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Molybdenum Sulphur Chemistry
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This article is published in Studies in Inorganic Chemistry.The article was published on 1994-01-01. It has received 1 citations till now. The article focuses on the topics: Molybdenum.read more
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Journal ArticleDOI
Preparation and crystal structure of [Mo{S2P(OMe)2}3] and an improved route to [MoCl3(thf)3]
Jonathan R. Dilworth,Jon Zubieta +1 more
TL;DR: The complex [MoCl3(thf)3] as mentioned in this paper ] is prepared in high yield by the tin reduction of [NH4][S2P(OMe)2] in thf.
Journal ArticleDOI
Preparation and redox properties of the cuboidal molybdenum(III) aqua ion [Mo4S4(H2O)12]4+
TL;DR: In this paper, a procedure for the electrochemical preparation of the orange cuboidal MoIII aqua ion [Mo4S4(H2O)12]4+(peak 378 nm; Iµ= 1 100 M-1 cm-1 per Mo4) from Mo4S 4(H 2O) 12]5+(reduction potential 210 mV) is described.
Journal ArticleDOI
Preparation and X-ray crystal structure analysis of a novel, trinuclear nitrido complex [{Et2NCS2)3MoN}2Mo(S2CNEt2)3]3+[PF6–]3
TL;DR: In this paper, the structure of MoN(S2CNEt2)3 with NaBF4 in methanol has been determined by X-ray diffraction.
Journal ArticleDOI
Crystal and molecular structure of diaquahydrogen(I)µ-oxo-[bis(diethyldithiocarbamato)oxomolybdate(IV)][bis(diethyldithiocarbamato)oxomolybdenum(V)] bis{µ-oxo-bis[bis(diethyldithiocarbamato)oxomolybdenum(V)]}(1), and µ-oxo-bis[bis(diethyldithiocarbamato)oxomolybdenum(V)](2), and the single-crystal electron spin resonance spectrum of (1)
TL;DR: In this paper, the authors used the heavy-atom method and refined the result to R 0.052 using 2 340 reflections, which is the state-of-the-art.