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Metal injection molding of nanostructured W-Cu composite powder

J.-C Kim, +3 more
- 01 Jan 1999 - 
- Vol. 35, Iss: 4, pp 47-55
TLDR
In this paper, a debinding cycle was identified which resulted in a high surface quality of the bionic parts, shape retention, and complete removal of binder, and an intermediate isostatic repressing step increased bionic density but did not contribute significantly to densification during sintering.
Abstract
Nanostructured W-Cu composite powder was fabricated by mechanical alloying. Compacts were then prepared from the powder in the as-milled conditions, and after a thermal reduction treatment, by metal injection molding using a multicomponent wax/polyethylene/stearic acid binder system. A debinding cycle was identified which resulted in a high surface quality of the bionic parts, shape retention, and complete removal of the binder. An intermediate isostatic repressing step increased the bionic density but did not contribute significantly to densification during sintering. Densities >96% of theorical were achieved in the injection molded compacts for both powder conditions via liquid phase sintering, notwithstanding the low brown density after debinding. This high sinterability is attributed to grain growth of the W and a double rearrangement process in the powder due to its intrinsic nanostructural characteristics.

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Fabrication of metal matrix composites by metal injection molding—A review

TL;DR: In this paper, the status of the research and development in fabricating metal matrix composites by MIM is reviewed, with a major focus on material systems, fabrication methods, resulting material properties and microstructures.
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Solid state and liquid phase sintering of mechanically activated W–20 wt.% Cu powder mixture

TL;DR: In this paper, the effect of mechanical alloying on the sintering response of composite compacts was investigated and the densification, microstructure, hardness, and electrical conductivity after solid phase Sintering (SPS) and liquid phase sinterings (LPS) were examined.
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Effects of tungsten particle size and copper content on densification of liquid-phase-sintered W-Cu

TL;DR: In this paper, the authors evaluate the effects of Cu volume fraction and particle size on liquid-phase sintering of W-Cu and show that particle rearrangement is limited for low Cu volume fractions and large W particle sizes.
Journal ArticleDOI

Preparation of W-Cu alloy with high density and ultrafine grains by mechanical alloying and high pressure sintering

TL;DR: In this article, the changes of morphology and structural evolution of W-Cu powders during mechanical alloying process were observed and studied, and the effects of temperature and pressure on the density of sintered compacts were studied.
Journal ArticleDOI

Structural changes during synthesizing of nanostructured W–20 wt% Cu composite powder by mechanical alloying

TL;DR: In this paper, the morphological changes and structural evolution of the composite powder during MA was studied by employing scanning electron microscopy (SEM), X-ray diffraction (XRD), energy dispersive Xray (EDX), laser particle size analyzer (LPS), inductively coupled plasma (ICP) spectrometry, atomic absorption spectrophotometery (AAS), and the bulk powder density measurement.
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