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Journal ArticleDOI

Solid phase extractive preconcentration of uranium on to 5,7-dichloroquinoline- 8-ol modified naphthalene

Joseph Mary Gladis, +1 more
- 27 Mar 2002 - 
- Vol. 35, Iss: 3, pp 501-515
TLDR
In this paper, the preparation of solid reagent, (5,7dichloroquinoline-8-ol) modified naphthalene for preconcentration of uranium is described.
Abstract
The preparation of solid reagent, (5,7-dichloroquinoline-8-ol) modified naphthalene for preconcentration of uranium is described. The uranium-5,7-dichloroquinoline-8-ol complex is quantitatively re...

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Citations
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Journal ArticleDOI

Preconcentration techniques for uranium(VI) and thorium(IV) prior to analytical determination-an overview.

TL;DR: Various off-line and on-line procedures developed for uranium(VI) and thorium(IV) prior to their analytical determination since 1990 were critically reviewed in terms of enrichment factor, retention/sorption capacity, validation using certified reference materials and application to complex real samples.
Journal ArticleDOI

Amberlite XAD-4 functionalized with succinic acid for the solid phase extractive preconcentration and separation of uranium(VI).

TL;DR: The accuracy of the developed solid phase extractive preconcentration method in conjunction with Arsenazo III procedure was tested by analyzing marine sediment and soil reference material and has been successfully employed for the analysis of soil and sediment samples.
Journal ArticleDOI

Removal of uranium(VI) ions from aqueous solutions using Schiff base functionalized SBA-15 mesoporous silica materials

TL;DR: Thermodynamic investigations revealed that the adsorption of uranyl ions by the adsorbents was spontaneous and endothermic and the maximum adsorbent capacity was 54 and 105.3 mg uranyl/g adsorent, respectively.
Journal ArticleDOI

Solid phase extractive preconcentration of uranium(VI) onto diarylazobisphenol modified activated carbon

TL;DR: The above procedure has been successfully employed for analysis of uranium(VI) in soil and sediment samples and in conjunction with the Arsenazo III procedure was tested by analysing MESS-3, a marine sediment certified reference material.
Journal ArticleDOI

Synthesis of salicylaldehyde-modified mesoporous silica and its application as a new sorbent for separation, preconcentration and determination of uranium by inductively coupled plasma atomic emission spectrometry.

TL;DR: The sorbent exhibited excellent stability and its sorption capacity under optimum conditions has been found to be 10mg of uranium per gram of sorbent, and the method was applied for the recovery and determination of uranium in different water samples.
References
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Journal ArticleDOI

Solid phase extraction of ultra trace copper(II) using octadecyl silica membrane disks modified by a naphthol-derivative Schiff’s base

TL;DR: In this article, a simple and reliable method for the extraction and determination of ultra trace amounts of copper(II) ions using octadecyl-bonded silica membrane disks modified by a recently synthesized Schiff's base (2,2′-[1,2-ethanediyl bis(nitriloethylidyne)] bis(1-naphthalene)) and atomic absorption spectrometry is presented.
Journal ArticleDOI

Determination of picomolar concentrations of titanium, gallium and indium in sea water by inductively coupled plasma mass spectrometry following an 8-hydroxyquinoline chelating resin preconcentration

TL;DR: In this article, the authors measured the concentrations of dissolved titanium, gallium and indium in sea water using inductively coupled plasma mass spectrometry (ICP-MS) after concentration and separation from the major ions via an 8-hydroxyquinoline chelating ion exchange resin (TSK-8HQ).
Book

Enrichment techniques for inorganic trace analysis

敦 水池
TL;DR: In this paper, the authors discuss the applicability and limitations of enrichment techniques combined with instrumental determination techniques for trace analysis of natural waters and gaseous samples, and the final two chapters are devoted to special enrichment techniques used in trace analyses.
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