We present a comprehensive overview of sensor technology exploiting optical whispering gallery mode (WGM) resonances. After a short introduction we begin by detailing the fundamental principles and theory of WGMs in optical microcavities and the transduction mechanisms frequently employed for sensing purposes. Key recent theoretical contributions to the modeling and analysis of WGM systems are highlighted. Subsequently we review the state of the art of WGM sensors by outlining efforts made to date to improve current detection limits. Proposals in this vein are numerous and range, for example, from plasmonic enhancements and active cavities to hybrid optomechanical sensors, which are already working in the shot noise limited regime. In parallel to furthering WGM sensitivity, efforts to improve the time resolution are beginning to emerge. We therefore summarize the techniques being pursued in this vein. Ultimately WGM sensors aim for real-world applications, such as measurements of force and temperature, or alternatively gas and biosensing. Each such application is thus reviewed in turn, and important achievements are discussed. Finally, we adopt a more forward-looking perspective and discuss the outlook of WGM sensors within both a physical and biological context and consider how they may yet push the detection envelope further.

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Whispering gallery mode sensors

An approach to achieve simultaneous measurement of refractive index and temperature is proposed by using a Mach–Zehnder interferometer realized on tapered single-mode optical fiber. The attenuation peak wavelength of the interference with specific order in the transmission spectrum shifts with changes in the environmental refractive index and temperature. By utilizing S-band and C/L-band light sources, simultaneous discrimination of refractive index and temperature with the tapered fiber Mach–Zehnder interferometer is demonstrated with the corresponding sensitivities of −23.188 nm/RIU (refractive index unit) and 0.071 nm/ °C, and −26.087 nm/RIU (blueshift) and 0.077 nm/°C (redshift) for the interference orders of 169 and 144, respectively.

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Tapered fiber Mach–Zehnder interferometer for simultaneous measurement of refractive index and temperature

Fiber optic interferometers to sense various physical parameters including temperature, strain, pressure, and refractive index have been widely investigated. They can be categorized into four types: Fabry-Perot, Mach-Zehnder, Michelson, and Sagnac. In this paper, each type of interferometric sensor is reviewed in terms of operating principles, fabrication methods, and application fields. Some specific examples of recently reported interferometeric sensor technologies are presented in detail to show their large potential in practical applications. Some of the simple to fabricate but exceedingly effective Fabry-Perot interferometers, implemented in both extrinsic and intrinsic structures, are discussed. Also, a wide variety of Mach-Zehnder and Michelson interferometric sensors based on photonic crystal fibers are introduced along with their remarkable sensing performances. Finally, the simultaneous multi-parameter sensing capability of a pair of long period fiber grating (LPG) is presented in two types of structures; one is the Mach-Zehnder interferometer formed in a double cladding fiber and the other is the highly sensitive Sagnac interferometer cascaded with an LPG pair.

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Interferometric Fiber Optic Sensors

The hydrothermal technique provides an excellent possibility for processing of advanced materials whether it is bulk single crystals, or fine particles, or nanoparticles. The advantages of hydrothermal technology have been discussed in comparison with the conventional methods of materials processing. The current trends in hydrothermal materials processing has been described in relation to the concept of soft solution processing, as a single-step low energy consuming fabrication technique. Also some recent developments in multi-energy processing of materials such as microwave-hydrothermal, mechanochemical-hydrothermal, electrochemical-hydrothermal, sonar-hydrothermal, etc. have been discussed. An overview of the past, present and future perspective of hydrothermal technology as a tool to fabricate advanced materials has been given with appropriate examples.

Hydrothermal processing of materials: past, present and future

We propose and demonstrate a thinned fiber based Mach-Zehnder interferometer for multi-purpose sensing applications. The sensor head is formed by all-fiber in-line singlemode-multimode-thinned-singlemode (SMTS) fiber structure, only using the splicing method. The principle of operation relies on the effect that the thinned fiber cladding modes interference with the core mode by employing a multimode fiber as a mode coupler. Experimental results showed that the liquid refractive index information can be simultaneously provided from measuring the sensitivity of the liquid level. A 9.00 mm long thinned fiber sensor at a wavelength of 1538.7228 nm exhibits a water level sensitivity of -175.8 pm/mm, and refractive index sensitivity as high as -1868.42 (pm/mm)/RIU, respectively. The measuring method is novel, for the first time to our knowledge. In addition, it also demonstrates that by monitoring the wavelength shift, the sensor at a wavelength of 1566.4785 nm exhibits a refractive index sensitivity of -25.2935 nm/RIU, temperature sensitivity of 0.0615 nm/°C, and axial strain sensitivity of -2.99 pm/μe, respectively. Moreover, the sensor fabrication process is very simple and cost effective.

All-fiber Mach-Zehnder interferometers for sensing applications

A novel refractive index (RI) sensor based on a fiber Mach-Zehnder interferometer was realized by concatenating two single-mode fiber tapers separated by a middle section. The proposed device had a minimum insertion loss of 3 dB and maximum interferometric extinction ratio over 20 dB. The resolution (0.171 nm) of the two-taper sensor to its surrounding RI change (0.01) was found to be comparable to that (0.252 nm) of similar structures made from an identical long-period gratings pair, and its ease of fabrication makes it a low-cost alternative to existing sensing applications.

Refractive Index Sensing With Mach–Zehnder Interferometer Based on Concatenating Two Single-Mode Fiber Tapers

A simple refractive index sensor based on a Michelson interferometer in a single-mode fiber is constructed and demonstrated. The sensor consists of a single symmetrically abrupt taper region in a short piece of single-mode fiber that is terminated by ~500 nm thick gold coating. The sensitivity of the new sensor is similar to that of a long-period-grating-type sensor, and its ease of fabrication offers a low-cost alternative to current sensing applications.

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Refractive index sensor based on an abrupt taper Michelson interferometer in a single-mode fiber

Mach-Zehnder and Michelson interferometers using core-offset attenuators were demonstrated. As the relative offset direction of the two attenuators in the Mach-Zehnder interferometer can significantly affect the extinction ratio of the interference pattern, single core-offset attenuator-based sensors appear more robust and repeatable. A novel fiber Michelson interferometer refractive index (RI) sensor was subsequently realized by a single core-offset attenuator and a layer of ~ 500-nm gold coating. The device had a minimum insertion loss of 0.01 dB and maximum extinction ratio over 9 dB. The sensitivity (0.333 nm) of the new sensor to its surrounding RI change (0.01) was found to be comparable to that (0.252 nm) of an identical long period gratings pair Mach-Zehnder interferometric sensor, and its ease of fabrication makes it a low-cost alternative to existing sensing applications.

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Single-Mode Fiber Refractive Index Sensor Based on Core-Offset Attenuators

A Mach-Zehnder interferometer with two abrupt single-mode fiber tapers is simulated, constructed, and demonstrated. The interferometer has an insertion loss of 5 dB and an extinction ratio over 15 dB. The interferometer is tested as a strain sensor based on the maximum attenuation wavelength shift with a comparable sensitivity (slope: 2000 nm/ epsiv, R 2 = 0.996) with long-period-grating-type sensor and promises low fabrication cost.

In-Line Abrupt Taper Optical Fiber Mach–Zehnder Interferometric Strain Sensor

Novel in-line single-mode fiber interferometers- Mach-Zehnder and Michelson-have been designed, fabricated, and tested as refractive index (RI) sensors. Abrupt tapers and connector-offset attenuators are proposed as alternatives to long period gratings (LPGs) as mode-coupling mechanisms to transfer optical power between core and cladding modes in optical fiber. The coupling coefficients between core and cladding modes in the proposed designs were calculated using numerical packages and the devices were subsequently implemented using commercially available fusion splicer. For an abrupt taper, most coupling occurs between the LP01 and LP0 m modes, with the first ten modes accounting for 98% of the incident mode energy. For a connector-offset attenuator, coupling mainly occurs between the LP01 and LP1 m modes, with the first ten LP0 m modes and first ten LP1 m modes accounting for 92% of the incident mode energy. In particular, in the case of connector-offset attenuator, the relative direction between the two connector-offsets was found to be very important to the interference performance. Interference patterns were realized in simulation for the interferometers using both mode-coupling mechanisms. Three interferometers were realized in the experiment using abrupt taper-Mach-Zehnder and Michelson-and connector-offset attenuator-Michelson. They showed large extinction ratios (up to 23 dB) and small insertion losses (smaller than 3 dB). Although it is difficult to make Mach-Zehnder interferometers using connector-offset attenuator pair due to the lack of polarization control in the fusion splicer, some evidence of constructive interference was observed in the experiment. The interferometers were tested as RI sensors using the maximum attenuation wavelength shift. Given that the minimum resolution of optical spectrum analyzer is 10 pm, ~ 10-4 difference of RI can be detected by the proposed interferometric sensors, providing similar performance as LPG-based interferometers at a lower cost and simpler fabrication process.

Zhaobing Tian

Papers

Refractive Index Sensing With Mach–Zehnder Interferometer Based on Concatenating Two Single-Mode Fiber Tapers

Refractive index sensor based on an abrupt taper Michelson interferometer in a single-mode fiber

Single-Mode Fiber Refractive Index Sensor Based on Core-Offset Attenuators

In-Line Abrupt Taper Optical Fiber Mach–Zehnder Interferometric Strain Sensor

In-Line Single-Mode Optical Fiber Interferometric Refractive Index Sensors