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How to make nitride boron ceramic? 


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To make nitride boron ceramic, several methods can be employed based on the desired properties of the ceramic. One method involves using boron nitride powder and boron oxide powder in specific proportions for sintering through double-heating-mode, ensuring uniform temperature fields . Another approach combines boron nitride and boron carbide powders, followed by vacuum sintering to create a boron nitride-boron carbide composite ceramic with high strength and toughness . Additionally, a method involving nitridation sintering after pre-pressing forming is utilized to produce nitride modified boron carbide composite ceramic with enhanced density, bending strength, and hardness . For high-strength boron nitride ceramic, nano cubic boron nitride powder is sintered using spark plasma or hot-pressing equipment . Lastly, a low-oxygen-content boron nitride ceramic is prepared by heat treatment and hot pressing sintering with nitrogen introduction to reduce oxygen content .

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To make nitride boron ceramic, heat treat boron nitride powder in an atmosphere, then conduct hot pressing sintering while introducing nitrogen to reduce oxygen content to less than 0.1 wt%.
To make high-strength boron nitride ceramic, use single-particle-size nano cubic boron nitride powder, conduct pre-pressing forming, then sinter in spark plasma or hot-pressing equipment, and finally cool and demold.
Boron nitride ceramic is made from 95-99% boron nitride powder and 1-5% boron oxide powder through double-heating-mode sintering involving current and radiation heating, achieving high density and compactness.
To make boron nitride-boron carbide composite ceramic, mix boric acid and urea, ball mill, heat at 950-1200°C for boron nitride powder, then add boron carbide, ball mill, and sinter.
The nitride modified boron carbide composite ceramic is made by matching ceramic raw materials, pre-pressing forming, and vacuum nitridation sintering, resulting in high density, bending strength of 338 MPa, and hardness of 32.10 GPa.

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How to produce boron nitride from molten salt?5 answersBoron nitride (BN) can be produced from molten salt through various methods. One approach involves the synthesis of BN nanosheets in molten KCl–NaCl salt media using a single precursor compound, ethylenediamine bisborane, heated to 1000 °C for two minutes. Another method includes the preparation of carbon-doped BN (BCN) nanosheets at 1100 °C in molten LiCl-KCl using boric acid, melamine, and glucose as starting materials. Additionally, BN can be electrodeposited from B2O3 in NaCl–CaCl2 under N2 atmosphere, with a theoretical decomposition voltage range of −1.73 to −1.66 V at 800–1000 °C. Furthermore, BN nanosheets can be synthesized by heating a mixture of alkali borohydride and an ammonium salt to at least 500°C, with NaN3 potentially included to enhance yield.
What is the effect of boron nitride on the strength and ductility of metals?5 answersThe addition of boron nitride (BN) to metal matrix composites can have a significant effect on their strength and ductility. In the case of Ti-4Al-3Mo-1V alloys, the inclusion of trace amounts of boron (0.01-0.1 wt.%) leads to the refinement of the microstructure and improved superplasticity, resulting in high elongation and strain rate sensitivity. Boron also accelerates recrystallization and globularization of the microstructure, reducing flow stress values and increasing post-forming yield strength. In Ti-Nb-microalloyed steels, boron addition improves hot ductility during cooling and lowers the austenite-to-ferrite transformation temperature, preventing the formation of intergranular ferrite and brittle zones. However, the effect of boron on strength and ductility can vary depending on the alloy composition. High levels of boron (>1%) can deteriorate superplastic properties and decrease ductility. Additionally, the distribution state of boron in weld metals can affect their tensile and creep ductility, with boron segregation at grain boundaries enhancing ductility.
How can hexagonal boron nitride be synthesized?5 answersHexagonal boron nitride (h-BN) can be synthesized using various methods. One approach is the chemical vapor deposition (CVD) method, where the substrate is heated at a first temperature and then exposed to precursors containing boron and nitrogen at a specific partial pressure and temperature. Another method is the dual temperature zone low-pressure CVD, where a single ammonia borane precursor is used on a non-catalytic substrate. The growth rate and crystal quality of h-BN films can be controlled by adjusting the position in the dual temperature zone. Scalable approaches for high-quality h-BN synthesis have been reviewed, highlighting the challenges of maintaining stoichiometric balance and stacking order between layers. Controllable synthesis of h-BN using CVD has been explored to achieve full control over domain size, orientation, morphology, layer number, and stacking order. These methods provide a basis for the preparation of large area wafer thick h-BN films and the utilization of h-BN in various applications.
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How to make ceramic coating better?5 answersTo make ceramic coating better, several methods can be employed. One approach is to use a ceramic surface coating method that involves preparing a paint with specific raw materials, coating the ceramic with the paint, and roasting it at a high temperature. Another method is to improve the ceramic cutter coating by using a combination of thermoplastic plastics, silicon nitride, bamboo powder, molybdenum powder, and other raw materials. Additionally, a coating method using an acrylic emulsion type clear coating can be applied to the ceramic substrate to enhance the leveling properties and thickness of the coating film. Another technique involves depositing a ceramic coating on a substrate by heating a ceramic material with an electron beam source, which improves the evaporation rate and results in an improved ceramic coating. Finally, a high hardness wear-resistant and weather-resistant metal ceramic coating can be prepared by mixing and melting alumina and silica, cross-linking polyurethane, and incorporating graphite and fluorine-containing polymer particles.

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