Chloridobis(ethyl-enediamine-κN,N')(n-pentyl-amine-κN)cobalt(III) dichloride monhydrate.
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...For related structures, see: Anbalagan et al. (2009); Lee et al. (2007); Ramesh et al. (2008); Ravichandran et al. (2009)....
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...…= (Fo2 + 2Fc2)/3 S = 1.10 (Δ/σ)max = 0.006 5510 reflections Δρmax = 0.52 e Å−3 181 parameters Δρmin = −0.35 e Å−3 3 restraints Extinction correction: SHELXL97 (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 Primary atom site location: structure-invariant direct methods Extinction…...
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"Chloridobis(ethyl-enediamine-κN,N')..." refers background in this paper
...Bruker Kappa-APEX2 CCD diffractometer Absorption correction: multi-scan (Blessing, 1995) Tmin = 0.719, Tmax = 0.816 23262 measured reflections 5510 independent reflections 4506 reflections with I > 2 (I) Rint = 0.029...
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...…Radiation source: fine-focus sealed tube 4506 reflections with I > 2σ(I) Monochromator: graphite Rint = 0.029 T = 293 K θmax = 30.7º ω and φ scans θmin = 1.7º Absorption correction: multi-scan (Blessing, 1995) h = −15→15 Tmin = 0.719, Tmax = 0.816 k = −8→10 23262 measured reflections l = −33→33...
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