基礎講座 電気泳動(Electrophoresis)

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50 Years of Image Analysis

This article reports on the International Nanofluid Property Benchmark Exercise, or INPBE, in which the thermal conductivity of identical samples of colloidally stable dispersions of nanoparticles or “nanofluids,” was measured by over 30 organizations worldwide, using a variety of experimental approaches, including the transient hot wire method, steady-state methods, and optical methods. The nanofluids tested in the exercise were comprised of aqueous and nonaqueous basefluids, metal and metal oxide particles, near-spherical and elongated particles, at low and high particle concentrations. The data analysis reveals that the data from most organizations lie within a relatively narrow band (±10% or less) about the sample average with only few outliers. The thermal conductivity of the nanofluids was found to increase with particle concentration and aspect ratio, as expected from classical theory. There are (small) systematic differences in the absolute values of the nanofluid thermal conductivity among the various experimental approaches; however, such differences tend to disappear when the data are normalized to the measured thermal conductivity of the basefluid. The effective medium theory developed for dispersed particles by Maxwell in 1881 and recently generalized by Nan et al. [J. Appl. Phys. 81, 6692 (1997)], was found to be in good agreement with the experimental data, suggesting that no anomalous enhancement of thermal conductivity was achieved in the nanofluids tested in this exercise.

A Benchmark Study on the Thermal Conductivity of Nanofluids

Review of thermal conductivity in composites: Mechanisms, parameters and theory

Evaporating characteristics of sessile droplet on hydrophobic and hydrophilic surfaces

This study examines the effect of environmental and experimental conditions, such as temperature and time, on the wettability properties of titania nanotube (TNT) surfaces fabricated by anodization. The fabricated TNTs are 60–130 nm inner diameter and 7–10  µm height. One-microliter water droplets were used to define the wettability of the TNT surfaces by measuring the contact angles. A digital image analysis algorithm was developed to obtain contact angles, contact radii and center heights of the droplets on the TNT surfaces. Bare titanium foil is inherently less hydrophilic with approximately 60°–80° contact angle. The as-anodized TNT surfaces are more hydrophilic and annealing further increases this hydrophilic property. Furthermore, it was found that the TNT surface became more hydrophobic when aged in air over a period of three months. It is believed that the surface wettability can be changed due to alkane contamination and organic contaminants in an ambient atmosphere. This work can provide guidelines to better specify the environmental conditions that changes surface properties of TNT surfaces and therefore affect their desirable function in specific applications such as orthopedic implants.

http://iopscience.iop.org/article/10.1088/0957-4484/22/31/315704/pdf

Wettability changes of TiO 2 nanotube surfaces

The present study investigates the optical characteristics and the spectral and angular responses of a Kretschmann surface plasmon resonance (SPR) sensor configuration that is widely used in biological and chemical sensing applications. In order to examine the influence of wave interference and optical properties of thin films on angular variation of reflectance at different incident angles, the Kretschmann SPR configurations made of gold films with 30, 52, and 70 nm thicknesses were fabricated and the reflectance was detected using a 633 nm He-Ne laser, θ-2θ rotation stages, and a silicon pin photo-detector. In particular, this study involved the numerical analysis of angular and spectral variation of reflectance estimated using the characteristic transmission matrix (CTM) method. It was found that the SPR sensitivity became highly dependent on the gold film thickness, indicating that in the thinner gold film case, the reflectance was recovered slowly after the SPR angle, whereas as the gold film thickness increased, the magnitude difference between the maximum and the minimum reflectance measured near the SPR angle was smaller than in other cases. From the numerical analysis, it was shown that the phase shift is the most sensitive physical parameter for SPR sensor by comparing estimated FWHM values of reflectance, phase shift, and enhancement of magnetic field intensity. Therefore, it was concluded that an appropriate metal thickness of around 50 nm was found for higher sensitivity.

Spectral and Angular Responses of Surface Plasmon Resonance Based on the Kretschmann Prism Configuration

We report on the wetting dynamics of a 4.3 μL deionized (DI) water droplet impinging on microtextured aluminum (Al 6061) surfaces, including microhole arrays (hole diameter 125 μm and hole depth 125 μm) fabricated using a conventional microcomputer numerically controlled (μ-CNC) milling machine. This study examines the influence of the texture area fraction ϕs and drop impact velocity on the spreading characteristics from the measurement of the apparent equilibrium contact angle, dynamic contact angle, and maximum spreading diameter. We found that for textured surfaces the measured apparent contact angle (CA) takes on values of up to 125.83°, compared to a CA of approximately 80.59° for a nontextured bare surface, and that the spreading factor decreases with the increased texture area fraction because of increased hydrophobicity, partial penetration of the liquid, and viscous dissipation. In particular, on the basis of the model of Ukiwe and Kwok (Ukiwe, C.; Kwok, D. Y.Langmuir2005, 21, 666), we suggest a...

Seong Hyuk Lee

Papers

Evaporating characteristics of sessile droplet on hydrophobic and hydrophilic surfaces

Wettability changes of TiO 2 nanotube surfaces

Spectral and Angular Responses of Surface Plasmon Resonance Based on the Kretschmann Prism Configuration

Dynamic Wetting and Spreading Characteristics of a Liquid Droplet Impinging on Hydrophobic Textured Surfaces

Design and optimization of rotating triboelectric nanogenerator by water electrification and inertia