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Journal ArticleDOI

GC-MS characterization of proteinaceous and lipid binders in UV aged polychrome artifacts

TLDR
In this paper, the most significant results obtained from the characterization of protein and lipid binders in a broad range of reference paint materials prepared and stored at Opificio delle Pietre Dure in Florence were compared with those relevant to old paintings of different ages, and showed that UV light aging does not significantly affect the amino acid profile of protein binders.
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This article is published in Microchemical Journal.The article was published on 2000-12-01. It has received 94 citations till now. The article focuses on the topics: Oleic acid & Azelaic acid.

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Citations
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Analytical investigation of calcium oxalate films on marble monuments.

TL;DR: The correlation between organic material and oxalate contents suggests the origin of the films from degradation processes of past surface treatment.
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Characterisation of proteinaceous binders in artistic paintings by chromatographic techniques

TL;DR: This review discusses the application of chromatographic techniques (GC, HPLC and Py-GC) for the characterisation of proteinaceous materials in artistic paintings, including various methods of hydrolysis and derivatisation for GC and HPLC.
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Analytical chemistry in the field of cultural heritage

TL;DR: A review of analytical chemistry in the field of cultural heritage can be found in this paper, where a large number of analytical methodologies and tools (molecular and elemental spectroscopic techniques, chemometrics, chemical reactivity and modeling, etc.) are used to define: (a) the impacts of environmental stressors (natural and anthropogenic), (b) the decaying (chemical reactions) pathways of such materials in the surrounding environment, (c) the development of new remediation (cleaning, consolidation, rehabilitation, etc.).
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Analytical pyrolysis of proteins in samples from artistic and archaeological objects

TL;DR: In this paper, a study of proteins found in artistic and archaeological objects based on analytical pyrolysis was presented, in order to overcome limitations of wet chemical methods arising from the reduced solubility of aged proteins in samples of cultural heritage.
References
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Book

Organic Chemistry of Museum Objects

TL;DR: The Organic Chemistry of Museum Objects as mentioned in this paper is a survey of the chemical composition, properties and analysis of the whole range of organic materials incorporated into objects and artworks found in museum collections.
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The organic chemistry of museum objects

TL;DR: In this article, the causes and prevention of deterioration in practice of organic chemistry are discussed. But the authors do not discuss the effects of these causes on the performance of their analysis in practice.
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The Gas Chromatographic Examination of Paint Media. Part I. Fatty Acid Composition and Identification of Dried Oil Films

TL;DR: In this paper, the authors present a gas chromatographic examination of paint media and identify the Fatty Acid composition and identification of Dried Oil Films, which is the basis for this paper.
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Characterisation of proteinaceous binders and drying oils in wall painting samples by gas chromatography–mass spectrometry

TL;DR: In this paper, a reliable analytical procedure has been developed for the characterisation of drying oils and proteinaceous binders in samples of painted artworks, which is based on microwave assisted acid hydrolysis followed by the extraction of the lipid component with diethyl ether.
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Gas chromatographic-mass spectrometric approach to the problem of characterizing binding media in paintings

TL;DR: In this paper, a GC-MS method was proposed for the characterization of binding media in paint works of art, based on the determination of amino acids and fatty acids after hydrolysis with HC1 and derivatization with 2-propanol and trifluoroacetic anhydride.
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