtain spherical fine particles; (3) the spherical fine particles are calcined at 1000-1200 DEG C to obtain light-weight porous beads; (4) 15-30% of light-weight porous beads and 70-85% of aluminium oxide raw material are mixed by weight and mixed with 2-6% of binding agent by weight, after stirring is uniform, compression molding is carried out under 10-30 MPa, and calcination is carried out for 6-8 hours at 1600-1700 DEG C to obtain the light-weight high-strength calcium hexaluminate fire resistant material.

Journal ArticleDOI
TL;DR: The results indicated that an aluminium hydroxide adjuvant preparation was cytotoxic and mutagenic in human-Chinese hamster ovary (CHO) hybrid cells in vitro, suggesting that aluminium is associated with DSBs.
Abstract: Aluminium has been found in feline vaccine-associated sarcomas. In this study, we investigated the potential for aluminium to contribute directly to tumourigenesis. Our results indicated that an aluminium hydroxide adjuvant preparation was cytotoxic and mutagenic in human-Chinese hamster ovary (CHO) hybrid cells in vitro. Moreover, CHO cells deficient in DNA double strand break (DSB), but not single-strand break (SSB), repair, were particularly sensitive to aluminium exposure compared with repair proficient cells, suggesting that aluminium is associated with DSBs. In contrast to CHO cells, primary feline skin fibroblasts were resistant to the cytotoxic effects of aluminium compounds and exposure to an aluminium chloride salt promoted cell growth and cell cycle progression at concentrations much less than those measured in particular feline rabies vaccines. These findings suggest that aluminium exposure may contribute, theoretically, to both initiation and promotion of tumours in the absence of an inflammatory response.

Patent
26 Oct 2018
TL;DR: In this article, an insulation flexible facing brick which is prepared from the following raw materials in parts by weight cement, a ceramic filler, a phase-change energy storage microcapsule, an emulsion, a flame retardant, an inorganic pigment, quartz sands and water.
Abstract: The invention provides an insulation flexible facing brick which is prepared from the following raw materials in parts by weight cement, a ceramic filler, a phase-change energy storage microcapsule, an emulsion, a flame retardant, an inorganic pigment, quartz sands and water; the ceramic filler is made of hard ceramics; a core material of the phase-change energy storage microcapsule is a materialco-melted by paraffin and polyethylene; the cement is selected from one or more of portland cement, aluminate cement, sulphate aluminium cement, ferrous aluminate cement, fluoraluminate cement and phosphate cement; the flame retardant is selected from one or more of antimonous oxide, magnesium hydroxide and aluminium hydroxide; and the inorganic pigment is selected from one or more of titanium white, chrome yellow, iron blue, cadmium red, cadmium yellow, lithopone, carbon black, iron oxide red and iron oxide yellow. The flexible facing brick provided by the invention has good flexibility and mechanical performance and has the insulation performance obviously superior to other like products.

Patent
05 Jan 2018
TL;DR: In order to further raise flocculation effect of polymeric phosphate-aluminum chloride, the invention of as discussed by the authors provides a preparation technology for polymeric-phosphoric acid and aluminum hydroxide.
Abstract: The invention relates to the field of water treatment. In order to further raise flocculation effect of polymeric phosphate-aluminum chloride, the invention provides a preparation technology of polymeric phosphate-aluminum chloride. According to a preparation method of an aluminium salt coagulant, aluminium hydroxide, hydrochloric acid and calcium powder are used as main aluminium-containing raw materials. The preparation technology of the invention has more excellent flocculation effect, and the technology is simple and practical.

Patent
21 Sep 2018
TL;DR: In this article, a method for acid-making and co-production of mullite firebricks from phosphogypsum and fly ash, comprising the following steps: mixing phosphogypticpsum, fly ash and an additive and amodifier, grinding to prepare a raw material, sending the raw material into a kiln and roasting to preparing a clinker, water-milling and dissolving out the clinker and carrying out solid-liquid separation, roasting a solid obtained by separation and processing to prepare sulfuric acid, adding CO2 to a liquid obtained by
Abstract: The invention provides a method for acid-making and co-production of mullite firebricks from phosphogypsum and fly ash, comprising the following steps: mixing phosphogypsum, fly ash, an additive and amodifier, grinding to prepare a raw material, sending the raw material into a kiln and roasting to prepare a clinker, water-milling and dissolving out the clinker, carrying out solid-liquid separation, roasting a solid obtained by separation and processing to prepare sulfuric acid, adding CO2 to a liquid obtained by separation to obtain aluminium hydroxide, and preparing the mullite firebricks from the aluminium hydroxide, kaolinite, illite, montmorillonite, lapis amiridis, quartz stone, talcum powder, sawdust, expandable polystyrene spheres and polyvinyl alcohol. By comprehensive utilizationof phosphogypsum and fly ash, environmental pollution can be reduced, and added value is high. in addition, the prepared aluminium hydroxide is a good raw material for production of the mullite firebricks, and the prepared mullite firebricks have the advantage of low production cost.

Journal Article
TL;DR: In this article, bagasse ash and potassium salt were mixed at a weight ratio of 1:1.2 and then fused at 550 °C for 1 hour prior to the hydrothermal treatment.
Abstract: This work aim to synthesis of a 3A zeolite (K-LTA) obtained by a fusion process of potassium salt, synthesized from the bagasse ash. The bagasse ash and aluminium hydroxide sludge were sources of starting materials for K-A zeolite (3A zeolite) conversion using the alkali fusion hydrothermal process. The bagasse ash and potassium salt were mixed at the weight ratio of 1:1.2 and then fused at 550 °C for 1 hour prior to the hydrothermal treatment. After that, the hydroxide solution was added to the fused material slurry and thoroughly stirred at 105± 3 °C in the stainless steel reactor. The reaction time was varied from 1 to 6 hours. The results showed that the highest yield of 3A zeolite conversion was approximately 62% and was obtained from the mixtures containing hydroxide solution, stirred for 5 hours. Keywords— 3A zeolite, Bagasse Ash, Aluminium Hydroxide Sludge, Fusion Method, Waste Utilization

Patent
28 Nov 2018
TL;DR: In this article, a method for manufacturing colored aluminum hydroxide is described, which consists of forming a sodium aluminate solution at a first temperature, adding a colored pigment to the solution at the second temperature, and cooling the solution to which the colored pigment is added to a second temperature lower than the first temperature.
Abstract: A method for manufacturing colored aluminum hydroxide is disclosed. The method for manufacturing colored aluminum hydroxide according to the present invention comprises the steps of: (a) forming a sodium aluminate solution at a first temperature; (b) adding a colored pigment to the sodium aluminate solution at the first temperature; and (c) cooling the sodium aluminate solution to which the colored pigment is added to a second temperature lower than the first temperature to precipitate aluminum hydroxide; and (d) drying the precipitated aluminum hydroxide. In the step (d), the solvent is removed, and the colored pigment is coated on the surface of the precipitated aluminum hydroxide. According to the present invention, the colored aluminum hydroxide can be easily manufactured without coating with a separate colored pigment.

Patent
14 Feb 2018
TL;DR: In this article, a fire-retardant composition for manufacturing polymethylsiloxane or polymethylphenylsiloxideane rubber is described, which includes a coke-forming bulging component - oxidized graphite, glass glazed microspheres, pentaerythritol, phosphate mono-substituted ammonium, melamine, aluminium hydroxide, chopped glass fibre, water repellent - organosilicon fluid, a curing catalyst - gammaaminopropyltriethoxysilane in the following ratio of components,
Abstract: FIELD: chemistry.SUBSTANCE: composition is described for manufacturing a fire-retardant coating, that includes polymethylsiloxane or polymethylphenylsiloxane rubber, a coke-forming bulging component - oxidized graphite, glass glazed microspheres, a coke-forming bulging component - pentaerythritol, phosphate mono-substituted ammonium, a coke-forming bulging component - melamine, aluminium hydroxide, chopped glass fibre, water repellent - organosilicon fluid, a curing catalyst - gammaaminopropyltriethoxysilane in the following ratio of components, pts. wt : polymethylsiloxane or polymethylphenylsiloxane rubber 40.0-75.0, oxidized graphite 12.0-18.0, glass glazed microspheres 1.5-3.5, pentaerythritol 13.0-18.0, phosphate mono-substituted ammonium 13.0-18.0, melamine 4.0-6.5, aluminium hydroxide 7.0-14.0, chopped glass fibre 1.5-3.5, water repellent - organosilicon fluid 5.0-10.0, curing catalyst - gammaaminopropyltriethoxysilane 5.0-9.0. A method of manufacturing the compositionis is also described.EFFECT: coating with increased strength and improved processability is obtained.2 cl, 2 tbl

Patent
01 Jun 2018
TL;DR: In this paper, a comprehensive recovery treatment method for residual liquid after sponge indium being replaced from indium-containing aluminium is presented, which belongs to the field of wet-process metallurgy.
Abstract: The invention discloses a comprehensive recovery treatment method of residual liquid after sponge indium being replaced from indium-containing aluminium and belongs to the field of wet-process metallurgy. The comprehensive recovery treatment method adopts the technical process flow with the following steps: firstly adopting calcium oxide or calcium hydroxide to neutralize the residual liquid afterthe indium is replaced from chlorine-containing aluminium till the pH is 4.5-5, hydrolyzing to precipitate indium hydroxide, then using sodium hydroxide to continuously neutralize indium-hydroxide filtrate, reacting with aluminium chloride to generate Na3AlO3, reacting with calcium chloride to generate calcium hydroxide precipitate which can return for use, neutralizing filtrate from filtration of the calcium hydroxide by using hydrochloric acid to make Na3AlO3 hydrolyzed to generate aluminium hydroxide precipitate, filtering, then concentrating sodium chloride filtrate, electrolyzing, and respectively recovering chlorine gas and sodium hydroxide. The comprehensive recovery treatment method disclosed by the invention has the beneficial effect that the defects of comprehensive recovery andenvironment-protective treatment of the traditional technical process are overcome.

Patent
02 Mar 2018
TL;DR: In this paper, a cracking-resistant automobile paint consisting of 20-30 parts of nitrocellulose, 10-20 parts of epoxy resin, 5-10 parts of acrylic resin and 1-2 parts of an auxiliary agent was presented.
Abstract: The invention discloses a cracking-resistant automobile paint. The cracking-resistant automobile paint comprises the following components in parts by weight: 20-30 parts of nitrocellulose, 10-20 partsof epoxy resin, 5-10 parts of acrylic resin, 20-40 parts of xylene, 5-10 parts of aluminium hydroxide, and 1-2 parts of an auxiliary agent. By adding aluminium hydroxide and aluminium hydroxide as filling materials, under effect of xylene as a solvent, nitrocellulose, epoxy resin and acrylic resin are uniformly wetted on the surface of aluminium hydroxide, aluminium hydroxide in an automobile paint after solidification provides a structure support, the automobile paint intensity is increased, and cracking can be effectively prevented.

Patent
14 Dec 2018
TL;DR: In this article, a recycling method of a waste lithium iron phosphate battery is provided, which comprises the steps as follows: carrying out discharge and disassembling on the waste lithium IRP battery to obtain a positive plate; dissolving the positive plate in an acid, and after filtering, obtaining filtrate and filter residues; adding ammonium hydroxide into the filtrates, simultaneously stirring until the pH of the obtained solution is 1.0 to 1.6, and obtaining a mixed solution B containing lithium sulfate and aluminum sulfate, and adding a phosphorous compound and
Abstract: The invention provides a recycling method of a waste lithium iron phosphate battery, which comprises the steps as follows: carrying out discharge and disassembling on the waste lithium iron phosphatebattery to obtain a positive plate; dissolving the positive plate in an acid, and after filtering, obtaining filtrate and filter residues; adding ammonium hydroxide into the filtrate, simultaneously stirring until the pH of the obtained solution is 1.0 to 1.6, and obtaining a mixed solution B containing lithium sulfate and aluminum sulfate and ferric phosphate precipitates; adding ammonium hydroxide into the mixed solution B, simultaneously stirring until the pH of the obtained solution is 5.4 to 7.0, and obtaining lithium sulfate filtrate and aluminium hydroxide precipitates; and adding a phosphorous compound and alkali into the lithium sulfate filtrate, stirring until the pH of the obtained solution is 9.0 to 14.0, and after filtering to obtain precipitates, drying to obtain lithium phosphate. The invention further provides a preparation method of a lithium manganese ferric phosphate or lithium iron phosphate cathode material. The prepared lithium phosphate and ferric phosphate are used as raw materials for preparing the lithium manganese ferric phosphate or lithium iron phosphate cathode material.

Patent
22 May 2018
TL;DR: In this paper, a cable material and a preparation method for preparing a flame-retardant cable material was presented. But the preparation method of the cable material is not discussed.
Abstract: The invention relates to a cable material and a preparation method thereof, in particular to a method for preparing a flame-retardant cable material. In the present invention, sodium aluminate solution is neutralized with aluminum sulfate and ultra-fine aluminium hydroxide powder is obtained through gel crystallization. After the aluminum hydroxide powder is modified, the modified aluminum hydroxide powder is blended with other synergistic flame-retardant materials and matrix resin, pelleting is carried out and then hot-pressing is carried out to obtain the flame-retardant cable material. Thesurface of the EVA resin is coated by the aluminum hydroxide powder, and as crystal nuclei are continuously generated, a core-shell structured coated type composite powder is finally formed and functions as a flame retardant. Aluminum hydroxide is packed into the matrix resin to construct a carbonized layer, which can not only prevent heat and oxygen from entering, but also prevent small moleculesof flammable gas from escaping. Red phosphorus reacts with free radicals to inhibit production and degradation of free radicals, and polyphosphoric acid can be obtained during the reaction. Polyphosphoric acid can dehydrate and carbonize the flame-retardant materials, and thus make the cable material difficult to burn. When the matrix resin is burnt, the char yield of the matrix resin is high. The flame-retardant cable material disclosed by the invention has broad application prospects.

Patent
25 May 2018
TL;DR: In this article, a preparation method of a catalyst for methane conversion is described, which consists of zirconium sulfate solid acid, 2-methylimidazole and aluminium hydroxide slurry.
Abstract: The invention discloses a preparation method of a catalyst for methane conversion. The method comprises the following steps: zirconium sulfate solid acid, 2-methylimidazole and aluminium hydroxide slurry are mixed, and aluminium hydroxide slurry containing zirconium sulfate solid acid and 2-methylimidazole is obtained; then the aluminium hydroxide slurry containing zirconium sulfate solid acid and2-methylimidazole performs spray soaking on zinc supported alumina, and the catalyst for methane oxyhalogenation conversion is prepared after drying and roasting. The catalyst prepared with the method has the advantages that methane conversion rate and selectivity of halomethane as a target product are increased simultaneously, deep oxidation of halomethane is inhibited, and yield of halomethaneis increased obviously.

Patent
20 Apr 2018
TL;DR: In this paper, a soft environment-friendly low-smoke halogen-free polyolefin insulating material comprisesthe following components in parts by weight: an ethylene-vinyl acetate copolymer EVA, linear low-density polyethylene LLDPE, polyethylen EPPE, maleic anhydride grafted metallocene polyethylenes, powdered magnesium hydroxide, laminar aluminium hydroxides, polysilazane resin, silicon dioxide aerogel, magnesium stearate, silicone oil, an
Abstract: The invention discloses a soft environment-friendly low-smoke halogen-free polyolefin insulating material. The soft environment-friendly low-smoke halogen-free polyolefin insulating material comprisesthe following components in parts by weight: an ethylene-vinyl acetate copolymer EVA in which the content of VA (vinyl acetate) is 40%, linear low-density polyethylene (metallocene polyethylene) LLDPE, polyethylene EPPE, an ethylene-octene copolymer POE, maleic anhydride grafted metallocene polyethylene, powdered magnesium hydroxide, laminar aluminium hydroxide, polysilazane resin, silicon dioxide aerogel, magnesium stearate, silicone oil, an anti-oxidant, caged phosphate melamine salt, polyphenyl ether, a coupling agent, a lubricant and fluorophosphorous acid. According to the halogen-free efficient flame-retardant polyolefin cable material, the addition of magnesium hydroxide and aluminium hydroxide is reduced, the flame retardancy of a hydroxide can be greatly improved, the influence from addition of a flame retardant on the mechanical property is reduced, the favorable tensile strength is 15 MPa, the favorable elongation at break is 650%, and the mechanical performance of the cable material is further improved.

Patent
11 May 2018
TL;DR: In this paper, the utility model discloses a be used for battery solution circulation and filterable full automatic device of aluminium hydroxide, which comprises a liquid storage tank, aluminium-air cell pile andaluminium hydroxides filter the jar, the liquid storage pot top sets up and supplyes the mouth, inlet and pressure boost import, the bottom sets up drain pipe and aluminium cell pile right side is passed through pipe connection aluminium hydoxide and is filtered the jar.
Abstract: The utility model discloses a be used for battery solution circulation and filterable full automatic device of aluminium hydroxide, which comprises a liquid storage tank, aluminium -air cell pile andaluminium hydroxide filter the jar, the liquid storage pot top sets up and supplyes the mouth, inlet and pressure boost import, the bottom sets up drain pipe and aluminium -air cell pile, aluminium -air cell pile right side is passed through pipe connection aluminium hydroxide and is filtered the jar, aluminium hydroxide filters tank bottoms portion and sets up the deposit discharge port, the topsets up reactant entry and circulating pipe, aluminium hydroxide filters the jar and is soaking tank, jar body bottom sets up and adds the heat stirring device, the circulation of aluminium -air cellelectrolyte is filtered with aluminium hydroxide and is a complete cyclic process at whole in -process, the inlet can supply the higher electrolyte of concentration among the whole cyclic process, andaluminium hydroxide filtration jar can the effective filtration and the deposit of discharging, high durability and convenient use, the power consumption among the whole cyclic process can be solvedto the aluminium -air cell pile simultaneously, make things convenient for the environmental protection more, performance is high.

Patent
08 Jun 2018
TL;DR: In this article, the preparation method of the silver-loaded palygorskite heat-resistant liquid wallpaper is described, in particular the preparation of the wallpaper is related to the technical field of building material preparation.
Abstract: The invention relates to the technical field of building material preparation, in particular to a preparation method of silver-loaded palygorskite heat-resistant liquid wallpaper. According to the preparation method of the silver-loaded palygorskite heat-resistant liquid wallpaper, the silver-loaded palygorskite heat-resistant liquid wallpaper is prepared by taking modified epoxy resin as a matrix, taking a modified self-made nano-silicon dioxide powder, self-made silver-loaded palygorskite and modified aluminium hydroxide as fillers, and taking simethicone, gelatin and the like as auxiliary materials; firstly, the epoxy resin is modified by utilizing a silane coupling agent and diphenyl silanediol; the nano-silicon dioxide powder is subjected to surface modification through a dispersant,a coupling agent and an acidic solution, so that the antibacterial property of the wallpaper is improved; under a high-temperature condition, aluminium hydroxide is modified through a titanate coupling agent, so that the compatibility of the aluminium hydroxide and other filler is improved, the modified aluminium hydroxide is decomposed into aluminium oxide at a high temperature, and the aluminiumoxide can improve the chemical stability and the mechanical strength of glass, reduce a thermal expansion coefficient of the glass and remarkably improve the heat resistance of the liquid wallpaper,and has a wide application prospect.