scispace - formally typeset
Open AccessJournal Article

Synthesis ,characterization and antibacterial activity of mixed ligand complexes of some metals with 1-nitroso-2-naphthol and L-phenylalanine

N.K. Fayad, +2 more
- 01 Jan 2012 - 
- Vol. 2, Iss: 5, pp 18-29
TLDR
The mixed ligand complexes of Mn(II),FeFe(II ), Co(II,Ni(II) and Cd (II) with 1-nitroso-2-naphthol (NNPhH) and amino acid L-phenylalanine (C 9 H 10 NO 2 ) were synthesized and characterized by Melting points, Solubility, Molar conductivity as mentioned in this paper.
Abstract
The mixed ligand complexes of Mn(II),Fe(II ), Co(II),Ni(II),Cu(II), Zn(II) and Cd (II) with 1-nitroso-2-naphthol (C 10 H 7 NO 2 ), symbolized (NNPhH)] and amino acid L-phenylalanine ( C 9 H 10 NO 2 ) , symbolized ( phe H),  were synthesized and characterized by: Melting points, Solubility, Molar conductivity. determination the percentage of the metal in the complexes by flame(AAS), Molecular weight determined by  Rast’s Camphor method, susceptibility measurements, Spectroscopic Method [FT-IR and UV-Vis], And Program  [Chem office– CS .Chem.– 3D pro 2006] was used for draw compounds . The results showed that the deprotonated   two  ligands acts as a bidentate ligand ,  ( phe - ) was coordinated to the metal ions through the oxygen  of  the  carboxylic  group  and  the nitrogen of the amine and  the 1-nitroso-2-naphthol ligand was coordinated to the metal ions through the oxygen and nitrogen atoms. The electronic absorption spectra and magnetic susceptibility measurements of the complexes indicate octahedral geometry for all the complexes. Key words: phenyl alanine , amino acid) Complexes ,  1-nitroso-2-naphthol  ,mixed ligands   and Antibacterial     Activities

read more

Content maybe subject to copyright    Report

Citations
More filters
Journal ArticleDOI

Textbook of biochemistry with clinical correlations

TL;DR: This beautifully illustrated and well-written book, with an impressive array of authors, is aimed at both undergraduate and postgraduate level and emphasises the biochemistry of mammalian cells.
Journal ArticleDOI

An insight into the conformal flexibility and vibrational behavior of 2-nitroso-1-naphthol: A density functional theory approach

TL;DR: In this paper, the conformational stability of 2-nitrosol-1-naphthol (2N1N) was elucidated using potential energy surface scan studies.
Journal Article

Synthesis, Characterization, and Antibacterial Studies of Mn (II) , Fe (II) , Co(II) , Ni(II), Cu (II) and Cd(II) Mixed- Ligand Complexes Containing Amino Acid ( L-Valine) And (1,10- phenanthroline)

TL;DR: A new six mixed Ligand complexes of some transition metal ions Mn (II), Fe (II), Co(II) , Co( II) , Ni(II), Cu(ii)and non transition metal ion Cd(II)) with L-valine (Val H) as a primary LIGand and 1,10-phenanthroline (phen) as an secondary Ligands have been prepared.
Journal Article

Preparation , Characterization and Antimicrobial activities of {Fe(II),Co(II),Ni(II),Cu(II),and Zn(II)}Mixed Ligand Complexes Schiff base derived from Cephalexin drug and 4(dimethylamino)benzaldehyde with Nicotinamide

TL;DR: In this paper, a Schiff base ligand was obtained from 1:1:2 molar ratio reactions with metal ions and HL, 2NA on reaction with MCl 2.nH 2 O salt.
Journal Article

A Comparative Study of Microwave Assisted and Conventional Synthesis of Mixed Ligand Complexes with Cr(III), Co(II), Ni(II) Cu(II) and Cd(II)

TL;DR: In this paper, the primary ligand 2-amino acetic acid -6- chloro benzothiazole (L) was prepared as a chelating ligand, which was treated with the ions Cr(III), Co(II), Ni(II) Cu(II).
References
More filters
Book

Infrared and Raman Spectra of Inorganic and Coordination Compounds

TL;DR: In this article, the normal modes of vibration are illustrated and corresponding vibrational frequencies are listed for each type, including diatomic, triatomic, fouratomic, five-atomic, six-atomic and seven-atomic types.
Book

Advanced Inorganic Chemistry

TL;DR: Cotton and Wilkinson's Advanced Inorganic Chemistry (AIC) as discussed by the authors is one of the most widely used inorganic chemistry books and has been used for more than a quarter century.
Book

Spectrometric identification of organic compounds

TL;DR: In this paper, a sequence of procedures for identifying an unknown organic liquid using mass, NMR, IR, and UV spectroscopy is presented, along with specific examples of unknowns and their spectra.
Book

The infra-red spectra of complex molecules

TL;DR: In this article, the authors present a survey of research work in physics, physical sciences, and physical chemistry, focusing on physics, chemistry, physics, and biology. But they do not discuss their work in this paper.
Related Papers (5)