A metal nanoparticle composition for the fabrication of conductive features. The metal nanoparticle composition advantageously has a low viscosity permitting deposition of the composition by direct-write tools. The metal nanoparticle composition advantageously also has a low conversion temperature, permitting its deposition and conversion to an electrical feature on polymeric substrates.

Metal nanoparticle compositions

A polishing liquid composition includes composite oxide particles containing cerium and zirconium, a dispersing agent, and an aqueous medium. A powder X-ray diffraction spectrum of the composite oxide particles obtained by CuKα1 ray (λ=0.154050 nm) irradiation includes a peak (first peak) having a peak top in a diffraction angle 2θ (θ is a Bragg angle) range of 28.61 to 29.67°, a peak (second peak) having a peak top in a diffraction angle 2θ range of 33.14 to 34.53°, a peak (third peak) having a peak top in a diffraction angle 2θ range of 47.57 to 49.63°, and a peak (fourth peak) having a peak top in a diffraction angle 2θ range of 56.45 to 58.91°. A half-width of the first peak is 0.8° or less.

Polishing liquid composition

The invention relates to a monolithic white light emitting device using wafer bonding or metal bonding. In the invention, a conductive submount substrate is provided. A first light emitter is bonded onto the conductive submount substrate by a metal layer. In the first light emitter, a p-type nitride semiconductor layer, a first active layer, an n-type nitride semiconductor layer and a conductive substrate are stacked sequentially from bottom to top. In addition, a second light emitter is formed on a partial area of the conductive substrate. In the second light emitter, a p-type AlGaInP-based semiconductor layer, an active layer and an n-type AlGaInP-based semiconductor layer are stacked sequentially from bottom to top. Further, a p-electrode is formed on an underside of the conductive submount substrate and an n-electrode is formed on a top surface of the n-type AlGaInP-based semiconductor layer.

White light emitting device

An electrical conductor formed from one or more metallic inks. The electrical conductor comprises a network of interconnected metallic nodes. Each node comprises a metallic composition, e.g., one or more metals or alloys. The network defines a plurality of pores having an average pore volume of less than about 10,000,000 nm3. The electrical conductors advantageously have a high degree of conductivity, e.g., a resistivity of not greater than about 10x the resistivity of the (bulk) metallic composition, which forms the individual nodes.

Printable electrical conductors

Processes for the production of metal nanoparticles. In one aspect, the invention is to a process comprising the steps of mixing a heated first solution comprising a base and/or a reducing agent (e.g., a non-polyol reducing agent), a polyol, and a polymer of vinyl pyrrolidone with a second solution comprising a metal precursor that is capable of being reduced to a metal by the polyol. In another aspect, the invention is to a process that includes the steps of heating a powder of a polymer of vinyl pyrrolidone; forming a first solution comprising the powder and a polyol; and mixing the first solution with a second solution comprising a metal precursor capable of being reduced to a metal by the polyol.

Production of metal nanoparticles

Multi-component particles comprising inorganic nanoparticles distributed in an organic matrix and processes for making and using same. A flowing aerosol is generated that includes droplets of a precursor medium dispersed in a gas phase. The precursor medium contains a liquid vehicle and at least one precursor. At least a portion of the liquid vehicle is removed from the droplets of precursor medium under conditions effective to convert the precursor to the nanoparticles or the matrix and form the multi-component particles.

Multi-component particles comprising inorganic nanoparticles distributed in an organic matrix and processes for making and using same

This invention is directed to security features that are formed, created, printed from inks comprising metallic particles and/or metallic nanoparticles. Preferably, the security feature is a reflective security features that comprises metallic nanoparticles where the reflective security features are formed by a direct-writing process, e.g., an ink jet printing process, using an ink comprising metallic nanoparticles. The invention is also directed to the use of these security features in many applications and to processes for making them.

Security features, their use, and processes for making them

This invention is directed to direct write printed reflective features comprising metallic particles and/or metallic nanoparticles. Preferably, the reflective feature are formed by a direct-writing printing process, e.g., a piezo-electric, thermal, drop-on-demand or continuous ink jet printing process, using an ink comprising metallic particles, e.g., metallic nanoparticles. The invention is also directed to inks suitable for printing such reflective features using a direct write printing process and to processes for making such reflective features.

Ink jet printed reflective features and processes and inks for making them

In one aspect, the process includes providing a precursor medium comprising a liquid vehicle and a precursor to a component, and flame spraying the precursor medium under conditions effective to form a population of nanoparticles, wherein the nanoparticles include the component. The population of nanoparticles, as formed, comprises less than about 5 percent by volume particles having a particle size greater than 1.0 µm. A size distribution of the population of nanoparticles may have a d50 value less than about 500 nm, and it may be unimodal. The size distribution may have a geometric standard deviation of less than about 2. The process may occur continuously for at least four hours or more. Greater than about 90 percent by weight of the precursor to the component in the precursor medium may be converted to the component in the nanoparticles. The process typically occurs in an enclosed flame spray reactor.

Processes for forming nanoparticles in a flame spray system

In a first aspect, the process includes utilizing a precursor medium comprising particles and a nongaseous precursor to form product nanoparticles having a core/shell structure. In another aspect, the process includes utilizing an emulsion precursor medium comprising a nongaseous precursor and two liquid vehicles, wherein one of the liquid vehicles provides desirable thermal effects upon combustion. In another aspect the flame spray process includes modifying solid particles in a flame spray process to change the phase thereof.

Ned Jay Hardman

Papers

Multi-component particles comprising inorganic nanoparticles distributed in an organic matrix and processes for making and using same

Security features, their use, and processes for making them

Ink jet printed reflective features and processes and inks for making them

Processes for forming nanoparticles in a flame spray system

Processes for forming nanoparticles